CN210096956U - Heating and purifying device for chemical raw materials - Google Patents

Heating and purifying device for chemical raw materials Download PDF

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Publication number
CN210096956U
CN210096956U CN201920727704.7U CN201920727704U CN210096956U CN 210096956 U CN210096956 U CN 210096956U CN 201920727704 U CN201920727704 U CN 201920727704U CN 210096956 U CN210096956 U CN 210096956U
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purification
raw materials
pipe
heating
bucket
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CN201920727704.7U
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Chinese (zh)
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王林
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Suzhou Puluoda Biological Science and Technology Co Ltd
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Suzhou Puluoda Biological Science and Technology Co Ltd
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Abstract

The utility model discloses a heating purification device of industrial chemicals, including the purification bucket, the condenser pipe with put the thing net, the upper end threaded connection of purification bucket has sealed lid, and the upper end intermediate position of sealed lid is fixed with the spiral shell dish, the lower fixed surface of sealed lid has the motor, and the lower extreme of motor is connected with well core rod, exhaust pipe is installed in the upper right corner of sealed lid, and exhaust pipe's right-hand member is connected with the air pump, the connecting pipe is installed to the right-hand member of air pump, the condenser pipe is connected in the lower extreme of connecting pipe, and the outside arrangement of condenser pipe has the condensate tank, settle in the lower right corner of condensate tank has the collection box, and the lower extreme of collection box installs the support, put the thing net and settle in. This industrial chemicals's heating purification device sets up solid raw materials and purifies through the filtration mode, and liquid raw materials purifies through the distillation mode, collects solid purification and liquid purification in an organic whole, has strengthened its practicality greatly.

Description

Heating and purifying device for chemical raw materials
Technical Field
The utility model relates to a chemical industry processingequipment technical field specifically is industrial chemicals's heating purification device.
Background
The purification refers to separating impurities from a mixture to improve the purity of the mixture, and the purification is an important chemical method, has important functions in chemical research and chemical production, and is mainly used for purification in many important chemical research and chemical production, and common purification methods include filtration, crystallization, distillation, extraction and chromatography.
The industrial chemicals purification device on the market is difficult to have solid purification and liquid purification concurrently, and the functionality is relatively weak, and the practicality is not strong, and heats inhomogeneous in the use to and be difficult to carry out the problem of retrieving the recycle to the vapour that the purification produced, for this reason, we propose the heating purification device of industrial chemicals.
SUMMERY OF THE UTILITY MODEL
An object of the utility model is to provide a industrial chemicals's heating purification device to the industrial chemicals purification device on the market that proposes in solving above-mentioned background art is difficult to have solid purification and liquid purification concurrently, and functional weak, the practicality is not strong, and heats inhomogeneously in the use, and is difficult to retrieve the problem of recycling to the vapour that the purification produced.
In order to achieve the above object, the utility model provides a following technical scheme: heating purification device of industrial chemicals, including purification bucket, condenser pipe and putting the thing net, the upper end threaded connection of purification bucket has sealed lid, and the upper end intermediate position of sealed lid is fixed with the spiral shell dish, the lower fixed surface of sealed lid has the motor, and the lower extreme of motor is connected with well core rod, the upper right corner of sealed lid is installed and is arranged the steam extraction pipe, and the right-hand member of steam extraction pipe is connected with the air pump, the connecting pipe is installed to the right-hand member of air pump, the condenser pipe is connected in the lower extreme of connecting pipe, and the outside arrangement of condenser pipe has the condensate tank, settle in the lower right corner of condensate tank has the collection box, and the lower extreme of collection box installs the support, put the thing net and settle in the inboard of purification bucket, and the lower extreme of purification.
Preferably, the sealing ring is installed at the junction of the purification barrel and the sealing cover, the structure of the sealing ring is of an annular structure, and the sealing ring is made of silicon rubber.
Preferably, the structure of the purification barrel is a double-layer structure, and the interior of the purification barrel is connected with an electric heating wire.
Preferably, the purification barrel forms a communicating structure with the condensation pipe through the exhaust pipe, the air pump and the connecting pipe, and the condensation pipe penetrates through the inside of the condensation water tank.
Preferably, the slide rail has all been inlayed to the internal surface left and right sides of purification bucket, and the internal connection of slide rail has the slider, the slider with put the connected mode between the thing net for welded connection, and put the thing net and pass through and constitute sliding structure between slider and slide rail and the purification bucket.
Preferably, the lower end of the central rod is welded with a stirring shaft, and the stirring shaft is of a W-shaped structure.
Compared with the prior art, the beneficial effects of the utility model are that:
1. the heating and purifying device for the chemical raw materials is provided with the storage net in a hollow net shape, can receive solid raw materials and purify the solid raw materials in a filtering mode, can also place liquid raw materials in the purifying barrel and purify the liquid raw materials in a distillation mode, and integrates solid purification and liquid purification into a whole, so that the practicability of the device is greatly enhanced, and meanwhile, the storage net can slide up and down relative to the purifying barrel, so that the purified raw materials are conveniently stored and taken out;
2. the sealing ring is made of silicon rubber, so that the sealing effect between the purification barrel and the sealing cover can be enhanced, the air leakage in the purification process is avoided, the temperature in the purification barrel is prevented from being influenced, the purification barrel is divided into two layers, namely an inner barrel made of heat conducting materials and an outer barrel made of heat insulating materials, the heating wire is uniformly wrapped on the outer surface of the inner barrel of the purification barrel, and when the heating wire is used for heating, the temperature in the purification barrel can be uniformly diffused, and meanwhile, the outer part of the purification barrel cannot be overheated;
3. the shape that sets up the (mixing) shaft is the W shape, so that put the industrial chemicals who places on the thing net and stir to purification bucket inside, make industrial chemicals can be heated evenly, reinforcing purification effect, the setting is under the effect of air pump, can collect the inside of condenser pipe with the vapour of the inside evaporation of purification bucket, so that collect steam and carry out the condensation again, convenient recovery is recycled, certain resource has not only been practiced thrift, still avoided during the direct atmosphere of discharging of steam, contaminated air's problem.
Drawings
FIG. 1 is a schematic structural view of the present invention;
FIG. 2 is a schematic view of a partial enlarged structure at A in FIG. 1 according to the present invention;
fig. 3 is a schematic view of the overlooking structure of the joint of the sliding block and the sliding rail of the present invention.
In the figure: 1. a purification barrel; 2. a sealing cover; 3. a spiral disc; 4. an electric motor; 5. a center pole; 6. a steam exhaust pipe; 7. an air pump; 8. a connecting pipe; 9. a condenser tube; 10. a condensed water tank; 11. a recycling bin; 12. A support; 13. a storage net; 14. a discharge pipe; 15. a valve; 16. a seal ring; 17. an electric heating wire; 18. A stirring shaft; 19. a slider; 20. a slide rail.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
Referring to fig. 1-3, the present invention provides a technical solution: the heating and purifying device for the chemical raw materials comprises a purifying barrel 1, a sealing cover 2, a spiral disc 3, a motor 4, a central rod 5, a steam exhaust pipe 6, an air pump 7, a connecting pipe 8, a condensing pipe 9, a condensing water tank 10, a recycling tank 11, a support 12, a storage net 13, a discharge pipe 14, a valve 15, a sealing ring 16, a heating wire 17, a stirring shaft 18, a sliding block 19 and a sliding rail 20, wherein the upper end of the purifying barrel 1 is in threaded connection with the sealing cover 2, the spiral disc 3 is fixed at the middle position of the upper end of the sealing cover 2, the motor 4 is fixed on the lower surface of the sealing cover 2, the lower end of the motor 4 is connected with the central rod 5, the steam exhaust pipe 6 is installed at the upper right corner of the sealing cover 2, the air pump 7 is connected with the right end of the steam exhaust pipe 6, the connecting pipe 8 is installed at the right end of the air, A communicating structure is formed among the air pump 7, the connecting pipe 8 and the condensing pipe 9, the condensing pipe 9 penetrates through the interior of the condensing water tank 10, and the condensing pipe 9 is arranged under the action of the air pump 7, so that vapor evaporated in the purification barrel 1 can be collected in the condensing pipe 9, the vapor can be collected and condensed, the vapor can be recycled, certain resources are saved, and the problem that the vapor is directly discharged into the atmosphere to pollute the air is avoided;
a recycling tank 11 is arranged at the lower right corner of the condensed water tank 10, a support 12 is arranged at the lower end of the recycling tank 11, a storage net 13 is arranged at the inner side of the purifying barrel 1, a discharging pipe 14 is connected at the lower end of the purifying barrel 1, a valve 15 is arranged at the middle position of the discharging pipe 14, a sealing ring 16 is arranged at the joint of the purifying barrel 1 and the sealing cover 2, the sealing ring 16 is of an annular structure, the sealing ring 16 is made of silicon rubber, the sealing ring 16 is arranged and made of silicon rubber, the sealing effect between the purifying barrel 1 and the sealing cover 2 can be enhanced, gas leakage in the purifying process is avoided, the temperature inside the purifying barrel 1 is influenced, the structure of the purifying barrel 1 is of a double-layer structure, the heating wire 17 is connected inside the purifying barrel 1, the purifying barrel 1 is divided into two layers, and the inner barrel is respectively, the heating wire 17 is uniformly wrapped on the outer surface of the inner barrel of the purification barrel 1, so that when the heating wire 17 is used for heating, the temperature in the purification barrel 1 can be uniformly diffused, and meanwhile, the outer part of the purification barrel 1 cannot be overheated;
the lower end of the central rod 5 is welded with a stirring shaft 18, the structure of the stirring shaft 18 is a W-shaped structure, the shape of the stirring shaft 18 is W-shaped, so that chemical raw materials placed on a material placing net 13 in the purifying barrel 1 can be stirred, the chemical raw materials can be heated uniformly, the purifying effect is enhanced, sliding rails 20 are embedded on the left side and the right side of the inner surface of the purifying barrel 1, sliding blocks 19 are connected inside the sliding rails 20, the sliding blocks 19 are connected with the material placing net 13 in a welding mode, the material placing net 13 forms a sliding structure with the purifying barrel 1 through the sliding blocks 19 and the sliding rails 20, the material placing net 13 is in a hollow net shape, solid raw materials can be received and purified through a filtering mode, liquid raw materials can be placed in the purifying barrel 1 and purified through a distillation mode, the whole device integrates solid purification and liquid purification, and greatly enhances the practicability, meanwhile, the storage net 13 can slide up and down relative to the purification barrel 1, so that the purified raw materials can be conveniently stored and taken out.
The working principle is as follows: for the heating purification device of the chemical raw materials, firstly, the support 12 supports the whole device, when the solid chemical raw materials need to be purified, the screw disc 3 is rotated firstly, the screw disc 3 drives the sealing cover 2 to rotate, the screw thread action is generated between the sealing cover 2 and the purification barrel 1, so that the sealing cover 2 is opened, the object placing net 13 is pulled upwards, the sliding block 19 slides upwards in the sliding rail 20, then the solid chemical raw materials are placed at the bottom of the object placing net 13, the object placing net 13 is put back to the original position, the sealing cover 2 is covered at the same time, the sealing ring 16 arranged at the joint of the purification barrel 1 and the sealing cover 2 enhances the sealing effect of the whole device, then the motor 4 is started, the heating wire 17 is started simultaneously, the motor 4 works to drive the central rod 5 to rotate, the central rod 5 drives the stirring shaft 18 to stir the solid raw materials, and some fine, the heating wire 17 works to emit heat, so that the temperature in the whole purification barrel 1 rises, solid raw materials are heated, impurities are heated and melted, the impurities drip from the upper part to the lower part of the storage net 13 and are separated from the raw materials, the purification effect is achieved, after the purification operation is finished, the sealing cover 2 can be opened, the purified raw materials are taken out from the upper part of the purification barrel 1, the valve 15 is opened, and the impurities can flow out of the discharge pipe 14;
when liquid chemical raw materials need to be purified, firstly, the sealing cover 2 is opened, then the liquid chemical raw materials are added into the purifying barrel 1, the sealing cover 2 is closed, then the motor 4 is started, meanwhile, the heating wire 17 is started, the heating wire 17 works to emit heat, the temperature in the whole purifying barrel 1 is raised, the liquid raw materials are heated, impurities are heated and evaporated to form steam, the motor 4 works to drive the central rod 5 to rotate, the central rod 5 drives the stirring shaft 18 to stir the liquid raw materials, the evaporation of the impurities is accelerated, then the air pump 7 is started, the air pump 7 works to pump the evaporated gas in the purifying barrel 1 into the exhaust pipe 6 and convey the gas into the condensing pipe 9 through the connecting pipe 8, and the gas is conveyed into the condensing pipe 9 because the condensing pipe 9 is arranged in cold water of the condensing water tank 10, therefore, the steam in the condensing pipe 9 can be condensed into liquid and, therefore, the purpose of purifying the liquid chemical raw materials is achieved, and the using process of the whole chemical raw material heating and purifying device is completed.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims (6)

1. Chemical industry raw materials's heating purification device, including purification bucket (1), condenser pipe (9) and put thing net (13), its characterized in that: the upper end of the purification barrel (1) is in threaded connection with a sealing cover (2), a spiral disc (3) is fixed at the upper end middle position of the sealing cover (2), a motor (4) is fixed on the lower surface of the sealing cover (2), a center rod (5) is connected with the lower end of the motor (4), a steam exhaust pipe (6) is installed at the upper right corner of the sealing cover (2), an air pump (7) is connected with the right end of the steam exhaust pipe (6), a connecting pipe (8) is installed at the right end of the air pump (7), a condensing pipe (9) is connected to the lower end of the connecting pipe (8), a condensing water tank (10) is arranged outside the condensing pipe (9), a recovery box (11) is arranged at the lower right corner of the condensing water tank (10), a support (12) is installed at the lower end of the recovery box (11), a storage net (13) is arranged on the inner side of the purification barrel (1), and a valve (15) is arranged in the middle of the discharge pipe (14).
2. The heating purification device of chemical raw materials according to claim 1, characterized in that: purification bucket (1) and sealed junction of covering (2) install sealing washer (16), and the structure of sealing washer (16) is the loop configuration to the material of sealing washer (16) is the silicon rubber material.
3. The heating purification device of chemical raw materials according to claim 1, characterized in that: the structure of purification bucket (1) is bilayer structure, and the internal connection of purification bucket (1) has heating wire (17).
4. The heating purification device of chemical raw materials according to claim 1, characterized in that: purification bucket (1) constitutes the intercommunication structure through between exhaust pipe (6), air pump (7) and connecting pipe (8) and condenser pipe (9), and condenser pipe (9) run through in the inside of condensate tank (10).
5. The heating purification device of chemical raw materials according to claim 1, characterized in that: slide rail (20) are all inlayed to the internal surface left and right sides of purification bucket (1), and the internal connection of slide rail (20) has slider (19), slider (19) and the connected mode of putting between thing net (13) are welded connection, and put and constitute sliding structure between thing net (13) and purification bucket (1) through slider (19) and slide rail (20).
6. The heating purification device of chemical raw materials according to claim 1, characterized in that: the lower end of the central rod (5) is welded with a stirring shaft (18), and the structure of the stirring shaft (18) is a W-shaped structure.
CN201920727704.7U 2019-05-20 2019-05-20 Heating and purifying device for chemical raw materials Active CN210096956U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201920727704.7U CN210096956U (en) 2019-05-20 2019-05-20 Heating and purifying device for chemical raw materials

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201920727704.7U CN210096956U (en) 2019-05-20 2019-05-20 Heating and purifying device for chemical raw materials

Publications (1)

Publication Number Publication Date
CN210096956U true CN210096956U (en) 2020-02-21

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114558367A (en) * 2022-03-07 2022-05-31 湖北进创博生物科技有限公司 High-efficient filter equipment is used in preparation of 2-chlorine nicotinic acid

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114558367A (en) * 2022-03-07 2022-05-31 湖北进创博生物科技有限公司 High-efficient filter equipment is used in preparation of 2-chlorine nicotinic acid

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