CN209940482U - High-efficient purification equipment of kaolin - Google Patents
High-efficient purification equipment of kaolin Download PDFInfo
- Publication number
- CN209940482U CN209940482U CN201920464283.3U CN201920464283U CN209940482U CN 209940482 U CN209940482 U CN 209940482U CN 201920464283 U CN201920464283 U CN 201920464283U CN 209940482 U CN209940482 U CN 209940482U
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- China
- Prior art keywords
- stirring tank
- kaolin
- stirring
- purification equipment
- plastic filter
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- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 title claims abstract description 34
- 239000005995 Aluminium silicate Substances 0.000 title claims abstract description 24
- 235000012211 aluminium silicate Nutrition 0.000 title claims abstract description 24
- 238000000746 purification Methods 0.000 title claims abstract description 18
- 238000003756 stirring Methods 0.000 claims abstract description 78
- 239000004033 plastic Substances 0.000 claims abstract description 38
- 239000003638 chemical reducing agent Substances 0.000 claims abstract description 11
- 239000011521 glass Substances 0.000 claims abstract description 11
- 238000007790 scraping Methods 0.000 claims abstract description 8
- 239000007788 liquid Substances 0.000 claims description 8
- 238000007789 sealing Methods 0.000 claims description 5
- 239000004568 cement Substances 0.000 claims description 3
- 239000000463 material Substances 0.000 claims description 3
- 239000000853 adhesive Substances 0.000 claims 2
- 230000001070 adhesive effect Effects 0.000 claims 2
- SZVJSHCCFOBDDC-UHFFFAOYSA-N ferrosoferric oxide Chemical compound O=[Fe]O[Fe]O[Fe]=O SZVJSHCCFOBDDC-UHFFFAOYSA-N 0.000 abstract description 24
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 abstract description 19
- 239000002253 acid Substances 0.000 abstract description 17
- 239000002245 particle Substances 0.000 abstract description 15
- 229910052622 kaolinite Inorganic materials 0.000 abstract description 10
- 229910052742 iron Inorganic materials 0.000 abstract description 9
- 238000003825 pressing Methods 0.000 abstract description 7
- 238000000034 method Methods 0.000 abstract description 6
- 230000000694 effects Effects 0.000 abstract description 3
- 239000002002 slurry Substances 0.000 description 10
- 239000004576 sand Substances 0.000 description 6
- 238000005406 washing Methods 0.000 description 6
- 230000007797 corrosion Effects 0.000 description 3
- 238000005260 corrosion Methods 0.000 description 3
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N iron oxide Inorganic materials [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 3
- 238000000926 separation method Methods 0.000 description 3
- 238000004026 adhesive bonding Methods 0.000 description 2
- 238000004061 bleaching Methods 0.000 description 2
- 239000004927 clay Substances 0.000 description 2
- 239000002270 dispersing agent Substances 0.000 description 2
- 239000003292 glue Substances 0.000 description 2
- 230000005484 gravity Effects 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 235000013980 iron oxide Nutrition 0.000 description 2
- 239000002689 soil Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000004677 Nylon Substances 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 238000003889 chemical engineering Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000003780 insertion Methods 0.000 description 1
- 230000037431 insertion Effects 0.000 description 1
- VBMVTYDPPZVILR-UHFFFAOYSA-N iron(2+);oxygen(2-) Chemical class [O-2].[Fe+2] VBMVTYDPPZVILR-UHFFFAOYSA-N 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229920001778 nylon Polymers 0.000 description 1
- 238000004537 pulping Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- JVBXVOWTABLYPX-UHFFFAOYSA-L sodium dithionite Chemical compound [Na+].[Na+].[O-]S(=O)S([O-])=O JVBXVOWTABLYPX-UHFFFAOYSA-L 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 1
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Abstract
The utility model relates to the technical field of kaolin processing, in particular to high-efficiency kaolin purification equipment; the stirring tank is characterized in that a glass layer is arranged on the inner wall of the stirring tank, a feeding device is arranged on the left side of the top of the stirring tank, a bearing is arranged at the bottom of the stirring tank, a stirring shaft is inserted into the bearing, four plastic filter plates matched with the inner diameter of the stirring tank are arranged on the inner wall of the stirring tank in parallel, the stirring shaft penetrates through all the plastic filter plates, extends out of the stirring tank and is connected with a rotating shaft of a speed reducer, four scraping plates are arranged on the periphery of the stirring shaft, and a discharge pipe is communicated with the lower part of the; the method comprises the steps of firstly absorbing a part of ferroferric oxide by a magnet rod of a feeding device, then continuously pressing small ferroferric oxide particles by a plastic scraper and a plastic filter plate, and stripping off kaolinite on the surfaces of the ferroferric oxide particles, so that the ferroferric oxide can be conveniently dissolved by an acid solution, and the effect of reducing the content of iron elements is achieved.
Description
Technical Field
The utility model belongs to the technical field of the kaolin processing technique and specifically relates to a high-efficient purification equipment of kaolin.
Background
The known process for preparing the catalyst from kaolin comprises the steps of separating clay and impurities, mixing the clay and the impurities with a dispersant, pulping, desanding, stirring, bleaching (concentrated sulfuric acid and sodium hydrosulfite), washing, filter pressing and dehydrating, and obtaining the finished product. The finished product must not exceed a certain value for the iron element.
The iron removal process in the prior art mainly focuses on two procedures of sand removal and washing. The sand removal is to add a dispersing agent into the ore pulp to separate soil and sand in the kaolin ore more quickly and efficiently, and the sand (including iron sand) is removed under the action of gravity to obtain the kaolin ore pulp; in bleaching, the acid solution dissolves iron or iron oxides. However, in a part of ferroferric oxide enriched area, there is a case that the collected kaolin is purified: because the kaolinite in the kaolin has plasticity, wet soil can be molded into various shapes without being broken, and can be kept unchanged for a long time, the periphery of a small amount of ferroferric oxide particles is wrapped by the kaolinite, the ferroferric oxide particles can not fall off under the action of gravity due to the magnetic adsorption of the ferroferric oxide particles on the side wall of equipment (stainless steel) during sand removal, and enter washing equipment along with slurry, because the kaolinite at the periphery of the ferroferric oxide particles can not be completely removed by the existing washing equipment, and the part of ferroferric oxide can not be dissolved by an acid solution during washing.
Disclosure of Invention
Aiming at the defects of the prior art, the utility model provides a kaolin purification device which can remove iron oxide more easily.
The technical scheme of the utility model is that:
the utility model provides a high-efficient purification equipment of kaolin, it includes the agitator tank, its characterized in that: the inner wall of the stirring tank is provided with a glass layer (namely a glass lining stirring tank) for preventing the acid solution from corroding the stirring tank, the top of the stirring tank is provided with a speed reducer through a bracket, the top of the speed reducer is provided with a motor, the left side of the top of the stirring tank is provided with a feeding device, the right side of the top of the stirring tank is provided with a liquid inlet pipe, the bottom of the stirring tank is provided with a bearing, the bearing is inserted with a stirring shaft, the inner wall of the stirring tank is provided with four plastic filter plates which are matched with the inner diameter of the stirring tank in parallel, the center of each plastic filter plate is provided with a through hole corresponding to the stirring shaft, the stirring shaft penetrates through all the plastic filter plates and extends out of the stirring tank and is connected with a rotating shaft of the speed reducer, four scraping plates are arranged on the periphery of the stirring shaft and are respectively positioned above the four plastic filter plates, and the distance between each scraping plate and the corresponding plastic filter plate is less than or equal to three millimeters. Because the distance between the scraper and the plastic filter plate is small, the ferroferric oxide particles continuously lose kaolinite on the surface in the process of continuous pressing, the acid solution entering the liquid inlet pipe reacts with the ferroferric oxide to generate soluble substances, and the kaolinite is very fine, does not obstruct the rotation of the scraper and is not dissolved in the acid solution, so the separation and the purification are realized; the lower part of the stirring tank is communicated with a discharge pipe for connecting a belt filter press.
Specifically, the sealing ring is sleeved between the stirring tank and the stirring shaft, so that the sealing performance is improved.
Specifically, feed arrangement includes conical tube, handle, top cap and magnet stick, big-end-up and small and upper portion lateral wall are provided with a circular through-hole on the conical tube, and an inlet pipe is inserted to the through-hole, a magnet stick of vertical insertion in the conical tube, magnet stick top has a top cap through powerful adhesive bonding, the top cap top has a handle through powerful adhesive bonding, the gripping of being convenient for. Slurry enters the conical pipe from the feeding pipe, if a small amount of ferroferric oxide particles exist in the slurry, the slurry is easily adsorbed on the magnet rod, the magnet rod is lifted out and wiped by the handle regularly, and the ferroferric oxide particles on the surface can be removed, so that the iron removing efficiency is further improved.
Specifically, the lower end of a conical pipe of the feeding device is communicated with the stirring tank, and the periphery of the lower part of the conical pipe is bonded with the top of the stirring tank through glass cement.
Specifically, the stirring shaft and the scraper are made of plastic materials. Preventing corrosion of the acid solution.
Specifically, the bearing is a plastic bearing, and is prevented from being corroded by acid solution.
Specifically, the plastic filter plate is circular, the scraper is semicircular, the diameters of the plastic filter plate and the scraper are equal, and the pressing area is increased.
Specifically, the plastic filter plate is uniformly provided with through holes, the density of the through holes is four per square centimeter, and the aperture of each through hole is one millimeter.
Specifically, a foot pad is arranged at the bottom of the stirring tank.
The utility model has the advantages that: the method comprises the steps of firstly absorbing a part of ferroferric oxide by a magnet rod of a feeding device, then continuously pressing small ferroferric oxide particles by a plastic scraper and a plastic filter plate, and stripping off kaolinite on the surfaces of the ferroferric oxide particles, so that the ferroferric oxide can be conveniently dissolved by an acid solution, and the effect of reducing the content of iron elements is achieved.
Drawings
Fig. 1 is a schematic structural view of the present invention;
FIG. 2 is a schematic structural view of the feeding device of the present invention;
FIG. 3 is a schematic view of the feeder apparatus with the tapered tube removed (i.e., a schematic view of the extractable part);
FIG. 4 is a top view of the scraper of the present invention;
fig. 5 is a top view of the plastic filter plate of the present invention.
In the figure, 1, a stirring tank; 2. a support; 3. a speed reducer; 4. a motor; 5. a feeding device; 6. a feed pipe; 7. a liquid inlet pipe; 8. a stirring shaft; 9. a discharge pipe; 11. a glass layer; 12. a bearing; 13. a foot pad; 14. a plastic filter plate; 51. a tapered tube; 52. a handle; 53. a magnet bar; 54. a top cover; 81. a scraper.
Detailed Description
The following description of the embodiments of the present invention will be made with reference to the accompanying drawings:
as shown in fig. 1 and 2, a kaolin efficient purification device comprises a stirring tank 1, wherein a glass layer 11 (the stirring tank of glass lining is adopted in this embodiment, specifically, the stirring tank of glass lining provided by Jiangsu Yang chemical engineering equipment manufacturing Co., Ltd.) is arranged on the inner wall of the stirring tank 1, the stirring tank 1 is prevented from being corroded by an acid solution, a speed reducer 3 is installed on the top of the stirring tank 1 through a bracket 2, a motor 4 is installed on the top of the speed reducer 3, a feeding device 5 is arranged on the left side of the top of the stirring tank 1, a liquid inlet pipe 7 is arranged on the right side of the top of the stirring tank 1, a bearing 12 is arranged at the bottom of the stirring tank 1, a stirring shaft 8 is inserted into the bearing 12, four plastic filter plates 14 matched with the inner diameter of the stirring tank 1 are arranged on the inner wall of the stirring tank, the stirring shaft 8 penetrates through all the plastic filter plates 14 and extends out of the stirring tank 1 and is connected with a rotating shaft of the speed reducer 3, four scraping plates 81 are arranged on the periphery of the stirring shaft 8, the four scraping plates 81 are respectively positioned above the four plastic filter plates 14, and the distance between each scraping plate 81 and the corresponding plastic filter plate 14 is less than or equal to three millimeters. Because the distance between the scraper 81 and the plastic filter plate 14 is small, the kaolinite on the surface is continuously lost by ferroferric oxide particles in continuous pressing, the acid solution entering the liquid inlet pipe 7 reacts with the ferroferric oxide to generate soluble substances, and the kaolinite is very fine and smooth, does not obstruct the rotation of the scraper 81 and is not dissolved in the acid solution, so the separation and the purification are realized; the lower part of the stirring tank 1 is communicated with a discharge pipe 9 for connecting a belt filter press.
A sealing ring is sleeved between the stirring tank 1 and the stirring shaft 8, so that the sealing performance is improved.
The feeding device 5 comprises a conical tube 51, a handle 52, a top cover 54 and a magnet rod 53, wherein the conical tube 51 is large in size and small in size, a circular through hole is formed in the side wall of the upper portion of the conical tube 51, a feeding tube 6 is inserted into the through hole, the magnet rod 53 is vertically inserted into the conical tube 51, the top cover 54 is adhered to the top of the magnet rod 53 through strong glue, and the handle 52 is adhered to the top of the top cover 54 through the strong glue to facilitate grasping. Slurry enters the conical pipe 51 from the feeding pipe 6, if a small amount of ferroferric oxide particles exist in the slurry, the slurry is easily adsorbed on the magnetic iron rod 53, the magnetic iron rod 53 is lifted out and wiped by the handle 52 regularly, and the ferroferric oxide particles on the surface can be removed, so that the iron removing efficiency is further improved.
The lower end of a conical pipe 51 of the feeding device 5 is communicated with the stirring tank 1, and the periphery of the lower part of the conical pipe 51 is bonded with the top of the stirring tank 1 through glass cement.
The stirring shaft 8 and the scraper 81 are made of plastic materials. Preventing corrosion of the acid solution.
The bearing 12 is a plastic bearing to prevent corrosion by acid solution.
The plastic filter plate 14 is circular, the scraper 81 is semicircular, the diameters of the two are equal, and the pressing area is increased.
The plastic filter plate 14 is uniformly provided with through holes, the density of the through holes is four per square centimeter, and the aperture of each through hole is one millimeter.
And a foot pad 13 is arranged at the bottom of the stirring tank 1.
The plastic filter plate, the scraper and the stirring shaft in the embodiment are all made of nylon 1010 as raw materials, and have super-strong wear resistance.
The workflow of this embodiment:
1) injecting the desanded slurry into a feeding device from a feeding pipe;
2) the slurry enters a stirring tank after being adsorbed by the magnet rod;
3) meanwhile, acid solution (ph 4.5) is poured in through the liquid inlet pipe;
4) starting a motor for stirring;
5) the scraping plate and the plastic filter plate continuously strip kaolinite on the surfaces of ferroferric oxide particles, and the ferroferric oxide is dissolved by an acid solution;
6) and (3) injecting the slurry after the acid washing into a belt filter press from a discharge pipe (other filter presses have similar effects) to realize solid-liquid separation, wherein filter residues are relatively pure kaolin.
The foregoing embodiments and description have been provided to illustrate the principles and preferred embodiments of the present invention, and various changes and modifications may be made without departing from the spirit and scope of the invention, which fall within the scope of the invention as claimed.
Claims (9)
1. The utility model provides a high-efficient purification equipment of kaolin, it includes the agitator tank, its characterized in that: the stirring tank is characterized in that a glass layer is arranged on the inner wall of the stirring tank, a speed reducer is mounted at the top of the stirring tank through a support, a motor is mounted at the top of the speed reducer, a feeding device is arranged on the left side of the top of the stirring tank, a liquid inlet pipe is arranged on the right side of the top of the stirring tank, a bearing is arranged at the bottom of the stirring tank, a stirring shaft is inserted into the bearing, four plastic filter plates matched with the inner diameter of the stirring tank are arranged on the inner wall of the stirring tank in parallel, a through hole is formed in the center of each plastic filter plate and corresponds to the stirring shaft, the stirring shaft penetrates through all the plastic filter plates, extends out of the stirring tank and is connected with a rotating shaft of the speed reducer, four scraping plates; the lower part of the stirring tank is communicated with a discharge pipe.
2. The efficient kaolin purification equipment as set forth in claim 1, wherein: and a sealing ring is sleeved between the stirring tank and the stirring shaft.
3. The efficient kaolin purification equipment as set forth in claim 2, wherein: the feeding device comprises a conical tube, a handle, a top cover and a magnet rod, wherein a circular through hole is formed in the upper side wall, the lower side wall and the upper side wall of the conical tube are large and small, an inlet pipe is inserted into the through hole, the magnet rod is vertically inserted into the conical tube, the top cover is adhered to the top of the magnet rod through a strong adhesive, and the handle is adhered to the top of the top cover through the strong adhesive.
4. The efficient purification equipment for kaolin as claimed in claim 3, wherein: the lower end of a conical pipe of the feeding device is communicated with the stirring tank, and the periphery of the lower part of the conical pipe is bonded with the top of the stirring tank through glass cement.
5. The efficient purification equipment for kaolin as claimed in claim 4, wherein: the stirring shaft and the scraper are made of plastic materials.
6. The efficient purification equipment for kaolin as claimed in claim 5, wherein: the bearing is a plastic bearing.
7. The efficient purification equipment for kaolin as claimed in claim 6, wherein: the plastic filter plate is circular, the scraper is semicircular, and the diameters of the plastic filter plate and the scraper are equal.
8. The efficient purification equipment for kaolin as claimed in claim 7, wherein: the plastic filter plate is uniformly provided with through holes, the density of the through holes is four per square centimeter, and the aperture of each through hole is one millimeter.
9. The efficient purification equipment for kaolin as claimed in claim 8, wherein: a foot pad is arranged at the bottom of the stirring tank.
Priority Applications (1)
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CN201920464283.3U CN209940482U (en) | 2019-04-08 | 2019-04-08 | High-efficient purification equipment of kaolin |
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CN201920464283.3U CN209940482U (en) | 2019-04-08 | 2019-04-08 | High-efficient purification equipment of kaolin |
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CN201920464283.3U Active CN209940482U (en) | 2019-04-08 | 2019-04-08 | High-efficient purification equipment of kaolin |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111545345A (en) * | 2020-05-13 | 2020-08-18 | 华鼎国联四川动力电池有限公司 | Honeycomb type slurry iron remover for power battery homogenizing equipment |
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2019
- 2019-04-08 CN CN201920464283.3U patent/CN209940482U/en active Active
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111545345A (en) * | 2020-05-13 | 2020-08-18 | 华鼎国联四川动力电池有限公司 | Honeycomb type slurry iron remover for power battery homogenizing equipment |
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