CN209576681U - Additive synthesis temperature control system - Google Patents
Additive synthesis temperature control system Download PDFInfo
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- CN209576681U CN209576681U CN201920143223.1U CN201920143223U CN209576681U CN 209576681 U CN209576681 U CN 209576681U CN 201920143223 U CN201920143223 U CN 201920143223U CN 209576681 U CN209576681 U CN 209576681U
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- CN
- China
- Prior art keywords
- reaction kettle
- water bath
- autoclave body
- kettle
- anchor ear
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Abstract
The utility model belongs to chemosynthesis reaction apparatus field, and in particular to a kind of additive synthesis temperature control system.Including reaction kettle and thermostat water bath, the thermostat water bath be can external temperature sensor thermostat water bath, temperature sensor is had additional in the reaction kettle, the reaction kettle is laminated glass reaction kettle, the signal input part of the temperature sensor output end and thermostat water bath connects, the utility model using can external temperature sensor thermostat water bath, and reaction kettle is laminated glass reaction kettle, so that thermostat water bath monitors the water temperature in reaction kettle automatically, realize the monitoring in the pot of water temperature and outside pot, guarantee the constant temperature accuracy of temperature when reaction, the real simulation production reaction condition of reaction kettle, the consistency of guarantee test and actual production.
Description
Technical field
The utility model belongs to chemosynthesis reaction apparatus field, and in particular to a kind of additive synthesis temperature control system
System.
Background technique
Existing synthesis system includes reaction kettle, recirculated water bath, peristaltic pump, small powder dropwise addition bottle etc..
Recirculated water bath is connected with water inlet/water outlet of reaction kettle, realizes water-bath circulation to control temperature of reaction kettle；
Peristaltic pump imbibition end connects small powder and bottle is added dropwise, and outlet end connects reaction kettle feed inlet, and the dropwise addition speed of small powder is controlled by peristaltic pump
Degree.
Existing test reaction kettle and production synthesis reactor, thermal insulation property difference is big, and recirculated water bath is unable to adjust automatically
Temperature.When needing the synthesis condition of complete simulated production in test, need to manually adjust temperature water bath bath temperature, operation is multiple
Miscellaneous, temperature control effect is poor.Temperature is important synthetic reaction condition, therefore test kettle is caused not react in production process really
The problem of.
Utility model content
For the utility model in order to solve above-mentioned problems of the prior art, the utility model provides a kind of additive
Synthesis temperature control system, is capable of the constant of guarantee test temperature, and the real simulation production reaction condition of reaction kettle improves existing
Have pilot system can not accurate simulated production temperature rise the problem of, the consistency of guarantee test and actual production.
The specific technical solution that the utility model uses is:
Additive synthesis temperature control system, including reaction kettle and thermostat water bath, the thermostat water bath is can be outer
The thermostat water bath of jointing temp sensor, temperature sensor is had additional in the reaction kettle, and the reaction kettle is interlayer glass
The signal input part of glass reaction kettle, the temperature sensor output end and thermostat water bath connects, and the reaction kettle includes
The water outlet of first reaction kettle and the second reaction kettle, first reaction kettle is connect with the water inlet of the second reaction kettle, described
The water outlet of the second reaction kettle and the water inlet end of thermostat water bath connect, the water outlet of thermostat water bath and the first reaction kettle
Water inlet connection.
First reaction kettle and the second reaction kettle structure is identical, all includes the fixation of autoclave body and the support autoclave body
Frame is provided with the kettle cover of feed inlet on the autoclave body, is fixed with cricoid retainer plate, the fixation on the kettle cover
Hand-tighten bolts are threaded on circle, the autoclave body is connect by anchor ear with fixed frame, and the anchor ear is cyclic structure set
On the outside of autoclave body, the anchor ear is connect by connecting rod with fixed frame, and setting is twisted with hand on retainer plate on the anchor ear
The corresponding bolt hole of bolt location, the hand-tighten bolts pass through retainer plate and are threadedly coupled with the bolt hole formation on anchor ear, institute
The lower end for the autoclave body stated is provided with pallet, and the pallet is connect by connecting rod with fixed frame.
Agitating shaft is provided in the reaction kettle, the agitating shaft passes through kettle cover and protrudes into autoclave body inner cavity, and described stirs
Axis is mixed by the motor driven being suspended above reaction kettle, is provided with gimbal coupling between the motor and agitating shaft.
The motor by the column and the cantilever support that is arranged on column being connected with fixed frame, the cantilever with
Column is set with and is formed being slidably matched along column axis direction, and the motor is fixed on the free end of cantilever, the electricity
The output end of machine is arranged straight down.
The anchor ear is in the semicircle ring structure of left and right, is provided with engaging lug between the semicircle ring structure, two sides
Semicircle ring structure is connected by the bolt for being interspersed in engaging lug as close ring structure, and the autoclave body is clamped in the inner ring of anchor ear
Side.
The beneficial effects of the utility model are:
The utility model using can external temperature sensor thermostat water bath, and reaction kettle be laminated glass react
Kettle realizes the monitoring in the pot of water temperature and outside pot so that thermostat water bath monitors the water temperature in reaction kettle automatically, when guaranteeing reaction
The constant temperature accuracy of temperature, the real simulation production reaction condition of reaction kettle, the consistency of guarantee test and actual production.
Detailed description of the invention
Fig. 1 is the principles of the present invention block diagram；
Fig. 2 is the structural schematic diagram of the utility model reaction kettle；
Fig. 3 is the schematic diagram in anchor ear partial top direction；
In attached drawing, 1, water outlet, 2, water inlet, 3, autoclave body, 4, fixed frame, 5, kettle cover, 6, anchor ear, 7, agitating shaft, 8, electricity
Machine, 9, gimbal coupling, 10, column, 11, cantilever, 12, engaging lug, 13, pallet, 14, retainer plate, 15, hand-tighten bolts.
Specific embodiment
With reference to the accompanying drawing and specific embodiment the utility model is described in further detail:
Specific embodiment is as shown in Figures 1 and 2, and the utility model is a kind of additive synthesis temperature control system, including
Reaction kettle and thermostat water bath, the thermostat water bath be can external temperature sensor thermostat water bath, the reaction
Temperature sensor is had additional in kettle, the reaction kettle is laminated glass reaction kettle, the temperature sensor output end and perseverance
The signal input part of warm water bath connects, and the reaction kettle includes the first reaction kettle and the second reaction kettle, and described first is anti-
The water outlet 1 of kettle is answered to connect with the water inlet 2 of the second reaction kettle, the water outlet 1 and thermostat water bath of second reaction kettle
Water inlet end connection, the water outlet of thermostat water bath is connect with the water inlet 2 of the first reaction kettle.
The thermostat water bath that the utility model uses for, can external temperature sensor model DC-4030 water at low temperature
Bath, the settable thermostat temperature of the water-bath, low temperature heat automatically, and high temperature stops heating, are supervised by external temperature sensor
The temperature in reaction kettle is surveyed, guarantees that the closed loop of reaction temperature is controllable, which monitors that external temp sensor temperature is lower than
Begun to warm up when preset temperature to realize the constant of reaction temperature, guarantee the constant temperature effect of consersion unit, improve experimental facilities with
The consistency of performance of production equipment.The laminated glass reaction kettle improves the heat insulation effect of reaction kettle, avoids the big of temperature
Amplitude fluctuation, and the one or two reaction kettle being arranged is connected by circulation the volume for extending experimental facilities, further by experiment effect
It is mutually close with actual production, actual production equipment is simulated, the monitoring and control of reaction is convenient for.Arrow direction is in Fig. 1
The direction of reaction liquid flowing.
Further, first reaction kettle and the second reaction kettle structure are identical, all include autoclave body 3 and the support kettle
The fixed frame 4 of body 3 is provided with the kettle cover 5 of feed inlet on the autoclave body 3, is fixed with cricoid fixation on the kettle cover 5
14 are enclosed, is threaded with hand-tighten bolts 15 on the retainer plate 14, the autoclave body 3 is connect by anchor ear 6 with fixed frame 4,
The anchor ear 6 is that cyclic structure is sleeved on 3 outside of autoclave body, and the anchor ear 6 is connect by connecting rod with fixed frame 4, described
Anchor ear 6 on corresponding with 15 position of hand-tighten bolts on retainer plate 14 bolt hole of setting, the hand-tighten bolts 15 pass through fixation
Circle 14 is threadedly coupled with the bolt hole formation on anchor ear 6, and the lower end of the autoclave body 3 is provided with pallet, and the pallet 13 is borrowed
Connecting rod is helped to connect with fixed frame 4.Autoclave body 3 is embraced by anchor ear 6, autoclave body 3 is avoided to lodge, the pallet 13 of setting plays support kettle
The effect of body 3, the discharge outlet that autoclave body bottom end is arranged in pass through the leakage of pallet 13 on the outside, the water outlet of same 3 lower end of autoclave body setting
Mouth 1 is also stretched out in 13 downside of pallet, and the upper end of 3 side wall of autoclave body is arranged in the water inlet 2 of autoclave body 3.
Further, as shown in Fig. 2, being provided with agitating shaft 7 in the reaction kettle, the agitating shaft 7 passes through kettle cover
3 inner cavity of autoclave body is protruded into, the agitating shaft 7 drives by the motor 8 being suspended above reaction kettle, the motor 8 and stirring
Gimbal coupling 9 is provided between axis 7.Since agitating shaft 7 needs to protrude into autoclave body 3 across kettle cover, by universal joint
Shaft coupling 9 connects motor 8 and agitating shaft 7, reduces required precision when installation, guarantees peace and quiet, the stable rotation of agitating shaft.
Further, the motor 8 is by the column 10 being connected with fixed frame 4 and the cantilever 11 being arranged on column 10
Support, the cantilever 11 are set with column 10 and are formed being slidably matched along 10 axis direction of column, and the motor 8 is fixed
Output end in the free end of cantilever 11, the motor 8 is arranged straight down.By the position liter of cantilever 11 and column 10
Drop plays the mixing position adjusting for adjusting agitating shaft 7, by pass through 11 suit portion of cantilever between the cantilever 11 and column 10
The bolt of position is frictionally secured with the formation of column 10.
Further, as shown in figure 3, the anchor ear 6 in left and right semicircle ring structure, between the semicircle ring structure
It is provided with engaging lug 12, the semicircle ring structure of two sides is connected by the bolt for being interspersed in engaging lug 12 as close ring structure, institute
The autoclave body 3 stated is clamped in the inner ring side of anchor ear 6.Anchor ear 6 and autoclave body 3 are fixed by separate structure, guarantee the steady of autoclave body 3
Fixed, the connecting rod of anchor ear 6 is fixedly connected with fixed frame, so that autoclave body 3 forms a fixed connection with fixed frame, guarantees the stabilization of autoclave body
Property, the anchor ear 6 and pallet 13 are plastic material, and metal tie rods is avoided to form the cooling that heat bridge causes autoclave body, improve temperature
The constancy of degree.
Claims (5)
1. additive synthesis temperature control system, including reaction kettle and thermostat water bath, it is characterised in that: the water bath with thermostatic control
Pot for can external temperature sensor thermostat water bath, have additional temperature sensor, the reaction kettle in the reaction kettle
For laminated glass reaction kettle, the signal input part of the temperature sensor output end and thermostat water bath is connected, and described is anti-
Answering kettle includes the first reaction kettle and the second reaction kettle, the water inlet of water outlet (1) and the second reaction kettle of first reaction kettle
Mouth (2) connection, the water outlet (1) of second reaction kettle are connect with the water inlet end of thermostat water bath, and thermostat water bath goes out
Water end (W.E.) is connect with the water inlet (2) of the first reaction kettle.
2. additive synthesis temperature control system according to claim 1, it is characterised in that: first reaction kettle and
Second reaction kettle structure is identical, all the fixed frame (4) including autoclave body (3) and the support autoclave body (3), on the autoclave body (3)
It is provided with the kettle cover (5) of feed inlet, is fixed with cricoid retainer plate (14), the retainer plate on the kettle cover (5)
(14) it is threaded on hand-tighten bolts (15), the autoclave body (3) is connect by anchor ear (6) with fixed frame (4), and described embraces
Hoop (6) is that cyclic structure is sleeved on the outside of autoclave body (3), and the anchor ear (6) is connect by connecting rod with fixed frame (4), described
Anchor ear (6) on corresponding with hand-tighten bolts (15) position on retainer plate (14) bolt hole of setting, the hand-tighten bolts (15)
It is threadedly coupled across retainer plate (14) with the bolt hole formation on anchor ear (6), the lower end of the autoclave body (3) is provided with pallet
(13), the pallet (13) is connect by connecting rod with fixed frame (4).
3. additive synthesis temperature control system according to claim 2, it is characterised in that: setting in the reaction kettle
Have agitating shaft (7), the agitating shaft (7) passes through kettle cover and protrudes into autoclave body (3) inner cavity, and the agitating shaft (7) is by being suspended at
Motor (8) driving above reaction kettle, is provided with gimbal coupling (9) between the motor (8) and agitating shaft (7).
4. additive synthesis temperature control system according to claim 3, it is characterised in that: the motor (8) by
It the column (10) that is connected with fixed frame (4) and cantilever (11) on column (10) is set supports, the cantilever (11) and vertical
Column (10) is set with and simultaneously forms being slidably matched along column (10) axis direction, and the motor (8) is fixed on oneself of cantilever (11)
By holding, the output end of the motor (8) is arranged straight down.
5. additive synthesis temperature control system according to claim 2, it is characterised in that: the anchor ear (6) is in a left side
Right semicircle ring structure is provided with engaging lug (12) between the semicircle ring structure, and the semicircle ring structure of two sides is by interspersed
It is connected in the bolt of engaging lug (12) as close ring structure, the autoclave body (3) is clamped in the inner ring side of anchor ear (6).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201920143223.1U CN209576681U (en) | 2019-01-28 | 2019-01-28 | Additive synthesis temperature control system |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201920143223.1U CN209576681U (en) | 2019-01-28 | 2019-01-28 | Additive synthesis temperature control system |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN209576681U true CN209576681U (en) | 2019-11-05 |
Family
ID=68380990
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201920143223.1U Active CN209576681U (en) | 2019-01-28 | 2019-01-28 | Additive synthesis temperature control system |
Country Status (1)
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|---|---|
| CN (1) | CN209576681U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112892632A (en) * | 2019-12-04 | 2021-06-04 | 大唐环境产业集团股份有限公司 | Constant temperature water bath device |
-
2019
- 2019-01-28 CN CN201920143223.1U patent/CN209576681U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112892632A (en) * | 2019-12-04 | 2021-06-04 | 大唐环境产业集团股份有限公司 | Constant temperature water bath device |
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