CN209630650U - A kind of double amino sulfur trifluoride production systems - Google Patents
A kind of double amino sulfur trifluoride production systems Download PDFInfo
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- CN209630650U CN209630650U CN201920261213.8U CN201920261213U CN209630650U CN 209630650 U CN209630650 U CN 209630650U CN 201920261213 U CN201920261213 U CN 201920261213U CN 209630650 U CN209630650 U CN 209630650U
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- tube
- middle position
- distillery
- double amino
- amino sulfur
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Abstract
The utility model relates to double amino sulfur trifluoride production technical fields, and disclose a kind of double amino sulfur trifluoride production systems, the middle position of two lateral roof of tower body inner wall is connect with the two sides of distillery respectively, the upper container is located at the middle position inside distillery, and the middle position of upper container outer surface is connect by stabilizing bracket with the middle position for distilling chamber interior walls two sides.The utility model is passed through by the operation of blower and the cold air of cold air access tube, solenoid valve is opened simultaneously, in container under double amino sulfur trifluorides of liquid condition are entered by connecting tube, whole liquid be presented spiral-flow type dispersion and under, cold air is cooperated to arrange distributed cold gas, double amino sulfur trifluorides can be made to be rapidly cooled cooling, double amino sulfur trifluorides are rapidly cooled after impurity is precipitated in distillation to reach, the combinative stability for guaranteeing double amino sulfur trifluoride overall molecules simultaneously, to improve the purpose of yield.
Description
Technical field
The utility model relates to double amino sulfur trifluoride production technical fields, specially a kind of double amino sulfur trifluoride productions
System.
Background technique
Double amino sulfur trifluorides are a kind of chemical substances, and molecular formula C6H14F3NO2S, it is Celsius that boiling point is more than or equal to 80
Degree, the closed container that condition of storage is 2-8 DEG C, double amino sulfur trifluorides are a kind of new chemical synthetics, in Chemical Manufacture
In have critical role, in the production process of double amino sulfur trifluorides, need to the mixed solutions of double amino sulfur trifluorides into
Impurity is precipitated in row distillation, then carries out cooling down, but existing device can not be to the chemical property of double amino sulfur trifluorides
It is operated, is rapidly cooled after distillation, destruction is easily generated for the stability of molecule of double amino sulfur trifluorides, thus
Leading to entire process, there are many drawbacks, such as generate pernicious gas or cause double amino sulfur trifluoride solution variations, therefore
In the production of double amino sulfur trifluorides, need one kind that can quickly carry out cooling destilling tower after distillation.
Utility model content
The purpose of this utility model is to provide a kind of double amino sulfur trifluoride production systems, having reached makes double amino three
Sulfur fluoride is rapidly cooled after impurity is precipitated in distillation, while guaranteeing the combinative stability of double amino sulfur trifluoride overall molecules
Property, to improve the purpose of yield.
To achieve the above object, the utility model provides the following technical solutions: a kind of double amino sulfur trifluoride production systems,
Including tower body, distillery, upper container, lower container, stabilizing bracket, inlet tube, helix tube, snorkel, air distribution plate, steam access tube,
Vapour-discharge tube, connecting tube, solenoid valve, control panel, outlet tube, cold air row, cold air access tube, blower, under-chassis, in the tower body
The middle position of two lateral roof of wall is connect with the two sides of distillery respectively, and the upper container is located at the interposition inside distillery
It sets, and the middle position of upper container outer surface is connect by stabilizing bracket with the middle position for distilling chamber interior walls two sides, the feed liquor
One end of pipe is through the top distilled on the left of chamber interior walls and extends to inside it, the right end of the inlet tube and one end of helix tube
Connection, and the other end of helix tube is connected to the middle position at upper container front top, one end of the snorkel and upper container
The middle position at top is connected to, and the two sides of the air distribution plate are connect with the top of tower body inner wall two sides respectively, the snorkel
Top is connected to the middle position of air distribution plate bottom, and exhaust smoke hole is provided at the top of the air distribution plate, the steam access tube
One end is connected to the bottom on the left of distillery, and the top on the right side of the distillery is connected to one end of vapour-discharge tube, the company
One end of adapter tube is connected to the bottom of upper container, and the middle position of the lower container outer surface passes through stabilizing bracket and tower body inner wall
Two sides connection, the bottom of the connecting tube are connected to the top of lower container, and the solenoid valve is located in connecting tube, the outlet tube
One end be connected to the middle position of lower container bottom, and the other end of outlet tube through tower body right side and extend to outside it
Portion, the two sides of the control panel are connect with the two sides of tower body inner wall respectively, and the top of control panel is located under lower container bottom
It is square, through-hole is provided on the control panel, the two sides of the cold air row are connect with the two sides of tower body inner wall respectively, and cold air row
Top is located at the lower section of control panel bottom, and one end of the cold air access tube is connected to the middle position on cold air row right side, described
The bottom of blower is connect with the middle position of tower body inner wall bottom.
Preferably, the surrounding of the tower body bottom is connect with the top of four under-chassis respectively, and the bottom of under-chassis is connected with
Resilient cushion.
Preferably, the helix tube is arranged relative to the surrounding of distillation chamber interior walls in circulating type, and the material of helix tube is
Heat Conduction Material.
Preferably, the vertical cross-section shape of the upper container and lower container is taper, and upper container and lower container are opposite
In the middle position of connecting tube in symmetry status.
Preferably, the vertical cross-section shape of the through-hole is taper, and the diameter of via bottoms is twice of top diameter.
Preferably, the surrounding of the distillation chamber interior walls is provided with thermal insulation material, and the shape of distillery is rectangle.
The utility model provides a kind of double amino sulfur trifluoride production systems.Have it is following the utility model has the advantages that
(1), the utility model being separately provided by distillery, the double amino sulfur trifluorides of liquid by inlet tube and
When helix tube enters inside upper container, steam access tube is to being passed through high-temperature steam, the double amino sulfur trifluorides of liquid inside distillery
Distillation operation is sufficiently carried out when carrying out heating distillation when flowing in helix tube, while entering inside upper container, and is matched and closed
Container tapered form can be such that liquid is sufficiently heated evenly, to improve whole distilling rate and quality.
(2), the utility model is passed through by the operation of blower and the cold air of cold air access tube, while solenoid valve is opened, In
When double amino sulfur trifluorides of liquid condition enter lower container by connecting tube, whole liquid be presented spiral-flow type dispersion and under,
Cooperate cold air to arrange distributed cold gas, double amino sulfur trifluorides can be made to be rapidly cooled cooling, so that having reached makes
Double amino sulfur trifluorides are rapidly cooled after impurity is precipitated in distillation, while guaranteeing the group of double amino sulfur trifluoride overall molecules
Stability is closed, to improve the purpose of yield.
Detailed description of the invention
Fig. 1 is the front cut-away view of the utility model structure；
Fig. 2 is the front schematic view of the utility model structure tandem container；
Fig. 3 is the top view of the utility model structure air distribution plate.
In figure: 1 tower body, 2 distilleries, 3 upper containers, 4 lower containers, 5 stabilizing brackets, 6 inlet tubes, 7 helix tubes, 8 snorkels, 9
Air distribution plate, 10 exhaust smoke holes, 11 steam access tubes, 12 vapour-discharge tubes, 13 connecting tubes, 14 solenoid valves, 15 control panels, 16 through-holes,
17 outlet tubes, 18 cold air row, 19 cold air access tubes, 20 blowers, 21 under-chassis.
Specific embodiment
As shown in Figure 1-3, the utility model provides a kind of technical solution: a kind of double amino sulfur trifluoride production systems, packet
Include tower body 1, distillery 2, upper container 3, lower container 4, stabilizing bracket 5, inlet tube 6, helix tube 7, snorkel 8, air distribution plate 9, steam
Access tube 11, vapour-discharge tube 12, connecting tube 13, solenoid valve 14, control panel 15, outlet tube 17, cold air arrange 18, cold air access tube
19, the middle position of blower 20, under-chassis 21,1 inner wall of tower body, two lateral roof is fixedly connected with the two sides of distillery 2 respectively, upper appearance
Device 3 is located at the middle position inside distillery 2, and the middle position of 3 outer surface of upper container passes through in stabilizing bracket 5 and distillery 2
The middle position of wall two sides is fixedly connected, and the top that one end of inlet tube 6 is run through on the left of 2 inner wall of distillery simultaneously extends in it
The right end in portion, inlet tube 6 is connected to one end of helix tube 7, and the centre at 3 front top of the other end of helix tube 7 and upper container
One end of position connection, snorkel 8 is connected to the middle position at 4 top of upper container, and the two sides of air distribution plate 9 are respectively and in tower body 1
Wall is fixedly connected at the top of two sides, and the top of snorkel 8 is connected to the middle position of 9 bottom of air distribution plate, and the top of air distribution plate 9 is opened
Equipped with exhaust smoke hole 10, one end of steam access tube 11 is connected to the bottom in 2 left side of distillery, the top on 2 right side of distillery and steaming
One end of vapour discharge pipe 12 is connected to, and one end of connecting tube 13 is connected to the bottom of upper container 3, the interposition of lower 4 outer surface of container
It sets and is fixedly connected by stabilizing bracket 5 with the two sides of 1 inner wall of tower body, the bottom of connecting tube 13 is connected to the top of lower container 4, electromagnetism
Valve 14 is located in connecting tube 13, and one end of outlet tube 17 is connected to the middle position of lower 4 bottom of container, and outlet tube 17 is another
End is run through the right side of tower body 1 and is extended to outside it, and the two sides of control panel 15 are fixedly connected with the two sides of 1 inner wall of tower body respectively,
And the top of control panel 15 is located at the lower section of lower 4 bottom of container, and through-hole 16, the two sides point of cold air row 18 are offered on control panel 15
It is not fixedly connected with the two sides of 1 inner wall of tower body, and the top of cold air row 18 is located at the lower section of 15 bottom of control panel, cold air access tube
19 one end is connected to the middle position on 18 right side of cold air row, and the bottom of blower 20 and the middle position of 1 inner wall bottom of tower body are solid
Fixed connection, the surrounding of 1 bottom of tower body is fixedly connected with the top of four under-chassis 21 respectively, and the bottom of under-chassis 21 is fixedly connected with
Resilient cushion, helix tube 7 are arranged relative to the surrounding of 2 inner wall of distillery in circulating type, and the material of helix tube 7 is Heat Conduction Material,
The vertical cross-section shape of upper container 3 and lower container 4 is taper, and the centre of upper container 3 and lower container 4 relative to connecting tube 13
Position is in symmetry status, and the vertical cross-section shape of through-hole 16 is taper, and the diameter of 16 bottom of through-hole is twice of top diameter,
The surrounding of 2 inner wall of distillery is provided with thermal insulation material, and the shape of distillery 2 is rectangle, the utility model.
When in use, when the double amino sulfur trifluorides of liquid enter 3 inside of upper container by inlet tube 6 and helix tube 7,
Steam access tube 11 carries out when flowing in helix tube 7 to high-temperature steam, the double amino sulfur trifluorides of liquid are passed through inside distillery 2
Distillation operation, while operation and the cold air access tube 19 of blower 20 are sufficiently carried out when heating up and distill, while entering 3 inside of upper container
Cold air be passed through, while solenoid valve 14 open, liquid condition double amino sulfur trifluorides by connecting tube 13 entrance under container 4
When, whole liquid be presented spiral-flow type dispersion and under, the cold gas that cooperation cold air row 18 is distributed can make double amino trifluoros
Change sulphur and is rapidly cooled cooling.
Can to sum up obtain: the utility model is separately provided by distillery 2, passes through feed liquor in the double amino sulfur trifluorides of liquid
When pipe 6 and helix tube 7 enter 3 inside of upper container, for steam access tube 11 to high-temperature steam is passed through inside distillery 2, liquid is double
Amino sulfur trifluoride carries out heating distillation when flowing in helix tube 7, while sufficiently carrying out distillation work when entrance 3 inside of upper container
Industry, and cooperate 3 tapered form of upper container, can be such that liquid is sufficiently heated evenly, thus improve whole distilling rate with
And quality, the utility model are passed through by the operation of blower 20 and the cold air of cold air access tube 19, while solenoid valve 14 is opened, In
When double amino sulfur trifluorides of liquid condition enter lower container 4 by connecting tube 13, whole liquid be presented spiral-flow type dispersion and
Under, the cold gas that cooperation cold air row 18 is distributed can make double amino sulfur trifluorides be rapidly cooled cooling, to reach
It is rapidly cooled double amino sulfur trifluorides after impurity is precipitated in distillation, while guaranteeing double amino sulfur trifluoride overall molecules
Combinative stability, to improve the purpose of yield.
Claims (6)
1. a kind of double amino sulfur trifluoride production systems, including it is tower body (1), distillery (2), upper container (3), lower container (4), steady
Gu frame (5), inlet tube (6), helix tube (7), snorkel (8), air distribution plate (9), steam access tube (11), vapour-discharge tube
(12), connecting tube (13), solenoid valve (14), control panel (15), outlet tube (17), cold air arrange (18), cold air access tube (19), wind
Machine (20), under-chassis (21), it is characterised in that: the middle position of two lateral roof of tower body (1) inner wall respectively with distillery (2)
Two sides connection, the upper container (3) are located at the internal middle position of distillery (2), and the middle position of upper container (3) outer surface
It is connect by stabilizing bracket (5) with the middle position of distillery (2) inner wall two sides, distillery is run through in one end of the inlet tube (6)
(2) it the top on the left of inner wall and extends to inside it, the right end of the inlet tube (6) is connected to one end of helix tube (7), and spiral shell
The other end of coil (7) is connected to the middle position at upper container (3) front top, one end of the snorkel (8) and upper container
(3) the middle position connection at the top of, the two sides of the air distribution plate (9) are connect with the top of tower body (1) inner wall two sides respectively, described
The top of snorkel (8) is connected to the middle position of air distribution plate (9) bottom, is provided with exhaust smoke hole at the top of the air distribution plate (9)
(10), one end of the steam access tube (11) is connected to the bottom on the left of distillery (2), the top on the right side of the distillery (2)
Portion is connected to the one end of vapour-discharge tube (12), and one end of the connecting tube (13) is connected to the bottom of upper container (3), under described
The middle position of container (4) outer surface is connect by stabilizing bracket (5) with the two sides of tower body (1) inner wall, the connecting tube (13)
Bottom is connected to the top of lower container (4), and the solenoid valve (14) is located on connecting tube (13), one end of the outlet tube (17)
It is connected to the middle position of lower container (4) bottom, and the other end of outlet tube (17) runs through the right side of tower body (1) and extends to it
Under outside, the two sides of the control panel (15) are connect with the two sides of tower body (1) inner wall respectively, and the top of control panel (15) is located at
The lower section of container (4) bottom is provided with through-hole (16) on the control panel (15), the two sides of the cold air row (18) respectively with tower
The two sides of body (1) inner wall connect, and the top of cold air row (18) is located at the lower section of control panel (15) bottom, the cold air access tube
(19) one end is connected to the middle position on the right side of cold air row (18), the bottom and tower body (1) inner wall bottom of the blower (20)
Middle position connection.
2. a kind of double amino sulfur trifluoride production systems according to claim 1, it is characterised in that: tower body (1) bottom
The surrounding in portion is connect with the top of four under-chassis (21) respectively, and the bottom of under-chassis (21) is connected with resilient cushion.
3. a kind of double amino sulfur trifluoride production systems according to claim 1, it is characterised in that: the helix tube (7)
Surrounding relative to distillery (2) inner wall is arranged in circulating type, and the material of helix tube (7) is Heat Conduction Material.
4. a kind of double amino sulfur trifluoride production systems according to claim 1, it is characterised in that: the upper container (3)
Vertical cross-section shape with lower container (4) is taper, and upper container (3) and lower container (4) are relative in connecting tube (13)
Between position be in symmetry status.
5. a kind of double amino sulfur trifluoride production systems according to claim 1, it is characterised in that: the through-hole (16)
Vertical cross-section shape is taper, and the diameter of through-hole (16) bottom is twice of top diameter.
6. a kind of double amino sulfur trifluoride production systems according to claim 1, it is characterised in that: the distillery (2)
The surrounding of inner wall is provided with thermal insulation material, and the shape of distillery (2) is rectangle.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201920261213.8U CN209630650U (en) | 2019-03-01 | 2019-03-01 | A kind of double amino sulfur trifluoride production systems |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201920261213.8U CN209630650U (en) | 2019-03-01 | 2019-03-01 | A kind of double amino sulfur trifluoride production systems |
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| Publication Number | Publication Date |
|---|---|
| CN209630650U true CN209630650U (en) | 2019-11-15 |
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| CN201920261213.8U Expired - Fee Related CN209630650U (en) | 2019-03-01 | 2019-03-01 | A kind of double amino sulfur trifluoride production systems |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115448892A (en) * | 2022-09-19 | 2022-12-09 | 郑州铁路职业技术学院 | Synthetic method of benzothiadiazole heterocyclic compound |
-
2019
- 2019-03-01 CN CN201920261213.8U patent/CN209630650U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115448892A (en) * | 2022-09-19 | 2022-12-09 | 郑州铁路职业技术学院 | Synthetic method of benzothiadiazole heterocyclic compound |
| CN115448892B (en) * | 2022-09-19 | 2023-07-07 | 郑州铁路职业技术学院 | Synthesis method of benzothiadiazole heterocyclic compound |
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| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20191115 |