CN210125184U

CN210125184U - Distillation equipment

Info

Publication number: CN210125184U
Application number: CN201920581748.3U
Authority: CN
Inventors: 施云勇
Original assignee: Zaoyang Hongsheng Chemical Co Ltd
Current assignee: Zaoyang Hongsheng Chemical Co Ltd
Priority date: 2019-04-26
Filing date: 2019-04-26
Publication date: 2020-03-06
Anticipated expiration: 2029-04-26

Abstract

The utility model discloses a distillation device, which comprises a distillation retort and a sealing cover, wherein the sealing cover is sleeved at the top position of the distillation retort, the utility model is additionally provided with a fixing frame and a heating rod on the basis of the existing device, when a user uses liquid raw materials, the user can heat the raw materials by taking the heating rod as a main heating groove as an auxiliary heating groove to promote distillation reaction, thus effectively improving the working efficiency of the utility model, when the user uses the solid raw materials, the user can place the solid raw materials on a steaming tray, then place the steaming tray on the fixing frame, and heat the heating groove by an external heat source to promote the distillation reaction in the distillation retort, the utility model is additionally provided with an observation device on the basis of the existing device, and the user can confirm the residual water in the heating groove by the observation device at any time in the heating process of the heating groove, the occurrence of dry burning and other conditions is effectively avoided.

Description

Distillation equipment

Technical Field

The utility model belongs to the technical field of the chemical industry equipment is relevant, concretely relates to distillation equipment.

Background

The distillation equipment is a separation technology carried out under the condition of high vacuum, and has the characteristics of low distillation temperature, high system vacuum degree, short material heating time, high separation degree and the like; and the separation process is irreversible, and no boiling bubbling phenomenon exists. Is not suitable for separating high boiling point, heat-sensitive and easily oxidized substances, and has been widely applied to various industries such as extraction of vitamins and effective components of Chinese herbal medicines in the pharmaceutical industry, petrochemical industry, food industry, cosmetic industry, agriculture and the like.

The prior distillation equipment technology has the following problems: the existing distillation equipment is more suitable for liquid raw materials and powdery raw materials, solid raw materials can be adhered to the inner wall of the equipment when being placed in the distillation equipment for reaction, the water quantity in a heating groove is inconvenient for a user to observe in the use process of the existing distillation equipment, the user needs to supplement the water quantity according to work experience, and the work difficulty of the user is increased.

SUMMERY OF THE UTILITY MODEL

An object of the utility model is to provide a distillation plant to solve the solid formula raw materials that proposes among the above-mentioned background art and be not suitable for and be not convenient for observe the problem of the interior water yield of heating bath.

In order to achieve the above object, the utility model provides a following technical scheme: the utility model provides a distillation equipment, includes retort and closing cap, the closing cap has been cup jointed to the top position department of retort, the cooling tube has been cup jointed to the top intermediate position department of closing cap, the holding vessel has been cup jointed to the other end position department of cooling tube, the welding of the bottom position department of holding vessel has the holding vessel support, the left side bottom position department of retort is provided with the outlet, the right side bottom position department of retort sets up by the water injection pipe, the intermediate position department of water injection pipe has cup jointed the fixed bolster, the other end welding of fixed bolster is in the right side intermediate position department of retort, the bottom left side position department of water injection pipe is provided with viewing device, the welding of the bottom position department of retort has the retort support.

Preferably, the cooling pipe comprises a transmission pipe, a liquid injection port, a cooling box, a storage tank interface, a liquid discharge port and a distillation tank interface, the distillation tank interface is arranged at the bottom of the left side of the transmission pipe, the storage tank interface is arranged at the bottom of the right side of the transmission pipe, the cooling box is arranged at the middle position of the transmission pipe, the liquid injection port is arranged at the left side of the top of the cooling box, and the liquid discharge port is arranged at the left side of the bottom of the cooling box.

Preferably, the viewing device includes mounting groove, top mount, observation pipe, bottom mount, mounting bracket and communicating pipe, the intermediate position department of mounting bracket is provided with the mounting groove, the left side position department of mounting bracket is provided with communicating pipe, the right side top position department of mounting bracket is provided with the top mount, and the right side bottom position department of mounting bracket is provided with the bottom mount, right side position department between top mount and the bottom mount is provided with the observation pipe.

Preferably, the retort includes charge door, heating rod, a jar body, mount, heating tank and interlayer board, the top left side position department of the jar body is provided with the charge door, position department is provided with the interlayer board to the lower side in the middle of the inside of the jar body, the heating rod has been cup jointed to the top intermediate position department of interlayer board, the below position department of interlayer board is provided with the heating tank, the inside both sides position department of the jar body is provided with the mount.

Preferably, the storage tank has a height of 600cm and a diameter of 480 mm.

Preferably, the size of the distillation tank is 860mm in height and 670mm in diameter.

Preferably, the left side position department of top mount and bottom mount all is provided with communicating pipe, the one end position department of communicating pipe is in the left side of mounting bracket, and the other end position department of communicating pipe is connected with the observation pipe.

Preferably, the fixing frames are provided with three pairs, and the sizes and the shapes of the three pairs of fixing frames are the same.

Compared with the prior art, the utility model provides a distillation plant possesses following beneficial effect:

1. the utility model discloses installed mount and heating rod additional on current equipment basis, the user is when using liquid formula raw materials, and the user can use the heating rod to heat promotion distillation reaction as the assistance to the raw materials as the main heating groove, can effectual improvement the utility model discloses a work efficiency, when the user uses solid formula raw materials, the user can place solid formula raw materials on the steaming tray, then places the steaming tray on the mount, then heats the heating inslot through external heat source, promotes to carry out the distillation reaction in the retort, the effectual problem of avoiding solid formula raw materials inconvenient carrying out the reaction in the retort.

2. The utility model discloses installed viewing device additional on current equipment basis, the user is at the in-process through the heating of heating bath, and the user can confirm the surplus of the interior water yield of heating bath through viewing device at any time, the effectual appearance of having avoided the condition such as dry combustion method to appear.

Drawings

The accompanying drawings are included to provide a further understanding of the invention, and are incorporated in and constitute a part of this specification, illustrate embodiments of the invention, and together with the description, do not constitute a limitation of the invention, in which:

FIG. 1 is a schematic structural view of a distillation apparatus according to the present invention;

fig. 2 is a schematic view of a cooling tube structure according to the present invention;

fig. 3 is a schematic structural view of an observation device provided by the present invention;

FIG. 4 is a schematic structural view of a distillation tank provided by the present invention;

in the figure: 1. a cooling tube; 2. a storage tank; 3. a holding tank support; 4. a retort support; 5. an observation device; 6. a water injection pipe; 7. fixing a bracket; 8. a water outlet; 9. a distillation tank; 10. sealing the cover; 11. a conveying pipe; 12. a liquid injection port; 13. a cooling tank; 14. a storage tank interface; 15. a liquid discharge port; 16. a retort interface; 51. mounting grooves; 52. a top mount; 53. an observation tube; 54. a bottom mount; 55. a mounting frame; 56. a communicating pipe; 91. a feed inlet; 92. a heating rod; 93. a tank body; 94. a fixed mount; 95. a heating tank; 96. a division plate.

Detailed Description

The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.

Referring to fig. 1-4, the present invention provides a technical solution: a distillation device comprises a distillation tank 9 and a sealing cover 10, the sealing cover 10 is sleeved at the top position of the distillation tank 9, the distillation tank 9 comprises a feed inlet 91, a heating rod 92, a tank body 93, a fixing frame 94, a heating groove 95 and a interlayer plate 96, the feed inlet 91 is arranged at the left side position of the top of the tank body 93, the interlayer plate 96 is arranged at the lower middle position of the inside of the tank body 93, the heating rod 92 is sleeved at the middle position of the top of the interlayer plate 96, the heating groove 95 is arranged at the lower position of the interlayer plate 96, the fixing frames 94 are arranged at the two side positions of the inside of the tank body 93, the distillation tank 9 is a main working device of the utility model, the feed inlet 91 can assist a user to add liquid body type raw materials in the working process of the utility model, the heating rod 92 can carry out rapid heating, the working efficiency of the utility model is improved, the tank body 93 is a main structure device, the fixing frame 94 can be used for placing a steaming tray and other auxiliary solid raw materials, the heating tank 95 can be filled with tap water and the like for heating, the interlayer plate 96 is a device for fixedly installing the heating rod 92, the interior of the tank body 93 is divided into two parts, the heating tank 95 is formed below the tank body 93, the cooling pipe 1 is sleeved at the middle position of the top of the sealing cover 10, the cooling pipe 1 comprises a transmission pipe 11, a liquid injection port 12, a cooling box 13, a storage tank interface 14, a liquid discharge port 15 and a distillation tank interface 16, the distillation tank interface 16 is arranged at the bottom position of the left side of the transmission pipe 11, the storage tank interface 14 is arranged at the bottom position of the right side of the transmission pipe 11, the cooling box 13 is arranged at the middle position of the transmission pipe 11, the liquid injection port 12 is arranged at the left side position of the top of the cooling box 13, the liquid discharge port 15 is arranged at the left side position of the bottom of the cooling box 13, the cooling pipe 1 can cool, the conveying pipe 11 is used for conveying raw materials separated by distillation reaction in the distillation retort 9, the liquid injection port 12 is used for injecting cooling liquid into the cooling box 13, the cooling box 13 can be filled with the cooling liquid to cool the raw materials separated by distillation reaction in the distillation retort 9, the storage tank interface 14 is used for connecting and fixing the cooling pipe 1 and the storage tank 2 together, the liquid discharge port 15 is used for discharging the cooling liquid in the cooling box 13, the distillation retort interface 16 is used for connecting and fixing the cooling pipe 1 to the distillation retort 9, the storage tank 2 is sleeved at the position of the other end of the cooling pipe 1, the storage tank support 3 is welded at the position of the bottom of the storage tank 2, the water discharge port 8 is arranged at the position of the bottom of the left side of the distillation retort 9, the water injection pipe 6 is arranged at the position of the bottom of the right side of the distillation retort 9, the fixing support 7 is sleeved at the position of the middle position of the water injection pipe 6, the other end of the, the observation device 5 is arranged at the left position of the bottom of the water injection pipe 6, the observation device 5 comprises a mounting groove 51, a top fixing frame 52, an observation pipe 53, a bottom fixing frame 54, a mounting frame 55 and a communicating pipe 56, the mounting groove 51 is arranged at the middle position of the mounting frame 55, the communicating pipe 56 is arranged at the left position of the mounting frame 55, the top fixing frame 52 is arranged at the top position of the right side of the mounting frame 55, the bottom fixing frame 54 is arranged at the bottom position of the right side of the mounting frame 55, the observation pipe 53 is arranged at the right position between the top fixing frame 52 and the bottom fixing frame 54, the observation device 5 is a device for assisting a user to observe the water quantity in the heating tank 95, the mounting groove 51 and the mounting frame 55 are devices for installing and fixing the observation device 5 into the distillation retort 9, and the top fixing frame 52 and the, the observation tube 53 is a device for assisting a user in observing the amount of water in the heating tank 95, the connection tube 56 is a device for connecting and fixing the observation tube 53 and the heating water in the heating tank 95, and the retort support 4 is welded at the bottom of the retort 9.

Further, the storage tank 2 has a height of 600cm and a diameter of 480mm, and can effectively store the raw material separated by the distillation reaction in the distillation tank 9.

Further, the size of retort 9 is height 860mm, diameter 670mm, can effectual improvement the utility model discloses the working capacity that the single produced.

Further, the left side position department of top mount 52 and bottom mount 54 all is provided with communicating pipe 56, and the one end position department of communicating pipe 56 is in the left side of mounting bracket 55, and the other end position department of communicating pipe 56 is connected with observation pipe 53, adopts above-mentioned setting can be effectual with the water in the heating tank 95 and observe pipe 53 and communicate, and convenient to use person observes the surplus of the interior water yield of heating tank 95.

Further, three pairs of fixing frames 94 are provided, and the three pairs of fixing frames 94 are identical in size and shape.

The utility model discloses a theory of operation and use flow: after the utility model is installed, the user firstly checks whether the external appearance of the utility model is intact, confirms that the utility model is in a normal working state, then the user moves the utility model to a position where the utility model is needed to be used, then the storage tank bracket 3 and the distillation tank bracket 4 of the utility model are placed downwards at the position where the utility model is used, the user firstly carries out preparation work according to the type of raw materials used in the working process, the user can carry out main heating work through the heating rod 92 when the liquid raw materials are used, then the user opens the sealing cover 10, then the raw materials are poured into the distillation tank 9, then the user installs and fixes the sealing cover 10 on the distillation tank 9, then the user adds cooling liquid into the cooling box 13 through the liquid injection port 12, then the user connects the distillation tank interface 16 of the cooling pipe 1 to the distillation tank 9, then connects and fixes the storage tank interface 14 of the cooling pipe 1 to the storage tank 2, then the user starts the utility model, the heating rod 92 starts to heat the raw material in the distillation retort 9 to promote the distillation reaction, meanwhile, the user can add tap water and the like into the heating tank 95 through the water injection pipe 6 to carry out auxiliary heating, the distillation reaction is carried out after the raw material in the distillation retort 9 is heated, the separated raw material can enter the storage tank 2 through the cooling pipe 1, then in the process of passing through the cooling pipe 1, the raw material can be cooled under the assistance of the cooling box 13 when passing through the transmission pipe 11 and then enters the storage tank 2, meanwhile, in the working process of the utility model, the user can add the liquid raw material into the tank body 93 through the feed inlet 91, when the user uses the solid raw material, the user firstly takes the heating rod 92 off from the interlayer 96 plate, then the user places the solid raw material on the steaming tray, then places the steaming tray on the fixing frame 94 in the tank body 93, subsequently, tap water for heating or the like is supplied into the heating tank 95 through the water supply pipe 6, and then the user places an external heat source or the like at the bottom of the retort 9, the external heat source heats the water source in the heating tank 95 at the bottom of the retort 9, the heated water source raises the temperature above the partition plate 96 in the tank 93 to promote the distillation reaction of the raw material in the tank 93, and during the heating operation, the user can confirm the amount of the water for heating remaining in the heating tank 95 through the observation device 5, and the user can replenish the water at any time through the water supply pipe 6.

Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims

1. A retort apparatus comprising a retort (9) and a closure (10), characterized in that: a sealing cover (10) is sleeved at the top position of the distillation retort (9), a cooling pipe (1) is sleeved at the middle position of the top of the sealing cover (10), a storage tank (2) is sleeved at the other end of the cooling pipe (1), a storage tank support (3) is welded at the bottom of the storage tank (2), a water outlet (8) is arranged at the bottom of the left side of the distillation retort (9), a water injection pipe (6) is arranged at the bottom of the right side of the distillation retort (9), a fixed bracket (7) is sleeved at the middle position of the water injection pipe (6), the other end of the fixed bracket (7) is welded at the middle position of the right side of the distillation retort (9), an observation device (5) is arranged at the left side position of the bottom of the water injection pipe (6), the distillation retort support (4) is welded at the bottom of the distillation retort (9).

2. A distillation apparatus according to claim 1, wherein: the cooling pipe (1) comprises a transmission pipe (11), a liquid injection port (12), a cooling box (13), a storage tank interface (14), a liquid discharge port (15) and a distillation tank interface (16), the distillation tank interface (16) is arranged at the bottom of the left side of the transmission pipe (11), the storage tank interface (14) is arranged at the bottom of the right side of the transmission pipe (11), the cooling box (13) is arranged at the middle position of the transmission pipe (11), the liquid injection port (12) is arranged at the left side of the top of the cooling box (13), and the liquid discharge port (15) is arranged at the left side of the bottom of the cooling box (13).

3. A distillation apparatus according to claim 1, wherein: viewing device (5) are including mounting groove (51), top mount (52), observation pipe (53), bottom mount (54), mounting bracket (55) and communicating pipe (56), the intermediate position department of mounting bracket (55) is provided with mounting groove (51), the left side position department of mounting bracket (55) is provided with communicating pipe (56), the right side top position department of mounting bracket (55) is provided with top mount (52), and the right side bottom position department of mounting bracket (55) is provided with bottom mount (54), right side position department between top mount (52) and bottom mount (54) is provided with observation pipe (53).

4. A distillation apparatus according to claim 1, wherein: retort (9) are including charge door (91), heating rod (92), the jar body (93), mount (94), heating tank (95) and interlayer board (96), the top left side position department of the jar body (93) is provided with charge door (91), the inside middle position department under the centre of the jar body (93) is provided with interlayer board (96), the top intermediate position department of interlayer board (96) has cup jointed heating rod (92), the below position department of interlayer board (96) is provided with heating tank (95), the inside both sides position department of the jar body (93) is provided with mount (94).

5. A distillation apparatus according to claim 1, wherein: the storage tank (2) is 600cm in height and 480mm in diameter.

6. A distillation apparatus according to claim 1, wherein: the size of the distillation tank (9) is 860mm in height and 670mm in diameter.

7. A distillation apparatus according to claim 3, wherein: the left side positions of the top fixing frame (52) and the bottom fixing frame (54) are provided with communicating pipes (56), one end positions of the communicating pipes (56) are located on the left side of the mounting frame (55), and the other end positions of the communicating pipes (56) are connected with the observation pipe (53).

8. A distillation apparatus according to claim 4, wherein: the fixing frames (94) are provided with three pairs, and the sizes and the shapes of the three pairs of fixing frames (94) are the same.