CN209696911U - A kind of sufficient production antimony glycol reaction kettle of reaction - Google Patents
A kind of sufficient production antimony glycol reaction kettle of reaction Download PDFInfo
- Publication number
- CN209696911U CN209696911U CN201920436940.3U CN201920436940U CN209696911U CN 209696911 U CN209696911 U CN 209696911U CN 201920436940 U CN201920436940 U CN 201920436940U CN 209696911 U CN209696911 U CN 209696911U
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- Prior art keywords
- shell
- shaft
- reaction kettle
- forcing
- pump
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- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 title claims abstract description 52
- 229910052787 antimony Inorganic materials 0.000 title claims abstract description 23
- WATWJIUSRGPENY-UHFFFAOYSA-N antimony atom Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 title claims abstract description 23
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 title claims abstract description 23
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 9
- 238000010438 heat treatment Methods 0.000 claims description 22
- NJPPVKZQTLUDBO-UHFFFAOYSA-N novaluron Chemical compound C1=C(Cl)C(OC(F)(F)C(OC(F)(F)F)F)=CC=C1NC(=O)NC(=O)C1=C(F)C=CC=C1F NJPPVKZQTLUDBO-UHFFFAOYSA-N 0.000 claims description 12
- 238000007689 inspection Methods 0.000 claims description 8
- 238000007789 sealing Methods 0.000 claims description 7
- 239000000463 material Substances 0.000 abstract description 12
- 239000013078 crystal Substances 0.000 abstract description 4
- 238000010586 diagram Methods 0.000 description 4
- 238000003756 stirring Methods 0.000 description 3
- 229910000410 antimony oxide Inorganic materials 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- VTRUBDSFZJNXHI-UHFFFAOYSA-N oxoantimony Chemical compound [Sb]=O VTRUBDSFZJNXHI-UHFFFAOYSA-N 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 238000003303 reheating Methods 0.000 description 1
- 238000005316 response function Methods 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
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- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
A kind of sufficient production antimony glycol reaction kettle of reaction, it is related to a kind of reaction kettle, opposite sides in shaft (14) lower part is respectively equipped with the L shape air jet pipe (16) of open at one end and open end and the perforation of air passage (15) bottom end, multiple fumaroles (17) are respectively equipped in the other end of two L shape air jet pipes (16), " u "-shaped agitating paddle (21) are equipped in the lower end of shaft (14), cone (18) is placed in conical socket (25), and the upper end of shaft (14) is placed in through-hole (27)；The utility model is by being arranged L shape air jet pipe and " u "-shaped agitating paddle in the shaft in reaction kettle, shaft is pushed to rotate using L shape air jet pipe jet, " u "-shaped agitating paddle is driven persistently to rotate, and then material is pushed to be rotated, realizing not only hot steam can speed up the purpose that material reaction but also " u "-shaped agitating paddle can strike off the crystal for being attached to reaction kettle inner wall.
Description
[technical field]
The utility model relates to a kind of reaction kettles, more particularly, to a kind of reaction adequately production antimony glycol reaction
Kettle.
[background technique]
Reaction kettle can be understood as a kind of container physically or chemically reacted, is designed by the structure to container and is matched with parameter
Set, realize heating, evaporation, cooling and low, high speed mixture response function etc. technique require, existing reaction kettle be mostly
The inner vertical of reaction kettle is provided with a shaft, and motor and agitating paddle is respectively set in both ends of the shaft, and reaction solution is stirring
Under the action of paddle, reaction solution is driven mutually to merge, react in reaction kettle using motor driven agitating paddle；Due to ethylene glycol and
Antimony oxide reaction when heated, so design it is a material is heated using heat steam and accelerate instead
The reaction kettle answered is particularly suited for the production of production antimony glycol.
[summary of the invention]
In order to overcome the shortcomings in the background art, the utility model discloses a kind of sufficient antimony glycol that produces of reaction with instead
Kettle is answered, by the way that L shape air jet pipe and " u "-shaped agitating paddle are arranged in the shaft in reaction kettle, is pushed away using L shape air jet pipe jet
The rotation of turn axis, drives " u "-shaped agitating paddle persistently to rotate, and then material is pushed to be rotated, and realizing not only hot steam can
The purpose for accelerating material reaction and " u "-shaped agitating paddle that can strike off the crystal for being attached to reaction kettle inner wall.
In order to realize the goal of the invention, the utility model adopts the following technical solution:
A kind of reaction adequately production antimony glycol reaction kettle, including heating force (forcing) pump, shell and shaft, in shell
Equipped with cavity, the center of bottom is equipped with pedestal and is equipped with conical socket in the center of pedestal in shell, in shell
Top and the corresponding position of pedestal be equipped with through-hole, in shaft be equipped with upper end opening air passage, set in the lower end of shaft
There is cone, the opposite sides in shaft lower part is respectively equipped with the L shape spray of open at one end and open end and the perforation of air passage bottom end
Tracheae is respectively equipped with multiple fumaroles in the other end of two L shape air jet pipes, is equipped with " u "-shaped agitating paddle, cone in the lower end of shaft
Point is placed in conical socket, and the upper end of shaft is placed in through-hole, and the two sides of " u "-shaped agitating paddle connect with the inner wall of shell respectively
Touching, muff is coated in the middle part of housing exterior walls, forms cavity between muff and housing exterior walls, upper end and chamber in cavity
It is penetrated through between the upper end of body by connecting tube, is equipped with escape pipe in the lower end of cavity, is equipped in the top in case top middle position
Force (forcing) pump is heated, the snorkel of perforation air passage and heating pressurization pump output terminal is equipped between heating force (forcing) pump and through-hole, is sent
The lower end of tracheae and the upper end of shaft are in contact, and are equipped with air inlet pipe in the input terminal of heating force (forcing) pump.
The reaction adequately produces antimony glycol reaction kettle, and inspection socket, feed pipe A are additionally provided at the top of shell
With feed pipe B, cover board is hingedly connected on inspection socket.
The reaction adequately produces antimony glycol reaction kettle, and bracket is equipped between heating force (forcing) pump and shell,
It is socketed with sealing ring in the lower end of snorkel, the lower end of sealing ring and the top of shell are in close contact.
The reaction adequately produces antimony glycol reaction kettle, power supply line is equipped on heating force (forcing) pump, in power supply
The end of line is equipped with plug, is additionally provided with control switch on the power line.
The reaction adequately produces antimony glycol reaction kettle, and bearing is equipped between the upper end and through-hole of shaft.
The reaction adequately produces antimony glycol reaction kettle, is equipped with discharge nozzle in the bottom of shell.
The reaction adequately produces antimony glycol reaction kettle, and the lower end of snorkel and the upper end of shaft are matched for gap
It closes.
By adopting the above-described technical solution, the utility model has the following beneficial effects:
Reaction described in the utility model adequately produces antimony glycol reaction kettle, passes through the shaft in reaction kettle
Upper setting L shape air jet pipe and " u "-shaped agitating paddle push shaft to rotate using L shape air jet pipe jet, drive " u "-shaped stirring
Paddle persistently rotates, and then material is pushed to be rotated, and realizing not only hot steam can speed up material reaction but also " u "-shaped stirring
The purpose that paddle can strike off the crystal for being attached to reaction kettle inner wall；The utility model structure is simple, design is unique, using effect
It is good, wide market.
[Detailed description of the invention]
Fig. 1 is the structural schematic diagram of the utility model；
Fig. 2 is the schematic diagram of internal structure of the utility model shell；
Fig. 3 is the assembling structure schematic diagram of the utility model shaft and pedestal；
Fig. 4 is enlarged structure schematic diagram at the A in the utility model Fig. 2.
In figure: 1, air inlet pipe；2, force (forcing) pump is heated；3, snorkel；4, shell；5, cover board；6, inspection socket；7, muff；
8, escape pipe；9, connecting tube；10, feed pipe A；11, sealing ring；12, cavity；13, cavity；14, shaft；15, air passage；16,
L shape air jet pipe；17, fumarole；18, cone；19, plug；20, power supply line；21, " u "-shaped agitating paddle；22, feed pipe B；23,
Pedestal；24, discharge nozzle；25, conical socket；26, bearing；27, through-hole.
[specific embodiment]
The utility model can be explained in more detail by the following examples, the utility model is not limited to following
Embodiment, open the purpose of this utility model is intended to protect all changes and improvements in the scope of the utility model；
The reaction in conjunction with described in attached drawing 1~4 adequately produces antimony glycol reaction kettle, including heating force (forcing) pump 2, shell
4 and shaft 14, cavity 12 is equipped in shell 4, the center of bottom is equipped with pedestal 23 and in pedestal 23 in shell 4
Heart position is equipped with conical socket 25, through-hole 27 is equipped at the top of shell 4 and the corresponding position of pedestal 23, on the top of shell 4
Portion is additionally provided with inspection socket 6, feed pipe A10 and feed pipe B22, and cover board 5 is hingedly connected on inspection socket 6, in the bottom of shell 4
Equipped with discharge nozzle 24, it is equipped with the air passage 15 of upper end opening in shaft 14, cone 18 is equipped in the lower end of shaft 14, in shaft
The opposite sides of 14 lower parts is respectively equipped with the L shape air jet pipe 16, In of open at one end and open end and the perforation of 15 bottom end of air passage
The other end of two L shape air jet pipes 16 is respectively equipped with multiple fumaroles 17, is equipped with " u "-shaped agitating paddle 21 in the lower end of shaft 14,
Cone 18 is placed in conical socket 25, and the upper end of shaft 14 is placed in through-hole 27, is set between the upper end and through-hole 27 of shaft 14
There is bearing 26, the two sides of " u "-shaped agitating paddle 21 are in contact with the inner wall of shell 4 respectively, are coated with guarantor in the middle part of 4 outer wall of shell
Temperature covers 7, cavity 13 is formed between 4 outer wall of muff 7 and shell, by connecting between the upper end of cavity 13 and the upper end of cavity 12
Pipe 9 penetrates through, and is equipped with escape pipe 8 in the lower end of cavity 13, is equipped with heating force (forcing) pump 2, In in the top of 4 top center position of shell
It heats and is equipped with perforation air passage 15 between force (forcing) pump 2 and through-hole 27 and heats the snorkel 3 of 2 output end of force (forcing) pump, snorkel 3
Lower end and the upper end of shaft 14 are in contact, and the lower end of snorkel 3 and the upper end of shaft 14 are clearance fit, in heating force (forcing) pump 2
It is equipped with bracket between shell 4, is socketed with sealing ring 11, the lower end of sealing ring 11 and the top of shell 4 in the lower end of snorkel 3
It is in close contact, is equipped with power supply line 20 on heating force (forcing) pump 2, plug 19 is equipped in the end of power supply line 20, on power supply line 20
It is additionally provided with control switch, is equipped with air inlet pipe 1 in the input terminal of heating force (forcing) pump 2.
Implement reaction described in the utility model adequately production antimony glycol reaction kettle, in use, ethylene glycol is led to
It crosses feed pipe A10 to be injected into cavity 12, antimony oxide is injected into cavity 12 by feed pipe B22, then by air inlet
Pipe 1 connects hot steam source, and hot steam is sent to heating force (forcing) pump 2, will be hot after recycling heating 2 reheating of force (forcing) pump pressurization
Steam is successively delivered in L shape air jet pipe 16 through snorkel 3 and air passage 15, is finally erupted by fumarole 17, eruption
And the hot steam gone out pushes shaft 14 to rotate, and then L shape air jet pipe 16 and " u "-shaped agitating paddle 21 is driven to rotate, L shape jet
Pipe 16 and " u "-shaped agitating paddle 21 rotate the rotation for also having pushed mixed material, eruption and the hot steam that goes out also directly to material into
Row heating, accelerates the reaction of material, " u "-shaped agitating paddle 21 wiped off by the way when rotating be attached to 4 inner wall of shell solid it is attached
Object, further, hot steam is entered in the cavity 13 of insulating layer 7 after rising by appendix 9, is played in 4 periphery of shell
Heating prevents the effect of heat losses in shell 4, and material after the reaction was completed to be mixed is discharged by discharge nozzle 24, into lower step work
Sequence, the hot gas in muff 7 can be discharged by escape pipe 8, if reaction kettle breaks down, staff can pass through inspection socket
6 enter in cavity 12 and are overhauled, and can speed up material since the unique structure of the utility model realizes not only hot steam
The purpose that reaction and " u "-shaped agitating paddle can strike off the crystal for being attached to reaction kettle inner wall.
The non-detailed portion of the utility model is the prior art.
Claims (7)
1. a kind of reaction adequately production antimony glycol reaction kettle, including heating force (forcing) pump (2), shell (4) and shaft (14),
It is characterized in that: being equipped with cavity (12) in shell (4), pedestal (23) are equipped in the center of shell (4) interior bottom and the bottom of at
The center of seat (23) is equipped with conical socket (25), is equipped at the top of shell (4) and the corresponding position of pedestal (23) logical
Hole (27) is equipped with the air passage (15) of upper end opening in shaft (14), is equipped with cone (18) in the lower end of shaft (14), is turning
The opposite sides of axis (14) lower part is respectively equipped with the L shape air jet pipe of open at one end and open end and the perforation of air passage (15) bottom end
(16), multiple fumaroles (17) are respectively equipped in the other end of two L shape air jet pipes (16), are equipped in the lower end of shaft (14)
" u "-shaped agitating paddle (21), cone (18) are placed in conical socket (25), and the upper end of shaft (14) is placed in through-hole (27), " u "-shaped
The two sides of agitating paddle (21) are in contact with the inner wall of shell (4) respectively, are coated with muff (7) in the middle part of shell (4) outer wall,
Between muff (7) and shell (4) outer wall formed cavity (13), between the upper end of cavity (13) and the upper end of cavity (12) by
Connecting tube (9) perforation is equipped with escape pipe (8) in the lower end of cavity (13), is equipped with and adds in the top of shell (4) top center position
Hot force (forcing) pump (2), is equipped with perforation air passage (15) between heating force (forcing) pump (2) and through-hole (27) and heating force (forcing) pump (2) is defeated
The snorkel (3) of outlet, the lower end of snorkel (3) and the upper end of shaft (14) are in contact, in the input terminal of heating force (forcing) pump (2)
Equipped with air inlet pipe (1).
2. reaction according to claim 1 adequately produces antimony glycol reaction kettle, it is characterized in that: in shell (4)
Top is additionally provided with inspection socket (6), feed pipe A(10) and feed pipe B(22), cover board (5) are hingedly connected on inspection socket (6).
3. reaction according to claim 1 adequately produces antimony glycol reaction kettle, it is characterized in that: in heating force (forcing) pump
(2) between shell (4) be equipped with bracket, be socketed with sealing ring (11) in the lower end of snorkel (3), the lower end of sealing ring (11) and
The top of shell (4) is in close contact.
4. reaction according to claim 1 adequately produces antimony glycol reaction kettle, it is characterized in that: in heating force (forcing) pump
(2) power supply line (20) are equipped with, are equipped with plug (19) in the end of power supply line (20), are additionally provided with control on power supply line (20) and open
It closes.
5. reaction according to claim 1 adequately produces antimony glycol reaction kettle, it is characterized in that: in shaft (14)
Bearing (26) are equipped between upper end and through-hole (27).
6. reaction according to claim 1 adequately produces antimony glycol reaction kettle, it is characterized in that: in shell (4)
Bottom is equipped with discharge nozzle (24).
7. reaction according to claim 1 adequately produces antimony glycol reaction kettle, it is characterized in that: snorkel (3)
Lower end and the upper end of shaft (14) are clearance fit.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201920436940.3U CN209696911U (en) | 2019-04-02 | 2019-04-02 | A kind of sufficient production antimony glycol reaction kettle of reaction |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201920436940.3U CN209696911U (en) | 2019-04-02 | 2019-04-02 | A kind of sufficient production antimony glycol reaction kettle of reaction |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN209696911U true CN209696911U (en) | 2019-11-29 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201920436940.3U Active CN209696911U (en) | 2019-04-02 | 2019-04-02 | A kind of sufficient production antimony glycol reaction kettle of reaction |
Country Status (1)
| Country | Link |
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| CN (1) | CN209696911U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114570292A (en) * | 2022-03-15 | 2022-06-03 | 天驰药业有限公司 | Automatic add preparation jar of 2, 6-dichlorobenzonitrile of catalyst |
-
2019
- 2019-04-02 CN CN201920436940.3U patent/CN209696911U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114570292A (en) * | 2022-03-15 | 2022-06-03 | 天驰药业有限公司 | Automatic add preparation jar of 2, 6-dichlorobenzonitrile of catalyst |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of utility model: A fully reactive reactor for producing ethylene glycol antimony Effective date of registration: 20231102 Granted publication date: 20191129 Pledgee: Agricultural Bank of China Limited Luoyang Mengjin Sub-branch Pledgor: Luoyang Haihui New Material Co.,Ltd. Registration number: Y2023980063795 |
|
| PE01 | Entry into force of the registration of the contract for pledge of patent right |