CN210186892U - High-concentration ammonia water configuration device for sulfonamide synthesis - Google Patents

High-concentration ammonia water configuration device for sulfonamide synthesis Download PDF

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Publication number
CN210186892U
CN210186892U CN201920964257.7U CN201920964257U CN210186892U CN 210186892 U CN210186892 U CN 210186892U CN 201920964257 U CN201920964257 U CN 201920964257U CN 210186892 U CN210186892 U CN 210186892U
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fixedly connected
machine body
rotating rod
organism
servo motor
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CN201920964257.7U
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Liudi Zhao
赵六弟
Weiwen Qian
钱炜雯
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Wu Gan Pharmaceutical (suzhou) Co Ltd
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Wu Gan Pharmaceutical (suzhou) Co Ltd
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Abstract

The utility model relates to a synthetic high concentration aqueous ammonia configuration device of using of sulfanilamide, which comprises a bod, the lateral wall all is equipped with the moving mechanism of dewatering effect before the both ends of organism, outer wall fixedly connected with L shape bracing piece of organism, the one end fixedly connected with servo motor of organism is kept away from to L shape bracing piece, servo motor's the terminal fixedly connected with of drive shaft runs through the first rotation pole of organism, first rotation pole and the coaxial fixed connection of moving mechanism, coaxial fixedly connected with drive mechanism on the first rotation pole, the transmission is connected with rabbling mechanism on the drive mechanism, cavity is equipped with in the rabbling mechanism, be equipped with the intake pipe in the cavity, the upper end fixedly connected. The utility model discloses a servo motor's rotation can carry out the breakage to the bubble that aquatic produced well, makes the ammonia in the bubble fully fuse with water, has increased the efficiency of aqueous ammonia preparation, drives the actinobacillus wheel through servo motor and rotates, carries out the dewatering to organism both ends lateral wall repeatedly.

Description

High-concentration ammonia water configuration device for sulfonamide synthesis
Technical Field
The utility model relates to an aqueous ammonia configuration technical field especially relates to a synthetic high concentration aqueous ammonia configuration device of using of sulfanilamide.
Background
The synthesis of sulfanilamide generally adopts high-concentration ammonia water, the ammonia water is generally prepared by directly introducing ammonia gas into water to fully fuse the ammonia gas and the water, and the fused ammonia water is used for synthesizing sulfanilamide.
In the prior art, the efficiency of ammonia dissolving in water is too low, and because water is put into the device for a long time, the toilet surface of the device can generate a lot of water vapor to influence the production of ammonia, therefore, the device for preparing ammonia water with high concentration for sulfanilamide synthesis is provided, and the problems are solved.
Disclosure of Invention
The utility model aims at solving the defects existing in the prior art and providing a high-concentration ammonia water configuration device for sulfanilamide synthesis.
In order to achieve the above purpose, the utility model adopts the following technical scheme:
the utility model provides a synthetic high concentration aqueous ammonia configuration device of using of sulfonamide, includes the organism, the lateral wall all is equipped with the moving mechanism of dewatering effect before the both ends of organism, organism outer wall fixedly connected with L shape bracing piece, the one end fixedly connected with servo motor of organism is kept away from to L shape bracing piece, servo motor's the terminal fixedly connected with of drive shaft runs through the first rotation pole of organism, first rotation pole and the coaxial fixed connection of moving mechanism, coaxial fixedly connected with drive mechanism on the first rotation pole, the last transmission of drive mechanism is connected with rabbling mechanism, be equipped with well cavity in the rabbling mechanism, be equipped with the intake pipe in the well cavity, the upper end fixedly connected with check valve of intake pipe, the intercommunication is equipped with the gas inlet bottle on the check valve, the top surface fixed connection of gas inlet bottle and.
Preferably, the moving mechanism comprises a sliding groove arranged on the side wall of the front end of the machine body, a sliding block matched with the sliding groove is arranged in the sliding groove in a sliding mode, a spring is fixedly connected to the lower end of the sliding block, the lower end of the spring is fixedly connected with the bottom of the sliding groove, a sliding rod is fixedly connected to the side wall of the sliding block, a water removing brush is fixedly connected to one end, away from the sliding block, of the sliding rod, a steel wire line is fixedly connected to the lower end of the water removing brush, a pay-off wheel is fixedly connected to one end, away from the water removing brush, of the steel wire line.
Preferably, the transmission mechanism comprises a first helical gear coaxially and fixedly arranged outside the first rotating rod, a second helical gear is meshed on the first helical gear, the center of the second helical gear is fixedly connected with a second rotating rod penetrating through the L-shaped supporting rod, a first belt pulley is coaxially and fixedly connected outside the second rotating rod, and the first belt pulley is in transmission connection with the stirring mechanism.
Preferably, rabbling mechanism includes the second belt pulley of transmission connection on first belt pulley, coaxial fixedly connected with runs through the third dwang of organism top surface in the second belt pulley, the lower extreme fixedly connected with agitator disk of third dwang.
Preferably, the lower end of the machine body is provided with a roller.
Preferably, the gas inlet cylinder is fixedly connected with the top surface of the machine body through a fixing plate.
Compared with the prior art, the beneficial effects of the utility model are that:
1. the utility model discloses a servo motor's rotation drives the agitator disk and rotates, can carry out the breakage to the bubble that the aquatic produced well, makes the ammonia in the bubble fully fuse with water, has increased the efficiency of aqueous ammonia preparation.
2. The utility model discloses a servo motor drives the actinobacillus wheel and rotates, and the actinobacillus wheel twines the steel wire line on it, makes the downstream of dewatering brush, because the resettability of spring and servo motor's positive and negative rotation make the dewatering brush rebound, has realized that the dewatering brush can be at the effect that the organism both ends lateral wall reciprocated, carries out the dewatering to organism both ends lateral wall repeatedly, prevents that organism both ends lateral wall from being covered with the configuration efficiency that steam influences the ammonia.
Drawings
FIG. 1 is a perspective view of a device for preparing high-concentration ammonia water for sulfonamide synthesis according to the present invention;
FIG. 2 is an enlarged view of a portion of FIG. 1 at A;
fig. 3 is a partially enlarged view of B in fig. 1.
In the figure: the automatic stirring device comprises a machine body 1, a moving mechanism 2, a 3L-shaped supporting rod, a servo motor 4, a first rotating rod 5, a transmission mechanism 6, a stirring mechanism 7, a hollow cavity 8, an air inlet pipe 9, a check valve 10, an air inlet bottle 11, a sliding chute 12, a sliding block 13, a spring 14, a sliding rod 15, a water removing brush 16, a steel wire 17, a wire paying-off wheel 18, a first helical gear 19, a second helical gear 20, a second rotating rod 21, a first belt pulley 22, a second belt pulley 23, a third rotating rod 24 and a stirring disc 25.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments.
In the description of the present invention, it is to be understood that the terms "upper", "lower", "front", "rear", "left", "right", "top", "bottom", "inner", "outer", and the like indicate orientations or positional relationships based on the orientations or positional relationships shown in the drawings, and are only for convenience of description and simplicity of description, and do not indicate or imply that the device or element being referred to must have a particular orientation, be constructed and operated in a particular orientation, and therefore, should not be construed as limiting the present invention.
Referring to fig. 1-3, a synthetic high concentration aqueous ammonia configuration device of using of sulfanilamide, including organism 1, lateral wall all is equipped with the moving mechanism 2 of dewatering effect before the both ends of organism 1, 1 outer wall fixedly connected with L shape bracing piece 3 of organism, and the one end fixedly connected with servo motor 4 of organism 1, servo motor 4's model are kept away from to L shape bracing piece 3: ACSM80-G01330LZ, the end fixedly connected with of drive shaft of servo motor 4 runs through the first rotation pole 5 of organism 1, first rotation pole 5 and the coaxial fixed connection of moving mechanism 2, coaxial fixedly connected with drive mechanism 6 on the first rotation pole 5, the last transmission of drive mechanism 6 is connected with rabbling mechanism 7, be equipped with well cavity 8 in the rabbling mechanism 7, be equipped with intake pipe 9 in the well cavity 8, the upper end fixedly connected with check valve 10 of intake pipe 9, the air input of ammonia can be controlled to check valve 10, the configuration is suitable for the aqueous ammonia of concentration, the intercommunication is equipped with into gas cylinder 11 on the check valve 10, the top surface fixed connection of gas cylinder 11 and organism 1, it passes through the top surface fixed connection of fixed plate and organism 1 to enter gas cylinder 11, it is for supporting admits gas cylinder 11 admits air, prevent that intake pipe 10 from moving down, the lower extreme.
Wherein, moving mechanism 2 is including setting up spout 12 at organism 1 front end lateral wall, it is equipped with rather than assorted slider 13 to slide in spout 12, slider 13 slides from top to bottom in spout 12, the lower extreme fixedly connected with spring 14 of slider 13, the lower extreme and the spout 12 bottom fixed connection of spring 14, the effect that sets up spring 14 is in order to cooperate servo motor 4's use to resume slider 13 to the original position, slider 13 lateral wall fixedly connected with slide bar 15, slide bar 15 keeps away from the one end fixedly connected with brush 16 that removes water of slider 13, the lower extreme fixedly connected with steel wire line 17 of brush 16 removes water, the one end fixedly connected with actinobacillus wheel 18 that removes water brush 16 is kept away from to steel wire line 17, actinobacillus wheel 18 can twine steel wire line 17 onto it, the center and the coaxial fixed connection of first rotor lever 5 of actinobacillus wheel 18.
Wherein, drive mechanism 6 includes coaxial fixed setting in the first helical gear 19 outside first dwang 5, and the meshing has second helical gear 20 on the first helical gear 19, and second helical gear 20 center fixedly connected with runs through the second dwang 21 of L shape bracing piece 3, sets up L shape bracing piece 3 and is in order to support second dwang 21 and fixed driving motor 4, and the outer coaxial fixedly connected with first belt pulley 22 of second dwang 21, first belt pulley 22 is connected with 7 transmissions of rabbling mechanisms.
Rabbling mechanism 7 includes that the transmission is connected in the second belt pulley 23 on first belt pulley 22, and first belt pulley 22 passes through the belt and is connected with the transmission of second belt pulley 23, and coaxial fixedly connected with runs through the third dwang 24 of 1 top surface of organism in the second belt pulley 23, and the lower extreme fixedly connected with agitator disk 25 of third dwang 24, agitator disk 25 are the fretwork setting, can carry out the breakage to the bubble of the ammonia of getting into water, can effectual improvement aqueous ammonia and the mixing efficiency of water.
In the utility model, when ammonia water is prepared, the single valve 10 is opened, the air inlet bottle 11 filled with ammonia gas is positioned at the upper end of the one-way valve 10, the ammonia gas in the air inlet bottle 11 enters the water in the machine body 1 through the air inlet pipe 9 and is fused with the water, because the ammonia gas can generate a plurality of bubbles when entering the water, the servo motor 4 is opened at the moment, the servo motor 4 drives the first rotating rod 5 to rotate, the first rotating rod 5 drives the first helical gear 19 to rotate, the first helical gear 19 drives the second helical gear 20 to rotate, the second helical gear 20 drives the second rotating rod 21 to rotate, the second rotating rod 21 drives the first belt pulley 22 to rotate, the first belt pulley 22 drives the second belt pulley 23 to rotate through a belt, the second belt pulley 23 drives the third rotating rod 24 to rotate, the third rotating rod 24 drives the stirring disc 25 to rotate, the bubbles are stirred, and the ammonia gas is fully contacted with the water, the configuration efficiency of aqueous ammonia has been improved, and simultaneously, servo motor 4 drives actinobacillus wheel 18 and rotates, and actinobacillus wheel 18 winding steel wire line 17 will remove water brush 16 and move down along the direction of spout 12, carries out a clearance to the steam on the both ends lateral wall of organism 1, because spring 14's reset action and servo motor 4 can positive and negative rotation, remove water brush 16 and resume after the normal position and continue to move down, go on repeatedly above-mentioned step, clear up repeatedly the steam of organism 1 both ends outer wall.
The above, only be the concrete implementation of the preferred embodiment of the present invention, but the protection scope of the present invention is not limited thereto, and any person skilled in the art is in the technical scope of the present invention, according to the technical solution of the present invention and the utility model, the concept of which is equivalent to replace or change, should be covered within the protection scope of the present invention.

Claims (6)

1. The high-concentration ammonia water configuration device for sulfonamide synthesis comprises a machine body (1) and is characterized in that moving mechanisms (2) with a water removing effect are arranged on the front side walls of the two ends of the machine body (1), an L-shaped supporting rod (3) is fixedly connected to the outer wall of the machine body (1), a servo motor (4) is fixedly connected to one end, far away from the machine body (1), of the L-shaped supporting rod (3), a first rotating rod (5) penetrating through the machine body (1) is fixedly connected to the tail end of a driving shaft of the servo motor (4), the first rotating rod (5) is fixedly connected with the moving mechanisms (2) in a coaxial mode, a transmission mechanism (6) is fixedly connected to the first rotating rod (5) in a coaxial mode, a stirring mechanism (7) is connected to the transmission mechanism (6) in a rotating mode, a hollow cavity (8) is arranged in the stirring mechanism (7), the upper end of the air inlet pipe (9) is fixedly connected with a one-way valve (10), an air inlet cylinder (11) is communicated with the one-way valve (10), and the air inlet cylinder (11) is fixedly connected with the top surface of the machine body (1).
2. The device for preparing high-concentration ammonia water for sulfanilamide synthesis according to claim 1, the moving mechanism (2) comprises a sliding chute (12) arranged on the side wall of the front end of the machine body (1), a sliding block (13) matched with the sliding groove (12) is arranged in the sliding groove (12) in a sliding way, the lower end of the sliding block (13) is fixedly connected with a spring (14), the lower end of the spring (14) is fixedly connected with the bottom of the sliding groove (12), the side wall of the sliding block (13) is fixedly connected with a sliding rod (15), one end of the sliding rod (15) far away from the sliding block (13) is fixedly connected with a water removing brush (16), the lower end of the dewatering brush (16) is fixedly connected with a steel wire (17), one end of the steel wire (17) far away from the dewatering brush (16) is fixedly connected with a paying-off wheel (18), the center of the paying-off wheel (18) is coaxially and fixedly connected with the first rotating rod (5).
3. The device for configuring high-concentration ammonia water for sulfonamide synthesis according to claim 1, wherein the transmission mechanism (6) comprises a first helical gear (19) coaxially and fixedly arranged outside the first rotating rod (5), a second helical gear (20) is meshed on the first helical gear (19), a second rotating rod (21) penetrating through the L-shaped supporting rod (3) is fixedly connected to the center of the second helical gear (20), a first belt pulley (22) is coaxially and fixedly connected outside the second rotating rod (21), and the first belt pulley (22) is in transmission connection with the stirring mechanism (7).
4. The device for preparing high-concentration ammonia water for sulfonamide synthesis according to claim 3, wherein the stirring mechanism (7) comprises a second belt pulley (23) in transmission connection with the first belt pulley (22), a third rotating rod (24) penetrating through the top surface of the machine body (1) is coaxially and fixedly connected in the second belt pulley (23), and a stirring disc (25) is fixedly connected at the lower end of the third rotating rod (24).
5. The device for preparing high-concentration ammonia water for sulfanilamide synthesis according to claim 1, wherein the lower end of the machine body (1) is provided with a roller.
6. The device for preparing high-concentration ammonia water for sulfonamide synthesis according to claim 1, wherein the gas inlet cylinder (11) is fixedly connected with the top surface of the machine body (1) through a fixing plate.
CN201920964257.7U 2019-06-25 2019-06-25 High-concentration ammonia water configuration device for sulfonamide synthesis Active CN210186892U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201920964257.7U CN210186892U (en) 2019-06-25 2019-06-25 High-concentration ammonia water configuration device for sulfonamide synthesis

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201920964257.7U CN210186892U (en) 2019-06-25 2019-06-25 High-concentration ammonia water configuration device for sulfonamide synthesis

Publications (1)

Publication Number Publication Date
CN210186892U true CN210186892U (en) 2020-03-27

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Family Applications (1)

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CN201920964257.7U Active CN210186892U (en) 2019-06-25 2019-06-25 High-concentration ammonia water configuration device for sulfonamide synthesis

Country Status (1)

Country Link
CN (1) CN210186892U (en)

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