CN209630647U - A kind of serialization preparation facilities of silicone oil - Google Patents
A kind of serialization preparation facilities of silicone oil Download PDFInfo
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- CN209630647U CN209630647U CN201920008437.8U CN201920008437U CN209630647U CN 209630647 U CN209630647 U CN 209630647U CN 201920008437 U CN201920008437 U CN 201920008437U CN 209630647 U CN209630647 U CN 209630647U
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- reaction kettle
- alembic
- silicone oil
- preparation facilities
- base substrate
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Abstract
The utility model discloses a kind of serialization preparation facilities of silicone oil, are related to silicone oil preparation technical field, mainly for solution must not continuous production and the problem that causes efficiency lower；The preparation facilities, including preparing reaction kettle, alembic and base substrate, reaction kettle lower end is prepared by supporting roofbolt to be fixed on base substrate upper surface, the preparation reactor bottom side wall is connected to inside alembic by conduction pipe, conduction pipe is inclined to set and the bottom end of conduction pipe is connected to alembic upper end, it prepares and is connected with inlet tube on the side wall of reaction kettle upper end, the bottom end of alembic is provided with the heating furnace to heat alembic, water and oil separator is additionally provided on base substrate, the liquid feeding end of water and oil separator is connected to the gas outlet of distillation upper end by gas-guide tube, liquefier is provided in the middle part of gas-guide tube.The utility model structure is simple, can continuity prepare silicone oil, processing efficiency is higher, can be purified and guarantee purity, and easy to operate, practicability is stronger.
Description
Technical field
The utility model relates to silicone oil preparation technical field, the serialization preparation facilities of specifically a kind of silicone oil.
Background technique
Silicone oil is commonly referred to as keeping the linear polysiloxanes product of liquid condition at room temperature, is generally divided into methyl-silicone oil
With two class of modified silicon oil, most common silicone oil monomethyl silicone oil, also referred to as common silicone oil, all methyl of organic group, first
Base silicone oil has good chemical stability, insulating properties, and hydrophobic performance is good.
The method of most common production silicone oil industrial at present are as follows: cyclosiloxane and end-capping reagent are in acidic catalyst or alkalinity
Preparation is reacted under catalyst action, and the silicone oil prepared at present all contains more impurity mostly, needs individually to be purified
Processing, increase process and can not continuity preparation production, production efficiency is lower.
Utility model content
The purpose of this utility model is to provide a kind of serialization preparation facilities of silicone oil, must not continuous production with solution
And the problem for causing efficiency lower.
To achieve the above object, the utility model provides the following technical solutions:
A kind of serialization preparation facilities of silicone oil, including reaction kettle, alembic and base substrate are prepared, it prepares under reaction kettle
By supporting roofbolt to be fixed on base substrate upper surface, the preparation reactor bottom side wall is connected to steaming by conduction pipe at end
It evaporates inside tank, conduction pipe is inclined to set and the bottom end of conduction pipe is connected to alembic upper end, prepares reaction kettle upper end side
Inlet tube is connected on wall, the bottom end of alembic is provided with the heating furnace to heat alembic, is additionally provided on base substrate
Water and oil separator, the liquid feeding end of water and oil separator are connected to the gas outlet of distillation upper end by gas-guide tube, set in the middle part of gas-guide tube
It is equipped with liquefier, the first valve is provided in the middle part of the conduction pipe, be provided with the second liner on the inside of the alembic, in second
A heating cavities are formed between gallbladder and distillation top tank structure, reaction kettle inner wall is prepared and is provided with the first liner, the first liner and system
A heat insulation cavity is formed between standby reaction kettle inner wall, is connected between the heat insulation cavity and heating cavities by connection tracheae
It connects, the second valve is installed on the connection tracheae.
Based on the above technical solution, the utility model also provides following optional technical solution:
In a kind of optinal plan: the end of the inlet tube is connected with multiple-way valve.
In a kind of optinal plan: being provided with multiple vertical liquefaction draft tubes in the liquefier, multiple liquefaction are through-flow
Pipe joins end to end connect between each other.
In a kind of optinal plan: described prepare is additionally provided with rotating bar axis inside reaction kettle, the connection of rotating bar axis top
In the stirring motor prepared on reaction kettle roof is arranged in, multiple agitator arms are provided on the side wall of rotating bar axis.
In a kind of optinal plan: described prepare is provided with connection and prepares safety inside reaction kettle on reaction kettle roof
Valve.
Compared to the prior art, the beneficial effects of the utility model are as follows:
1, the silicone oil of preparation can be purified by the setting of alembic and the first valve, guarantees its purity, and can connect
Continuous property preparation, improves the production efficiency of product；
2, the waste heat that can be generated in distillation by the connection setting of the second liner and the first liner is to preparing reaction kettle
The reaction efficiency for heating and silicone oil being accelerated to prepare, improves the efficiency of preparation；
3, the utility model structure is simple, can continuity prepare silicone oil, processing efficiency is higher, can be purified and guarantee it
Purity, easy to operate, practicability is stronger.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the utility model.
Fig. 2 is the structural schematic diagram in the utility model another kind embodiment inside liquefier.
Appended drawing reference annotation: reaction kettle 1, alembic 2, liquefier 3, water and oil separator 4, conduction pipe 5, the first valve are prepared
Door 6, gas-guide tube 7, safety valve 8, inlet tube 9, multiple-way valve 10, base substrate 11, support roofbolt 12, the first liner 13, connection gas
Pipe 14, the second valve 15, the second liner 16, heating furnace 17, rotating bar axis 18, agitator arm 19, stirring motor 20, liquefaction draft tube
21。
Specific embodiment
Following embodiment can be described in detail the utility model in conjunction with attached drawing, similar or identical in attached drawing or explanation
Part uses identical label, and in practical applications, and shape, thickness or the height of each component can be expanded or shunk.This reality
It is only to illustrate the utility model with novel cited each embodiment, not to limit the scope of the utility model.To this
Spirit and scope of any modification apparent easy to know or change made by utility model without departure from the utility model.
Embodiment 1
Referring to Fig. 1, in the utility model embodiment, a kind of serialization preparation facilities of silicone oil, including prepare reaction kettle
1, alembic 2 and base substrate 11 prepare 1 lower end of reaction kettle by supporting roofbolt 12 to be fixed on 11 upper surface of base substrate, make
Standby 1 bottom sidewall of reaction kettle is connected to inside alembic 2 by conduction pipe 5, and conduction pipe 5 is inclined to set and conduction pipe
5 bottom end is connected to 2 upper end of alembic, prepares and is connected with inlet tube 9 on 1 upper end side wall of reaction kettle, and the end of inlet tube 9 connects
It is connected to multiple-way valve 10, the setting of multiple-way valve 10 can connect multiple inlet tubes and enter convenient for liquid feeding and prepare inside reaction kettle 1, steam
The bottom end for evaporating tank 2 is provided with heating furnace 17 to heat alembic 2, is additionally provided with water and oil separator 4, water on base substrate 11
The liquid feeding end of oil eliminator 4 is connected to the gas outlet on 2 top of alembic by gas-guide tube 7, is provided with liquefier in the middle part of gas-guide tube 7
3, the first valve 6 is provided in the middle part of the conduction pipe 5, and the second liner 16, the second liner 16 are provided on the inside of the alembic 2
A heating cavities are formed between 2 inner wall of alembic, are prepared 1 inner wall of reaction kettle and are provided with the first liner 13, the first liner 13
A heat insulation cavity is formed between 1 inner wall of reaction kettle with preparing, and passes through connection tracheae between the heat insulation cavity and heating cavities
14 are connected, and the second valve 15 is equipped on the connection tracheae 14, and stoste generates silicon in the reaction that carries out for preparing reaction kettle 1
Oil is flow in alembic 2 by opening 6 silicone oil of the first valve by conduction pipe 5, and alembic 2 is under the heating of heating furnace 17
Silicone oil is distilled, the silicone oil of distillation flows into liquefier 3 in the form of gas, liquefies under the cooling effect of liquefier 3
And water-oil separation is carried out by water and oil separator 4, to can effectively improve the preparation purity of silicone oil by distillation, pass through first
The setting of valve 6 is prepared and is reacted inside reaction kettle 1 when alembic 2 is distilled, and then can be carried out continuously silicone oil system
It is standby, the efficiency of preparation is improved, and the setting of the second liner 16 and the first liner 13 can flow to guarantor in the cavity hot gas of heating cavities
In warm cavity, and then the temperature for preparing the reaction of reaction kettle 1 can be provided, guarantee the efficiency of silicone oil preparation, set in the liquefier 3
Multiple vertical liquefaction draft tubes 21 are equipped with, multiple liquefaction draft tubes 21 join end to end between each other to be connect, and then is improved liquefied
Efficiency.
Embodiment 2
Referring to Fig. 2, the utility model embodiment difference from example 1 is that: it is described to prepare inside reaction kettle 1
It is additionally provided with rotating bar axis 18,18 top of rotating bar axis is connected to the stirring motor 20 for being arranged in and preparing on 1 roof of reaction kettle, turns
It is provided with multiple agitator arms 19 on the side wall of lever axis 18, drives the rotation of agitator arm 19 that can accelerate silicone oil by stirring motor 20
Raw material comes into full contact with, and improves reaction efficiency, and described prepare is provided with connection on 1 roof of reaction kettle and prepares inside reaction kettle 1
Safety valve 8 to avoid because of reaction so that prepare pressure in reaction kettle 1 it is excessively high due to influence the preparation reaction of silicone oil.
The above, the only specific embodiment of the disclosure, but the protection scope of the disclosure is not limited thereto, it is any
Those familiar with the art can easily think of the change or the replacement in the technical scope that the disclosure discloses, and should all contain
It covers within the protection scope of the disclosure.Therefore, the protection scope of the disclosure should be subject to the protection scope in claims.
Claims (5)
1. a kind of serialization preparation facilities of silicone oil, including reaction kettle (1), alembic (2) and base substrate (11) are prepared, it prepares
Reaction kettle (1) lower end is by supporting roofbolt (12) to be fixed on base substrate (11) upper surface, which is characterized in that the preparation reaction
Kettle (1) bottom sidewall is connected to alembic (2) inside by conduction pipe (5), and conduction pipe (5) is inclined to set and diversion pipe
The bottom end in road (5) is connected to alembic (2) upper end, prepares and is connected with inlet tube (9), alembic on the side wall of reaction kettle (1) upper end
(2) bottom end is provided with the heating furnace (17) to heat alembic (2), and base substrate is additionally provided with water and oil separator on (11)
(4), the liquid feeding end of water and oil separator (4) is connected to the gas outlet on alembic (2) top by gas-guide tube (7), in gas-guide tube (7)
Portion is provided with liquefier (3), is provided with the first valve (6) in the middle part of the conduction pipe (5)；
It is provided with the second liner (16) on the inside of the alembic (2), forms one between the second liner (16) and alembic (2) inner wall
A heating cavities prepare reaction kettle (1) inner wall and are provided with the first liner (13), the first liner (13) and prepare in reaction kettle (1)
A heat insulation cavity is formed between wall, is connected between the heat insulation cavity and heating cavities by connecting tracheae (14), it is described
The second valve (15) are installed in connection tracheae (14).
2. the serialization preparation facilities of silicone oil according to claim 1, which is characterized in that the end of the inlet tube (9)
It is connected with multiple-way valve (10).
3. the serialization preparation facilities of silicone oil according to claim 1, which is characterized in that setting in the liquefier (3)
There are multiple vertical liquefaction draft tubes (21), multiple liquefaction draft tubes (21) join end to end connect between each other.
4. the serialization preparation facilities of silicone oil according to claim 1 to 3, which is characterized in that described to prepare reaction kettle
(1) internal to be additionally provided with rotating bar axis (18), rotating bar axis (18) top, which is connected to, to be arranged on preparing reaction kettle (1) roof
Stirring motor (20) is provided with multiple agitator arms (19) on the side wall of rotating bar axis (18).
5. the serialization preparation facilities of silicone oil according to claim 4, which is characterized in that described to prepare reaction kettle (1) top
It is provided with connection on wall and prepares the internal safety valve (8) of reaction kettle (1).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201920008437.8U CN209630647U (en) | 2019-01-03 | 2019-01-03 | A kind of serialization preparation facilities of silicone oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201920008437.8U CN209630647U (en) | 2019-01-03 | 2019-01-03 | A kind of serialization preparation facilities of silicone oil |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN209630647U true CN209630647U (en) | 2019-11-15 |
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ID=68477012
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| Application Number | Title | Priority Date | Filing Date |
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| CN201920008437.8U Active CN209630647U (en) | 2019-01-03 | 2019-01-03 | A kind of serialization preparation facilities of silicone oil |
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| CN (1) | CN209630647U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114225859A (en) * | 2021-12-21 | 2022-03-25 | 名之图(苏州)高新材料有限公司 | Low-loss silicone oil processing system |
| CN114768284A (en) * | 2021-12-22 | 2022-07-22 | 广州锐澄医疗技术有限公司 | Purification method of silicone oil for intraocular tamponade |
-
2019
- 2019-01-03 CN CN201920008437.8U patent/CN209630647U/en active Active
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114225859A (en) * | 2021-12-21 | 2022-03-25 | 名之图(苏州)高新材料有限公司 | Low-loss silicone oil processing system |
| CN114225859B (en) * | 2021-12-21 | 2024-02-23 | 名之图(苏州)高新材料有限公司 | Low-loss silicone oil processing system |
| CN114768284A (en) * | 2021-12-22 | 2022-07-22 | 广州锐澄医疗技术有限公司 | Purification method of silicone oil for intraocular tamponade |
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