CN209772084U

CN209772084U - polyaniline production synthesizer

Info

Publication number: CN209772084U
Application number: CN201822197388.5U
Authority: CN
Inventors: 颜海燕
Original assignee: Xian Technological University
Current assignee: Xian Technological University
Priority date: 2018-12-17
Filing date: 2018-12-17
Publication date: 2019-12-13
Anticipated expiration: 2028-12-17

Abstract

The utility model belongs to the technical field of a preparation method of a dimensional polyaniline material, in particular to a polyaniline production and synthesis device, which comprises a reaction kettle, wherein one side of the reaction kettle is provided with a cleaning bin, and a drying bin is arranged on one side of the cleaning bin; the utility model discloses an inside utilizing the fan to blow in the outside air reation kettle, utilizing the principle of air pressure boost to blow off the material from the discharge gate, can be convenient for the staff take out the material fast, solved the problem that the material can not take out fast, through utilizing registrates between discharge gate and the feed inlet, can make things convenient for the staff to carry out lower part work with the material fast and shift.

Description

Polyaniline production synthesizer

Technical Field

The utility model belongs to the technical field of the preparation method of dimension polyaniline material, concretely relates to polyaniline produces synthesizer.

Background

Polyaniline has the characteristics of cheap raw materials, simple and convenient synthesis, stable product performance, high conductivity, excellent corrosion resistance and the like, is widely applied to the fields of electronic products, luminescent materials, batteries, electrostatic shielding, microwave absorption, metal corrosion resistance and the like, and is a high polymer material with high commercial application value.

The prior art has the following problems:

1. In the existing polyaniline production and synthesis device, when polyaniline materials are synthesized, workers generally pour the materials out, or open a discharge hole at the bottom to flow the materials out by using gravity, and the methods take longer time to take out the materials and are inconvenient for the workers to take out the materials;

2. The existing polyaniline production synthesis device is generally characterized in that a cooling pipe is arranged inside to control the temperature, but the material temperature is controlled by only one cooling pipe, so that the problem that the material cannot be sufficiently cooled is solved, the cooling pipe is easy to block due to the problem of working environment, and needs to be overhauled frequently, and the cooling pipe is not convenient to disassemble and overhaul.

SUMMERY OF THE UTILITY MODEL

To solve the problems set forth in the background art described above. The utility model provides a polyaniline produces synthesizer, has the material of being convenient for and takes out, is convenient for cool off and be convenient for maintain the characteristics of cooling tube.

In order to achieve the above object, the utility model provides a following technical scheme: the utility model provides a polyaniline produces synthesizer, includes reation kettle to and reation kettle one side is equipped with the washing storehouse, washs the dry storehouse that storehouse one side was placed, bolted connection fixed plate is passed through to reation kettle's surface one side, pressure boost gas tank has been placed to the upper surface of fixed plate, there is the fan through bolted connection in the inside of pressure boost gas tank, there is the pressure boost trachea pressure boost gas tank's one end even, the upper surface at reation kettle is connected to pressure boost trachea one end, reation kettle's surface one side below closes soon and is connected with the discharge gate, the surperficial intermediate position block of discharge gate has rotatory ring, the inside upper surface welding of discharge gate has fixed stop, the inside one side welding that is located fixed stop of rotatory ring has movable baffle, the fan is connected with external power source.

Preferably, a cooler is placed on one side of the surface of the reaction kettle, a plurality of cooling pipes are connected to one side of the cooler in a screwing mode, and one ends of the plurality of cooling pipes are connected to the inside of the reaction kettle.

Preferably, the lower surface of fixed plate has agitator motor through bolted connection, there is the stirring leaf at the bull stick axle top of agitator motor's output through rivet connection, and the top that the bull stick axle surface is located the stirring leaf evenly is connected with a plurality of puddlers through the rivet, agitator motor is connected with external power source.

Preferably, a plurality of feeding pipes are arranged on the upper surface of the reaction kettle.

preferably, the dust-proof filter screen is connected to one side of the fan in the pressurized air box through a bolt.

preferably, the joint of the surface of the cooling pipe and the reaction kettle is wound with a waterproof adhesive tape, and the cooling pipe is screwed with the reaction kettle through threads.

preferably, one end of the discharge hole is sleeved with the feed inlet.

Compared with the prior art, the beneficial effects of the utility model are that:

1. The utility model discloses an inside utilizing the fan to blow in the outside air reation kettle, utilize the principle of air pressure boost to blow off the material from the discharge gate, the staff of can being convenient for takes out the material fast, the problem that the material can not take out fast has been solved, through utilizing the registrate between discharge gate and the feed inlet, can make things convenient for the staff to carry out lower part work with the material fast and shift, the problem that the staff shifts material speed slowly and be not convenient for work and shift has been solved, can be convenient for fixed pressure boost gas tank of staff and agitator motor through setting up the fixed plate.

2. The utility model discloses an inside a plurality of cooling tubes that set up of reation kettle, two material cooling fast have been solved to convenient, can not cool off fast to and the not good problem of cooling effect, the cooling tube utilizes screw thread swivelling joint on the reaction, can the work of being convenient for dismantle the cooling tube and overhaul, utilize waterproof adhesive tape can prevent that reation kettle inside coolant liquid from flowing out.

Drawings

The accompanying drawings are included to provide a further understanding of the invention, and are incorporated in and constitute a part of this specification, illustrate embodiments of the invention, and together with the description serve to explain the invention and not to limit the invention. In the drawings:

Fig. 1 is a schematic structural view of the present invention;

FIG. 2 is an enlarged schematic view of the structure at A in FIG. 1;

FIG. 3 is a schematic view of the discharge hole structure of the present invention;

fig. 4 is a schematic view of a section structure of the discharge hole in the present invention;

FIG. 5 is a schematic view of the structure of the reaction kettle of the present invention;

FIG. 6 is a schematic view of the bottom structure of the reaction vessel of the present invention;

FIG. 7 is a schematic view of a partial structure of a connection mode of a cooling pipe and a reaction kettle in the present invention;

In the figure: 1. pressurizing the air pipe; 2. a fixing plate; 3. a reaction kettle; 4. stirring blades; 5. a discharge port; 6. a drying bin; 7. cleaning the bin; 8. a pressurized gas tank; 9. a feed pipe; 10. a stirring motor; 11. a rotating ring; 12. fixing a baffle plate; 13. moving the baffle; 14. a fan; 15. a dustproof filter screen; 16. a cooling tube; 17. a cooler; 18. a stirring rod; 19. a feed inlet; 20. a waterproof tape.

Detailed Description

The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.

Example 1

Referring to fig. 1-7, the present invention provides the following technical solutions: a polyaniline production synthesizer comprises a reaction kettle 3, a cleaning bin 7 is arranged on one side of the reaction kettle 3, a drying bin 6 is arranged on one side of the cleaning bin 7, one side of the surface of the reaction kettle 3 is connected with a fixing plate 2 through a bolt, a pressurized air box 8 is arranged on the upper surface of the fixing plate 2, a fan 14 is connected inside the pressurized air box 8 through a bolt, one end of the pressurized air box 8 is connected with a pressurized air pipe 1, one end of the pressurized air pipe 1 is connected with the upper surface of the reaction kettle 3, a discharge hole 5 is connected below one side of the surface of the reaction kettle 3 in a screwing mode, a rotating ring 11 is clamped in the middle position of the surface of the discharge hole 5, a fixed baffle 12 is welded on the inner upper surface of the discharge hole 5, a movable baffle 13 is welded on one side, which the inner portion of the rotating ring 11 is located on the fixed baffle 12, the fan 14 is connected with an external power supply, the fan 14, the worker simultaneously rotates the rotary ring 11 to overlap the movable baffle 13 with the fixed baffle 12, thereby forming the reaction vessel 3. Inside air can flow into washing storehouse 7 from discharge gate 5 through pressure in, can bring the polyaniline into washing storehouse 7 during air flow in, the staff's of being convenient for material shifts and the problem of taking out, and 3 inside bottoms of reation kettle are the inclined plane, can be convenient for the material toward discharge gate 5 department flow.

specifically, cooler 17 has been placed to reation kettle 3's surperficial one side, one side of cooler 17 closes soon and is connected with a plurality of cooling tubes 16, the inside at reation kettle 3 is connected to a plurality of cooling tubes 16 one end, and stagger about cooling tubes 16 and puddler 18, 18 rotatory time of puddler do not have the influence to cooling tubes 16, and puddler 18 glues the material when stirring, can accelerate cooling tubes 16 to the cooling of material, the temperature of better control material, and the cooling rod sets up a plurality of in reation kettle 3 inside, can more conveniently lose the material and cool off the temperature control, utilize threaded connection, the dismouting of cooling tubes 16 that can be convenient for, the staff of being convenient for overhauls cooling tubes 16.

Specifically, there is agitator motor 10 fixed plate 2's lower surface through bolted connection, there is stirring leaf 4 at the bull stick axle top of agitator motor 10's output through rivet connection, the top that the bull stick axle surface is located stirring leaf 4 is evenly connected with a plurality of puddlers 18 through the rivet, agitator motor 10 is connected with external power source, agitator motor 10 can be convenient for the staff to stir the material, it is more abundant to set up the material stirring that stirring leaf 4 and puddler 18 can be convenient for.

specifically, a plurality of inlet pipes 9 have been seted up to reation kettle 3's upper surface, and inlet pipe 9 upper end all closes soon to be connected with the lid, can prevent that the air from flowing out from inlet pipe 9 when fan 14 blows in the air toward reation kettle 3 is inside, and prevent that the dust from the inlet pipe 9 from wafting into inside reation kettle 3.

Specifically, a dust screen 15 is bolted to one side of the fan 14 inside the plenum box 8. When fan 14 blows outside air into reaction kettle 3, dust screen 15 can obstruct outside dust and prevent dust from entering reaction kettle 3.

specifically, the winding of the surface of cooling tube 16 and 3 junctions of reation kettle has waterproof sticky tape 20, and cooling tube 16 closes with reation kettle 3 through the screw soon to be connected, and cooling tube 16 and 3 junctions of reation kettle outside one end registrates waterproof rubber circle, can prevent that 3 inside liquid of reation kettle from flowing out.

Specifically, the one end registrates feed inlet 19 of discharge gate 5, 19 surperficial intermediate position blocks of feed inlet have rotatory ring 11, and 19 internal weld of feed inlet has fixed stop 12, utilize discharge gate 5 and 19 registrates feed inlet, can be convenient for reation kettle 3, load and unload between washing storehouse 7 and the dry storehouse 6, registrate discharge gate 5 and feed inlet 19 and can make reation kettle 3, accomplish work together between washing storehouse 7 and the dry storehouse 6, divide and begin, can make them accomplish work alone.

In this embodiment, the cooler 17 is manufactured by tayaoxin hydromechanical manufacturing, inc, model GLC1-0.4, which is now a known technology that is publicly and widely used in everyday life.

In this embodiment, the stirring motor 10 is a model Y31, a known technology widely used in daily life and disclosed by the southern convening limited motor limited company.

The utility model discloses a theory of operation and use flow: when the utility model is used, the material for manufacturing polyaniline is prepared by the staff, and is poured in through the inlet pipe 9, when the material is poured in from the inlet pipe 9, the staff starts the stirring motor 10, the output end of the stirring motor 10 can drive the rotating shaft to rotate, the rotating shaft can drive the stirring blade 4 and the stirring rod 18 to rotate, the stirring blade 4 and the stirring rod 18 can stir the material in the reaction kettle 3, when the stirring motor 10 is started, the cooler 17 can also inject the cooling liquid into the cooling pipe 16 to control the temperature of the material, when the polyaniline material is manufactured, the staff opens the fan 14, the fan 14 rotates to convey the external air into the reaction kettle 3 through the pressurization air pipe 1, the staff rotates the rotating ring 11 simultaneously to make the movable baffle 13 coincide with the fixed baffle 12, the air in the reaction kettle 3 can flow into the cleaning bin 7 through the pressure from the discharge port 5, can drive the polyaniline material and remove when the air flows, after the material sanitization in rinsing storehouse 7, the staff opens the pressure boost case 8 of rinsing storehouse 7 top and opens the discharge gate 5 of rinsing storehouse 7 one side, blow in the material and dry in the storehouse 6 and dry, and discharge gate 5 and feed inlet 19 are for registrates, 19 surfaces of feed inlet are also provided with discharge gate 5, can be convenient for the staff with reation kettle 3, carry out the dismouting between rinsing storehouse 7 and the dry storehouse 6, when cooling tube 16 stopped up, the staff can take off cooling tube 16 from reation kettle 3 through the rotation, maintain.

Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that modifications may be made to the embodiments described in the foregoing embodiments, or equivalents may be substituted for elements thereof. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.

Claims

1. The utility model provides a polyaniline produces synthesizer, includes reation kettle (3) to and reation kettle (3) one side is equipped with cleaning bin (7), dry storehouse (6) that cleaning bin (7) one side was placed, its characterized in that: the utility model discloses a reactor, including reation kettle (3), fixed plate (2) are passed through bolted connection to surface one side of reation kettle (3), pressure boost gas tank (8) have been placed to the upper surface of fixed plate (2), the inside of pressure boost gas tank (8) has fan (14) through bolted connection, the one end of pressure boost gas tank (8) even has pressure boost trachea (1), the upper surface at reation kettle (3) is connected to the one end of pressure boost trachea (1), the surperficial one side below of reation kettle (3) closes soon and is connected with discharge gate (5), the surperficial intermediate position block of discharge gate (5) has rotatory ring (11), the inside upper surface welding of discharge gate (5) has fixed stop (12), the inside one side welding that is located fixed stop (12) of rotatory ring (11) has movable stop (13), fan (14) are connected with external power source.

2. The apparatus for synthesizing polyaniline according to claim 1, wherein: cooler (17) have been placed to reation kettle (3) surface one side, one side of cooler (17) closes soon and is connected with a plurality of cooling tubes (16), and a plurality of cooling tube (16) one end is connected in reation kettle (3).

3. the apparatus for synthesizing polyaniline according to claim 1, wherein: the lower surface of fixed plate (2) has agitator motor (10) through bolted connection, there are stirring leaf (4) at the bull stick axle top of the output of agitator motor (10) through rivet connection, and the top that the bull stick axle surface is located stirring leaf (4) evenly is connected with a plurality of puddlers (18) through the rivet, agitator motor (10) are connected with external power source.

4. The apparatus for synthesizing polyaniline according to claim 1, wherein: a plurality of feeding pipes (9) are arranged on the upper surface of the reaction kettle (3).

5. The apparatus for synthesizing polyaniline according to claim 1, wherein: and a dustproof filter screen (15) is connected to one side of the fan (14) in the pressurizing air box (8) through a bolt.

6. The apparatus for synthesizing polyaniline according to claim 2, wherein: the surface of cooling tube (16) and reation kettle (3) junction winding have waterproof sticky tape (20), cooling tube (16) and reation kettle (3) are connected through the screw thread closure soon.

7. the apparatus for synthesizing polyaniline according to claim 1, wherein: one end of the discharge hole (5) is sleeved with a feed inlet (19).