CN209872382U - High-efficient irritability's aqueous ammonia synthesis equipment of preventing - Google Patents
High-efficient irritability's aqueous ammonia synthesis equipment of preventing Download PDFInfo
- Publication number
- CN209872382U CN209872382U CN201920441923.9U CN201920441923U CN209872382U CN 209872382 U CN209872382 U CN 209872382U CN 201920441923 U CN201920441923 U CN 201920441923U CN 209872382 U CN209872382 U CN 209872382U
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- water absorption
- pipe
- absorption bottle
- purification jar
- ammonia
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Abstract
The utility model discloses a synthetic equipment of irritability's aqueous ammonia is prevented to high efficiency, including the purification jar, the inner chamber top of purification jar is provided with potassium permanganate suspension and sodium hydroxide suspension, the roof is installed through the feed liquor pipe in the top of purification jar, first conveyer pipe is installed to one side of liquid ammonia steel storage tank, the distilled water holding vessel is installed to the inboard of support frame, the connector head is installed to the one end of distilled water holding vessel, the base is installed to the bottom of support frame. The utility model discloses a five liquid ammonia storage steel jars are installed on the top of purification jar, and through first duct connection between liquid ammonia storage steel jar and the purification jar, through its convenient transport, and install the high pure water absorption bottle in the both sides of purification jar, are provided with the cold water groove at the inner wall of high pure water absorption bottle, have the refrigeration coil pipe at the internally mounted in cold water groove, have made things convenient for the washing gas of liquid ammonia greatly through it, and can avoid gas excessive.
Description
Technical Field
The utility model relates to an aqueous ammonia synthesis equipment technical field specifically is a irritability's aqueous ammonia synthesis equipment is prevented to high efficiency.
Background
The ammonia water refers to an aqueous solution of ammonia gas, which has strong pungent smell and weak alkalinity, ammonia gas molecules are weakly hydrolyzed to generate hydroxide ions and ammonium ions in the ammonia water, the name of ammonium hydroxide is not very proper, and the ammonium hydroxide can not be separated from the solution only by describing ions in the ammonia water solution, the ammonia water is dissolved in high-purity water in an absorption bottle after washing gas by using steel bottle liquid ammonia as a raw material through 1% potassium permanganate, 5% sodium hydroxide suspension and two pure water washing bottles, the absorption bottle is cooled by using ice water, the flow rate of the ammonia gas is controlled, the high-purity grade can be achieved by careful operation, and the reagent ammonia water prepared by using purified distilled water is responsible.
The ammonia water synthesis equipment at the present stage has a plurality of defects, for example, the sealing effect is poor, the odor can be prevented from overflowing, the use is inconvenient, and the collection is inconvenient.
SUMMERY OF THE UTILITY MODEL
An object of the utility model is to provide a irritability's aqueous ammonia synthesizer is prevented to the high efficiency to propose in solving above-mentioned background art, sealed effect is poor, can prevent that the peculiar smell is excessive, uses inconveniently, collects inconvenient scheduling problem.
In order to achieve the above object, the utility model provides a following technical scheme: the utility model provides a synthetic equipment of high-efficient irritability-preventing aqueous ammonia, includes the purification jar, the inner chamber top of purification jar is provided with potassium permanganate suspension and sodium hydroxide suspension, the roof is installed through the feed liquor pipe in the top of purification jar, liquid ammonia storage steel tank is installed at the top of roof, first conveyer pipe is installed to one side of liquid ammonia storage steel tank, install first control valve on the first conveyer pipe, high-purity water absorption bottle is installed to one side of purification jar, the inside middle part of high-purity water absorption bottle is provided with pure water storage inner chamber, be provided with the cold water groove between the outer wall of pure water storage inner chamber and high-purity water absorption bottle, the internally mounted of cold water groove has refrigerating coil, the third conveyer pipe is installed to the bottom of high-purity water absorption bottle, install the third control valve on the third conveyer pipe, the second conveyer pipe is installed at the top of high-purity water absorption, install the second control valve on the second conveyer pipe, the support frame is installed to the below both sides of purification jar, the distilled water holding vessel is installed to the inboard of support frame, the connector is installed to the one end of distilled water holding vessel, the base is installed to the bottom of support frame.
Preferably, the top plate is of a hollow structure and is connected with the inner cavity of the purification tank through a liquid inlet pipe.
Preferably, the liquid ammonia storage steel tank is provided with five altogether, and five liquid ammonia storage steel tanks evenly install the top at the roof.
Preferably, the third transfer pipe is installed between the purification tank and the high purity water absorption bottle, and the second transfer pipe is installed between the high purity water absorption bottle and the distilled water storage tank.
Preferably, the high-purity water absorption bottles are provided with two high-purity water absorption bottles which are respectively and symmetrically arranged on the front surface and the back surface of the purification tank.
Preferably, the inner side of the support frame is provided with a clamping groove, and the distilled water storage tank is arranged on the inner side of the support frame in an embedding manner.
Compared with the prior art, the beneficial effects of the utility model are that:
1. the top end of the purification tank of the utility model is provided with five liquid ammonia storage steel tanks, the liquid ammonia storage steel tanks are connected with the purification tank through the first conveying pipe, the liquid ammonia storage steel tanks are convenient to convey through the liquid ammonia storage steel tanks, high-purity water absorption bottles are arranged on two sides of the purification tank, the inner wall of each high-purity water absorption bottle is provided with a cold water tank, and a refrigeration coil pipe is arranged inside the cold water tank, so that the liquid ammonia is greatly convenient to be washed, and the gas can be prevented from overflowing;
2. the utility model discloses an install the distilled water holding vessel between the support frame, and through second duct connection between distilled water holding vessel and the high pure water absorption bottle, made things convenient for the collection of aqueous ammonia through it, and can not appear leaking the problem outward, avoid revealing of irritability smell, improve the security.
Drawings
FIG. 1 is a schematic structural diagram of an efficient anti-irritant ammonia synthesis apparatus of the present invention;
fig. 2 is a top view of the fruit placing plate of the present invention;
figure 3 is a side view of the purification tank of the present invention.
In the figure: 1. a liquid ammonia storage steel tank; 2. a first delivery pipe; 3. a first control valve; 4. a liquid inlet pipe; 5. a top plate; 6. a second delivery pipe; 7. a second control valve; 8. a distilled water storage tank; 9. a base; 10. a purification tank; 11. a high purity water absorption bottle; 12. a third control valve; 13. a third delivery pipe; 14. a support frame; 15. a pipe connector; 16. suspension of potassium permanganate; 17. a sodium hydroxide suspension; 18. a refrigeration coil; 19. a cold water tank; 20. the pure water stores the inner chamber.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments.
Referring to fig. 1-3, the present invention provides an embodiment: the utility model provides a high-efficient irritability's aqueous ammonia synthesis equipment of preventing, including purification jar 10, the inner chamber top of purification jar 10 is provided with potassium permanganate suspension 16 and sodium hydroxide suspension 17, potassium permanganate suspension 16 and sodium hydroxide suspension 17 are used for purifying liquid ammonia and get rid of inside gaseous impurities, roof 5 is installed through feed liquor pipe 4 on the top of purification jar 10, liquid ammonia storage steel tank 1 is installed at the top of roof 5, liquid ammonia storage steel tank 1 is used for storing the liquid ammonia raw materials, first conveyer pipe 2 is installed to one side of liquid ammonia storage steel tank 1, first conveyer pipe 2 is used for carrying the liquid ammonia raw materials to in the purification jar 10, install first control valve 3 on the first conveyer pipe 2, high pure water absorption bottle 11 is installed to one side of purification jar 10, high pure water absorption bottle 11 is used for absorbing the liquid ammonia after the purification, the inside middle part of high pure water absorption bottle 11 is provided with storage inner chamber 20, a cold water tank 19 is arranged between the pure water storage inner cavity 20 and the outer wall of the high-purity water absorption bottle 11, the cold water tank 19 can accelerate cooling and control the flow rate of ammonia gas, a refrigeration coil 18 is arranged inside the cold water tank 19, a third delivery pipe 13 is arranged at the bottom of the high-purity water absorption bottle 11, the third delivery pipe 13 is used for delivering purified liquid ammonia into the high-purity water absorption bottle 11, a third control valve 12 is arranged on the third delivery pipe 13, a second delivery pipe 6 is arranged at the top of the high-purity water absorption bottle 11, the second delivery pipe 6 is used for delivering ammonia gas into a distilled water storage tank 8, a second control valve 7 is arranged on the second delivery pipe 6, support frames 14 are arranged at two sides below the purification tank 10, a distilled water storage tank 8 is arranged at the inner side of each support frame 14, the distilled water storage tank 8 is used for reacting with ammonia gas to prepare ammonia water, a connector 15 is arranged, the bottom end of the supporting frame 14 is provided with a base 9.
Further, roof 5 sets up to hollow structure, and roof 5 is connected with the inner chamber of purification jar 10 through feed liquor pipe 4, is used for storing steel jar 1 support to liquid ammonia through roof 5, and can the memory storage liquid ammonia through feed liquor pipe 4 reposition of redundant personnel to purification jar 10 in.
Further, liquid ammonia storage steel tank 1 is provided with five altogether, and 1 uniform mounting in the top of roof 5 of five liquid ammonia storage steel tanks is used for storing reserve liquid ammonia raw materials through liquid ammonia storage steel tank 1.
Further, a third transport pipe 13 is installed between the purification tank 10 and the high purity water absorption bottle 11, and a second transport pipe 6 is installed between the high purity water absorption bottle 11 and the distilled water storage tank 8, for transporting purified liquid ammonia into the high purity water absorption bottle 11 through the third transport pipe 13, and for transporting ammonia into the distilled water storage tank 8 through the second transport pipe 6.
Further, high-purity water absorption bottle 11 is provided with two altogether, and the symmetry is installed respectively at the front and the back of purification jar 10, is used for absorbing the liquid ammonia after the purification through high-purity water absorption bottle 11, prepares pure ammonia.
Further, the inner side of the support frame 14 is provided with a clamping groove, the distilled water storage tank 8 is installed on the inner side of the support frame 14 in an embedding mode, and the distilled water storage tank 8 is convenient to install and detach through the clamping groove on the inner side of the support frame 14.
The working principle is as follows: this equipment is when using, open first control valve 3 and make liquid ammonia carry to the feed liquor pipe 4 by first conveyer pipe 2 in, carry to purification jar 10 in through feed liquor pipe 4, carry to high pure water absorption bottle 11 in by third conveyer pipe 13 after 16 and the sodium hydroxide suspension 17 wash through potassium permanganate suspension in the purification jar 10, carry out the wash through the high pure water in the high pure water absorption bottle 11, absorb to in the pure water, after 19 coolings through the cold water groove, control the ammonia flow rate, then open second control valve 7, make the ammonia carry to distilled water holding vessel 8 in by second conveyer pipe 6, obtain the aqueous ammonia.
It is obvious to a person skilled in the art that the invention is not restricted to details of the above-described exemplary embodiments, but that it can be implemented in other specific forms without departing from the spirit or essential characteristics of the invention. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein. Any reference sign in a claim should not be construed as limiting the claim concerned.
Claims (6)
1. The utility model provides a synthetic equipment of irritability's aqueous ammonia is prevented to high efficiency, includes purification jar (10), its characterized in that: the inner chamber top of purification jar (10) is provided with potassium permanganate suspension (16) and sodium hydroxide suspension (17), roof (5) are installed through feed liquor pipe (4) on the top of purification jar (10), liquid ammonia storage steel tank (1) is installed at the top of roof (5), first conveyer pipe (2) is installed to one side of liquid ammonia storage steel tank (1), install first control valve (3) on first conveyer pipe (2), ultrapure water absorption bottle (11) is installed to one side of purification jar (10), the inside middle part of ultrapure water absorption bottle (11) is provided with pure water storage inner chamber (20), be provided with cold water groove (19) between the outer wall of pure water storage inner chamber (20) and ultrapure water absorption bottle (11), the internally mounted of cold water groove (19) has refrigeration coil pipe (18), third conveyer pipe (13) is installed to the bottom of ultrapure water absorption bottle (11), install third control valve (12) on third conveyer pipe (13), second conveyer pipe (6) are installed at the top of high purity water absorption bottle (11), install second control valve (7) on second conveyer pipe (6), support frame (14) are installed to the below both sides of purification jar (10), distilled water holding vessel (8) are installed to the inboard of support frame (14), connect pipe head (15) are installed to the one end of distilled water holding vessel (8), base (9) are installed to the bottom of support frame (14).
2. The high-efficiency anti-irritation ammonia water synthesis equipment according to claim 1, characterized in that: roof (5) set up to hollow structure, and roof (5) are connected with the inner chamber of purification jar (10) through feed liquor pipe (4).
3. The high-efficiency anti-irritation ammonia water synthesis equipment according to claim 1, characterized in that: liquid ammonia storage steel tank (1) are provided with five altogether, and five liquid ammonia storage steel tank (1) evenly install the top at roof (5).
4. The high-efficiency anti-irritation ammonia water synthesis equipment according to claim 1, characterized in that: the third delivery pipe (13) is installed between the purification tank (10) and the high-purity water absorption bottle (11), and the second delivery pipe (6) is installed between the high-purity water absorption bottle (11) and the distilled water storage tank (8).
5. The high-efficiency anti-irritation ammonia water synthesis equipment according to claim 1, characterized in that: the high-purity water absorption bottles (11) are provided with two high-purity water absorption bottles which are respectively and symmetrically arranged on the front and the back of the purification tank (10).
6. The high-efficiency anti-irritation ammonia water synthesis equipment according to claim 1, characterized in that: the inner side of the support frame (14) is provided with a clamping groove, and the distilled water storage tank (8) is installed on the inner side of the support frame (14) in an embedding mode.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201920441923.9U CN209872382U (en) | 2019-04-03 | 2019-04-03 | High-efficient irritability's aqueous ammonia synthesis equipment of preventing |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201920441923.9U CN209872382U (en) | 2019-04-03 | 2019-04-03 | High-efficient irritability's aqueous ammonia synthesis equipment of preventing |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN209872382U true CN209872382U (en) | 2019-12-31 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201920441923.9U Expired - Fee Related CN209872382U (en) | 2019-04-03 | 2019-04-03 | High-efficient irritability's aqueous ammonia synthesis equipment of preventing |
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| CN (1) | CN209872382U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115159543A (en) * | 2022-06-29 | 2022-10-11 | 镇江润晶高纯化工科技股份有限公司 | High-purity ammonia water preparation process capable of continuously preparing and reducing use energy consumption |
-
2019
- 2019-04-03 CN CN201920441923.9U patent/CN209872382U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115159543A (en) * | 2022-06-29 | 2022-10-11 | 镇江润晶高纯化工科技股份有限公司 | High-purity ammonia water preparation process capable of continuously preparing and reducing use energy consumption |
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| GR01 | Patent grant | ||
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| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20191231 |
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| CF01 | Termination of patent right due to non-payment of annual fee |