CN210251327U - Water diversion equipment in preparation process of direct addition type high-performance cobalt salt adhesion promoter - Google Patents
Water diversion equipment in preparation process of direct addition type high-performance cobalt salt adhesion promoter Download PDFInfo
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- CN210251327U CN210251327U CN201921091446.4U CN201921091446U CN210251327U CN 210251327 U CN210251327 U CN 210251327U CN 201921091446 U CN201921091446 U CN 201921091446U CN 210251327 U CN210251327 U CN 210251327U
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- separation
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- cobalt salt
- water diversion
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Abstract
The utility model discloses a water diversion equipment in direct addition type high performance cobalt salt binding increaser preparation process, locate including separation cauldron, level separation grid tray of lower half in the separation cauldron, wear to locate separation cauldron upper cover passes the charge-in pipeline of separation grid tray, separation cauldron inner chamber quilt separation grid tray separates into cavity and lower cavity, separation grid tray includes last grid tray, lower grid tray and wears to locate perpendicularly the separation pipeline between last grid tray and the lower grid tray, through the separation pipeline will go up the cavity with cavity intercommunication down, the separation cauldron bottom is equipped with the branch water gap, separation cauldron upper portion lateral wall is equipped with the branch hydraulic fluid port. The utility model provides an oil water separator increases the area of contact of one section synthetic fraction and the synthetic fraction of two-stage process and pipe wall, can accelerate the separation, improves the separation effect.
Description
Technical Field
The utility model belongs to the technical field of the production of promoter is binded to the cobalt salt, a production facility of promoter is binded to the cobalt salt is related to, the water diversion equipment in the promoter preparation process is binded to concretely relates to direct addition type high performance cobalt salt.
Background
In the rubber product industries such as radial steel wire tires, steel wire reinforced conveyer belts, steel braided rubber tubes and the like, the rubber-metal adhesion promoters commonly used at home and abroad at present are direct addition type cobalt salt adhesion promoters, and the main varieties of the adhesion promoters are cobalt neodecanoate, cobalt boroacylate and the like. The direct addition type cobalt salt adhesion promoter not only has high-strength adhesion performance and excellent dynamic mechanical property, but also has excellent performances of ageing resistance, thermal oxygen resistance, humidity resistance, salt water corrosion resistance and the like.
The patent CN106832401B granted by this company provides a direct-addition type high-performance cobalt salt adhesion promoter and a preparation method thereof, in the preparation process, distillation is required during the first-stage synthesis and the second-stage synthesis, and after the fraction is divided into water, the distillate is continuously refluxed to the reaction system in order to perform the next reaction.
SUMMERY OF THE UTILITY MODEL
To prior art not enough, the utility model aims to provide a divide water equipment in the improver preparation process is glued to direct addition type high performance cobalt salt, this equipment increase the area of contact of one section synthetic and two-stage process synthetic fraction and pipe wall, under the prerequisite of guaranteeing high separation precision, realize carrying out the water treatment of serialization to the fraction of one section synthesis and two-stage process synthesis in the improver preparation process is glued to direct addition type high performance cobalt salt.
The utility model discloses a realize through following technical scheme:
the water diversion equipment comprises a separation kettle, a separation grid plate horizontally arranged at the inner lower half part of the separation kettle, and a feed pipeline penetrating through the upper cover of the separation kettle and penetrating through the separation grid plate, wherein the inner cavity of the separation kettle is divided into an upper cavity and a lower cavity by the separation grid plate, the separation grid plate comprises an upper grid plate, a lower grid plate and a separation pipeline vertically penetrating between the upper grid plate and the lower grid plate, the upper cavity is communicated with the lower cavity through the separation pipeline, a water diversion port is formed in the bottom of the separation kettle, and a oil diversion port is formed in the side wall of the upper part of the separation kettle.
Furthermore, the separation pipeline is provided with a plurality of separation pipelines which are uniformly distributed.
Furthermore, the upper opening of the separation pipeline is flush with the upper surface of the upper grid plate, and the lower opening of the separation pipeline is flush with the lower surface of the lower grid plate.
The fraction of one section synthesis and two-section synthesis enters into the lower cavity of the separation kettle through the feeding pipeline, then rises through the densely distributed separation pipeline and enters into the upper cavity, the fraction is layered gradually in the rising process, the separation can be accelerated when the fraction of one section synthesis and two-section synthesis contacts with the pipe wall, the contact area of the fraction with the pipe wall is increased when the fraction passes through the densely distributed separation pipeline, therefore, the separation efficiency is accelerated, after the layering is finished, the organic phase is separated by opening the switch of the oil separation port, and the water phase is discharged by opening the switch of the water separation port.
Furthermore, an exhaust pipe is obliquely arranged above the side wall of the feeding pipeline, and an included angle between the central line of the exhaust pipe and the central line of the feeding pipeline is 30-60 degrees. The fraction of one section synthesis and two-section synthesis can bring uncondensed organic solvent gas in the pipeline in the process of conveying, if gas enters the separation grid plate and stays, the separation effect will be influenced, and therefore the exhaust pipe is arranged obliquely above the side wall of the feeding pipeline, gas is discharged in time, and the separation effect is guaranteed.
Further, the exhaust pipe is positioned in the separation kettle. When the feeding speed is too fast or too much in the feeding process of the fractions synthesized in the first section and the second section and overflows from the exhaust pipe, the fractions fall into the separation kettle, and the pollution to the environment is avoided.
Further, the outer side wall of the separation kettle is vertically provided with a liquid level meter. The liquid level meter is used for controlling the amount of fractions of the first-stage synthesis and the second-stage synthesis of each batch treatment, and the gas outlet of the gas exhaust pipe is ensured to be positioned above the liquid level.
Furthermore, the side wall of the separation kettle is provided with a sight glass with a lamp, and the sight glass with a lamp is convenient for observing the layering condition in the separation kettle.
Furthermore, the sight glass with the lamp and the oil distribution port are positioned on the same horizontal line. And the water-oil boundary and the oil layer separation condition can be conveniently observed during oil separation.
Furthermore, the lower part of the lower grid plate of the separation kettle is a cone. The vertebral body is more beneficial to water and oil stratification.
Furthermore, a support is arranged on the outer side wall of the separation kettle.
The utility model has the advantages that:
the utility model discloses set up the separation grid tray, one section synthetic and the synthetic fraction of two-stage process pass through the separation pipeline, with pipe wall surface contact for oil-water separation, under the prerequisite of guaranteeing the high separation precision, realize handling one section synthetic and the synthetic fraction of two-stage process in batches.
The utility model discloses be equipped with the blast pipe in the syncline top of charge-in pipeline lateral wall, in time get rid of the gas that contains in the waste water system, guarantee the separation effect, reduce the potential safety hazard.
The utility model discloses an exhaust pipe is located the separation cauldron, and feed rate is too fast or too much in one section synthetic fraction feeding process with the two-stage process, when spilling over from the exhaust pipe, falls into the separation cauldron, avoids the pollution to the environment.
The utility model discloses dispose the level gauge, the volume of the fraction of one section synthesis of not only steerable every batch processing and two-section synthesis is convenient for guarantee moreover that the gas outlet of blast pipe is located more than the liquid level.
The utility model discloses the configuration is taken the lamp sight glass, is convenient for observe the layering condition in the separation cauldron, moreover, is convenient for observe the water oil boundary and the oil reservoir condition of dividing during the branch oil.
The utility model discloses a part sets up to the centrum below separation cauldron's the lower grid tray, more is favorable to the layering of profit, further improves the separation precision.
Drawings
Fig. 1 is a schematic structural view of the present invention;
FIG. 2 is a schematic view of the external structure of one side of the separation kettle of the present invention;
FIG. 3 is a schematic view of the external structure of the other side of the separation kettle of the present invention;
fig. 4 is a top view of the present invention;
FIG. 5 is a top view of a separation grid according to the present invention;
the device comprises a separation kettle 1, an upper cavity 11, a lower cavity 12, a water diversion port 13, an oil diversion port 14, a separation grid plate 2, an upper grid plate 21, a lower grid plate 22, a separation pipeline 23, a feeding pipeline 3, an exhaust pipe 4, a liquid level meter 5, a sight glass with a lamp 6, a support 7 and a vent 8.
Detailed Description
The present invention will be further described with reference to the following specific examples.
As shown in fig. 1, the water diversion device in the preparation process of the direct addition type high-performance cobalt salt adhesion promoter comprises a separation kettle 1, a separation grid plate 2 horizontally arranged at the inner lower half part of the separation kettle 1, and a feed pipeline 3 penetrating through the upper cover of the separation kettle 1 and penetrating through the separation grid plate 2, wherein the inner cavity of the separation kettle 1 is divided into an upper cavity 11 and a lower cavity 12 by the separation grid plate 2, the discharge port of the feed pipeline 3 is positioned in the lower cavity 12, the separation grid plate 2 comprises an upper grid plate 21, a lower grid plate 22 and a separation pipeline 23 vertically penetrating between the upper grid plate 21 and the lower grid plate 22, the upper cavity 11 is communicated with the lower cavity 12 through the separation pipeline 23, the bottom of the separation kettle 1 is provided with a water diversion port 13, and the upper side wall of the separation kettle.
In the embodiment, 44 separation pipelines 23 are uniformly and densely distributed between the upper grid plate 21 and the lower grid plate 22; the upper opening of the separation pipe 23 is flush with the upper surface of the upper grid plate 21, and the lower opening of the separation pipe 23 is flush with the lower surface of the lower grid plate 22.
As shown in fig. 1, an exhaust pipe 4 is arranged obliquely upward on the upper side wall of the feed pipe 3, the outlet of the exhaust pipe 4 is positioned in the separation kettle 1, and the included angle between the central line of the exhaust pipe 4 and the central line of the feed pipe 3 is 30-60 °.
As shown in fig. 2 and 3, a liquid level meter 5 is vertically arranged on the outer side wall of the separation kettle 1, a sight glass 6 with a lamp is arranged on the side wall of the separation kettle 1, and the sight glass 6 with a lamp and the oil distribution port 14 are located on the same horizontal line.
In this embodiment, the lower part of the lower grid plate 22 of the separation kettle 1 is a cone, the outer side wall of the separation kettle 1 is provided with a support 7, and the upper cover of the separation kettle 1 is provided with a vent 8.
The oil-water separator is used for treating wastewater, and the method comprises the following specific steps: during the synthesis process of the cobalt salt adhesion promoter, fractions synthesized in a first section and synthesized in a second section enter a lower cavity 12 of a separation kettle 1 through a feeding pipeline 3, then ascend through a densely distributed separation pipeline 23 and enter an upper cavity 11, the fractions are gradually layered in the ascending process, the separation can be accelerated when the fractions are in contact with the pipe wall, the contact area of the fractions with the pipe wall is increased when the fractions pass through the densely distributed separation pipeline 23, the separation efficiency is accelerated, the layering condition is observed through a sight glass 6 with a lamp, after the layering is finished, a switch of an oil separation port 14 is opened to separate an organic phase, and the organic phase is input into the next reaction through a pipeline. Then the switch of the water separation port 13 is opened to discharge the water phase.
Claims (10)
1. The water diversion equipment in the preparation process of the direct addition type high-performance cobalt salt adhesion promoter comprises a separation kettle (1), a separation grid plate (2) horizontally arranged at the inner lower half part of the separation kettle (1), and a feeding pipeline (3) which is arranged on the upper cover of the separation kettle (1) in a penetrating way and penetrates through the separation grid plate (2), the inner cavity of the separation kettle (1) is divided into an upper cavity (11) and a lower cavity (12) by the separation grid plate (2), it is characterized in that the separation grid plate (2) comprises an upper grid plate (21), a lower grid plate (22) and a separation pipeline (23) vertically arranged between the upper grid plate (21) and the lower grid plate (22) in a penetrating way, the upper chamber (11) is communicated with the lower chamber (12) through the separation duct (23), the bottom of the separation kettle (1) is provided with a water diversion port (13), and the side wall of the upper part of the separation kettle (1) is provided with an oil diversion port (14).
2. The water diversion device in the preparation process of the direct addition type high-performance cobalt salt adhesion promoter according to claim 1, characterized in that: the separation pipelines (23) are uniformly distributed.
3. The water diversion device in the preparation process of the direct addition type high-performance cobalt salt adhesion promoter according to any one of claims 1 or 2, characterized in that: the upper opening of the separation pipeline (23) is flush with the upper surface of the upper grid plate (21), and the lower opening of the separation pipeline (23) is flush with the lower surface of the lower grid plate (22).
4. The water diversion device in the preparation process of the direct addition type high-performance cobalt salt adhesion promoter according to claim 1, characterized in that: an exhaust pipe (4) is obliquely arranged above the side wall of the upper part of the feeding pipeline (3), and an included angle between the central line of the exhaust pipe (4) and the central line of the feeding pipeline (3) is 30-60 degrees.
5. The water diversion device in the preparation process of the direct addition type high-performance cobalt salt adhesion promoter according to claim 4, characterized in that: the exhaust pipe (4) is positioned in the separation kettle (1).
6. The water diversion device in the preparation process of the direct addition type high-performance cobalt salt adhesion promoter according to claim 1, characterized in that: the outer side wall of the separation kettle (1) is vertically provided with a liquid level meter (5).
7. The water diversion device in the preparation process of the direct addition type high-performance cobalt salt adhesion promoter according to claim 1, characterized in that: the side wall of the separation kettle (1) is provided with a sight glass (6) with a lamp.
8. The water diversion device in the preparation process of the direct addition type high-performance cobalt salt adhesion promoter according to claim 7, characterized in that: the sight glass with the lamp (6) and the oil distribution port (14) are positioned on the same horizontal line.
9. The water diversion device in the preparation process of the direct addition type high-performance cobalt salt adhesion promoter according to claim 1, characterized in that: the lower part of the lower grid plate (22) of the separation kettle (1) is a cone.
10. The water diversion device in the preparation process of the direct addition type high-performance cobalt salt adhesion promoter according to claim 1, characterized in that: the outer side wall of the separation kettle (1) is provided with a support (7), and the upper cover of the separation kettle (1) is provided with a vent (8).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201921091446.4U CN210251327U (en) | 2019-07-12 | 2019-07-12 | Water diversion equipment in preparation process of direct addition type high-performance cobalt salt adhesion promoter |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201921091446.4U CN210251327U (en) | 2019-07-12 | 2019-07-12 | Water diversion equipment in preparation process of direct addition type high-performance cobalt salt adhesion promoter |
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| Publication Number | Publication Date |
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| CN210251327U true CN210251327U (en) | 2020-04-07 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201921091446.4U Active CN210251327U (en) | 2019-07-12 | 2019-07-12 | Water diversion equipment in preparation process of direct addition type high-performance cobalt salt adhesion promoter |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113428936A (en) * | 2021-07-03 | 2021-09-24 | 河北金谷再生资源开发有限公司 | Treatment facility of biodiesel waste water |
-
2019
- 2019-07-12 CN CN201921091446.4U patent/CN210251327U/en active Active
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113428936A (en) * | 2021-07-03 | 2021-09-24 | 河北金谷再生资源开发有限公司 | Treatment facility of biodiesel waste water |
| CN113428936B (en) * | 2021-07-03 | 2023-01-06 | 河北金谷再生资源开发有限公司 | Treatment facility of biodiesel waste water |
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