CN210057428U - Self-circulation acid purification device - Google Patents
Self-circulation acid purification device Download PDFInfo
- Publication number
- CN210057428U CN210057428U CN201920509088.8U CN201920509088U CN210057428U CN 210057428 U CN210057428 U CN 210057428U CN 201920509088 U CN201920509088 U CN 201920509088U CN 210057428 U CN210057428 U CN 210057428U
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- CN
- China
- Prior art keywords
- panel
- evaporation tank
- casing
- self
- acid purification
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 239000002253 acid Substances 0.000 title claims abstract description 42
- 238000000746 purification Methods 0.000 title claims abstract description 31
- 238000001704 evaporation Methods 0.000 claims abstract description 42
- 230000008020 evaporation Effects 0.000 claims abstract description 25
- 238000010438 heat treatment Methods 0.000 claims abstract description 11
- 239000007788 liquid Substances 0.000 claims abstract description 11
- 230000008878 coupling Effects 0.000 claims description 4
- 238000010168 coupling process Methods 0.000 claims description 4
- 238000005859 coupling reaction Methods 0.000 claims description 4
- 238000007789 sealing Methods 0.000 claims description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- 230000009286 beneficial effect Effects 0.000 abstract 1
- 238000004821 distillation Methods 0.000 description 5
- 239000007789 gas Substances 0.000 description 5
- 150000007513 acids Chemical class 0.000 description 4
- 238000009835 boiling Methods 0.000 description 4
- 239000003153 chemical reaction reagent Substances 0.000 description 4
- 239000012535 impurity Substances 0.000 description 4
- 239000002184 metal Substances 0.000 description 4
- 101100298222 Caenorhabditis elegans pot-1 gene Proteins 0.000 description 2
- -1 HNO3 Chemical class 0.000 description 2
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 2
- 239000004809 Teflon Substances 0.000 description 2
- 229920006362 Teflon® Polymers 0.000 description 2
- 238000005260 corrosion Methods 0.000 description 2
- 230000007797 corrosion Effects 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 229910017604 nitric acid Inorganic materials 0.000 description 2
- 239000004033 plastic Substances 0.000 description 2
- 229920003023 plastic Polymers 0.000 description 2
- 230000005855 radiation Effects 0.000 description 2
- 238000001179 sorption measurement Methods 0.000 description 2
- 239000012498 ultrapure water Substances 0.000 description 2
- TVEXGJYMHHTVKP-UHFFFAOYSA-N 6-oxabicyclo[3.2.1]oct-3-en-7-one Chemical compound C1C2C(=O)OC1C=CC2 TVEXGJYMHHTVKP-UHFFFAOYSA-N 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 239000003517 fume Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 238000009423 ventilation Methods 0.000 description 1
Images
Landscapes
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The utility model discloses a self-circulation acid purification device, which comprises an evaporation tank, a heating sleeve, a funnel, a collection bottle and a frame body, wherein the evaporation tank is arranged on the frame body, the bottom end of the evaporation tank is provided with the heating sleeve, the top end of the evaporation tank is provided with the funnel, the funnel is communicated with the inside of the evaporation tank, the bottom end of the evaporation tank is provided with a liquid discharge pipe, and the evaporation tank is connected with the collection bottle through a pipeline; the frame body sets up in the casing, casing one side sets up the opening, and the slide rail is installed to this open-ended upper and lower both sides, be provided with the panel on the casing, this panel with slide rail sliding fit, the top of casing is provided with the fan that is arranged in taking out the casing gas. The beneficial effects of the utility model are that the switchable is ventilated or inclosed casing to can realize the safe purification of self-loopa acid purification device.
Description
Technical Field
The utility model particularly relates to a self-loopa sour purification device.
Background
An acid purification device: also called acid distiller, high purity acid extraction system, acid purification device, sub-boiling distiller, high purity acid distillation purifier. In routine laboratory analysis, various acids and reagents are widely used in routine sample processing and analysis. The acid purification device utilizes the heat radiation principle, keeps the liquid temperature lower than the boiling point temperature for evaporation, and then condenses the acid vapor to prepare high-purity water and high-purity reagent, and is widely applied to sample treatment and analysis. The high-purity acid distillation system adopts Teflon corrosion-resistant non-adsorption plastics as containers, and can treat common laboratory acids such as HNO3, HCL, HF and the like. Experiments prove that after the acid with the metal impurity content of about 10ppb is distilled once, the metal impurity content can be reduced to about less than 0.01 ppb. The prior acid purification device needs to be safely carried out in a fume hood or other ventilated environments, so that the prior acid purification device is troublesome.
SUMMERY OF THE UTILITY MODEL
To the above insufficiency, the utility model aims to provide a self-circulation acid purification device, the switchable ventilation or inclosed casing to can realize self-circulation acid purification device's safe purification.
The utility model aims at realizing the purpose through the technical scheme, which comprises an evaporating pot, a heating sleeve, a funnel, a collecting bottle and a frame body, wherein the evaporating pot is arranged on the frame body, the bottom end of the evaporating pot is provided with the heating sleeve, the top end of the evaporating pot is provided with the funnel, the funnel is communicated with the inside of the evaporating pot, the bottom end of the evaporating pot is provided with a liquid discharge pipe, and the evaporating pot is connected with the collecting bottle through a pipeline;
the frame body sets up in the casing, casing one side sets up the opening, and the slide rail is installed to this open-ended upper and lower both sides, be provided with the panel on the casing, this panel with slide rail sliding fit, the top of casing is provided with the fan that is arranged in taking out the casing gas.
As a further aspect of the present invention, the two sides of the panel are provided with sealing rubber strips, and the panel is provided with handles.
As a further proposal of the utility model, the height of the opening is larger than that of the frame body.
As a further aspect of the present invention, a work indicator is further installed on the housing.
As a further aspect of the present invention, the frame body comprises a round bar, a first panel and a second panel, the end faces of the first panel and the second panel are opposite, the round bar sequentially penetrates through the corners of the first panel and the second panel, and the top fixed connection first panel of the evaporation tank is the bottom fixed connection second panel of the evaporation tank.
As a further aspect of the present invention, the casing is worn to establish by the fluid-discharge tube, be provided with the water valve on the fluid-discharge tube.
Due to the adoption of the technical scheme, the utility model discloses following advantage has: the evaporating pot is mounted on the frame body, a heating sleeve is arranged at the bottom end of the evaporating pot, a funnel is arranged at the top end of the evaporating pot, the funnel is communicated with the inside of the evaporating pot, a liquid discharge pipe is arranged at the bottom end of the evaporating pot, and the evaporating pot is connected with the collecting bottle through a pipeline; the frame body sets up in the casing, casing one side sets up the opening, and the slide rail is installed to this open-ended upper and lower both sides, be provided with the panel on the casing, this panel with slide rail sliding fit, the top of casing is provided with the fan that is arranged in taking out the casing gas. Can be switched to a ventilated or closed shell, thereby realizing the safe purification of the self-circulation acid purification device.
Additional advantages, objects, and features of the invention will be set forth in part in the description which follows and in part will become apparent to those having ordinary skill in the art upon examination of the following or may be learned from practice of the invention.
Drawings
The drawings of the present invention are described below.
Fig. 1 is a schematic view of a first three-dimensional structure of a self-circulation acid purification device.
Fig. 2 is a second perspective view of the self-circulating acid purification apparatus.
FIG. 3 is a schematic diagram of a panel removal configuration from a circulating acid purification apparatus.
Detailed Description
The present invention will be further explained with reference to the drawings and examples.
As shown in fig. 1 to 3, the utility model discloses a self-circulation acid purification device, which comprises an evaporation tank 1, a heating jacket 2, a funnel 3, a collection bottle 4 and a frame body, wherein the evaporation tank 1 is installed on the frame body, the heating jacket 2 is arranged at the bottom end of the evaporation tank 1, the funnel 3 is arranged at the top end of the evaporation tank 1, the funnel 3 is communicated with the inside of the evaporation tank 1, a liquid discharge pipe 5 is arranged at the bottom end of the evaporation tank 1, and the evaporation tank 1 is connected with the collection bottle 4 through a pipeline;
the support body sets up in casing 7, casing 7 one side sets up the opening, and slide rail 6 is installed to the upper and lower both sides of this open-ended, be provided with panel 8 on the casing 7, this panel 8 with slide rail 6 sliding fit, the top of casing 7 is provided with the fan 9 that is arranged in taking casing 7 gas out.
Sealing rubber strips 10 are arranged on two sides of the panel 8, and a handle 14 is arranged on the panel 8. The panel 8 is convenient to push and pull, the shell 7 is convenient to close and open, and the height of the opening is larger than that of the frame body. The frame body is convenient to take out or put in, a work indicating lamp is further installed on the shell 7, and the indicating lamp and the heating jacket 2 work simultaneously. When the panel 8 is closed, it is known that the heating jacket 2 is operating.
The support body is including round bar 11, first panel 12 and second panel 13, first panel 12 and 13 terminal surfaces of second panel are relative, the turning of first panel 12 and second panel 13 is worn to establish in proper order by round bar 11, the first panel 12 of top rigid coupling of evaporating pot 1 is the bottom rigid coupling second panel 13 of evaporating pot 1.
The liquid discharge pipe 5 penetrates through the shell 7, and a water valve is arranged on the liquid discharge pipe 5.
The use method and the working principle thereof are as follows: an acid purification device: also called acid distiller, high purity acid extraction system, acid purification device, sub-boiling distiller, high purity acid distillation purifier. In routine laboratory analysis, various acids and reagents are widely used in routine sample processing and analysis. The acid purification device utilizes the heat radiation principle, keeps the liquid temperature lower than the boiling point temperature for evaporation, and then condenses the acid vapor to prepare high-purity water and high-purity reagent, and is widely applied to sample treatment and analysis. The high-purity acid distillation system adopts Teflon corrosion-resistant non-adsorption plastics as containers, and can treat common laboratory acids such as HNO3, HCL, HF and the like. Experiments have shown that after one distillation of an acid having a metal impurity content of about 10ppb, the metal impurity content can be reduced to <0.01 ppb. Place in casing 7, the acid of purification under airtight environment does not receive environmental pollution, ensures sour purity, also can ensure the security of purification simultaneously, sets up that fan 9 can in time get rid of because of pipeline reveals or gaseous unexpected gas in casing 7, the utility model discloses well fan 9 is given vent to anger the back and is connected with the exhaust pipe, carries out corresponding tail gas treatment back, discharges again to the atmosphere in, avoids causing the influence to the environment.
Finally, the above embodiments are only used for illustrating the technical solutions of the present invention and not for limiting, and although the present invention has been described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that modifications or equivalent substitutions may be made to the technical solutions of the present invention without departing from the spirit and scope of the present invention.
Claims (6)
1. A self-circulation acid purification device is characterized by comprising an evaporation tank, a heating sleeve, a funnel, a collection bottle and a frame body, wherein the evaporation tank is mounted on the frame body, the heating sleeve is arranged at the bottom end of the evaporation tank, the funnel is arranged at the top end of the evaporation tank, the funnel is communicated with the inside of the evaporation tank, a liquid discharge pipe is arranged at the bottom end of the evaporation tank, and the evaporation tank is connected with the collection bottle through a pipeline;
the frame body sets up in the casing, casing one side sets up the opening, and the slide rail is installed to this open-ended upper and lower both sides, be provided with the panel on the casing, this panel with slide rail sliding fit, the top of casing is provided with the fan that is arranged in taking out the casing gas.
2. The self-circulating acid purification apparatus of claim 1, wherein: sealing rubber strips are arranged on two sides of the panel, and a handle is arranged on the panel.
3. The self-circulating acid purification apparatus of claim 1, wherein: the height of the opening is greater than that of the shelf body.
4. The self-circulating acid purification apparatus of claim 1, wherein: and the shell is also provided with a working indicator lamp.
5. The self-circulating acid purification apparatus of claim 1, wherein: the support body is including the round bar, first panel and second panel terminal surface are relative, the turning of first panel and second panel is worn to establish in proper order by the round bar, the first panel of top rigid coupling of evaporating pot is the bottom rigid coupling second panel of evaporating pot.
6. The self-circulating acid purification apparatus of claim 1, wherein: the liquid discharge pipe penetrates through the shell, and a water valve is arranged on the liquid discharge pipe.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201920509088.8U CN210057428U (en) | 2019-04-16 | 2019-04-16 | Self-circulation acid purification device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201920509088.8U CN210057428U (en) | 2019-04-16 | 2019-04-16 | Self-circulation acid purification device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN210057428U true CN210057428U (en) | 2020-02-14 |
Family
ID=69436874
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201920509088.8U Active CN210057428U (en) | 2019-04-16 | 2019-04-16 | Self-circulation acid purification device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN210057428U (en) |
-
2019
- 2019-04-16 CN CN201920509088.8U patent/CN210057428U/en active Active
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20240426 Address after: Building 2, 1st Floor, and Building 3, No. 188 Jinou Road, Jinshanwei Town, Jinshan District, Shanghai, December 2015 Patentee after: Shanghai saifute semiconductor materials Co.,Ltd. Country or region after: China Address before: 215300 room 3, 399 Dechang Road, Shipai town, Kunshan City, Suzhou City, Jiangsu Province Patentee before: JIANGSU SAIFUTE SEMICONDUCTOR MATERIAL DETECTION TECHNOLOGY Co.,Ltd. Country or region before: China |
|
| TR01 | Transfer of patent right |