CN209549439U - The preparation facilities of phase double emulsion gel in a kind of DHA algal oil is high - Google Patents

The preparation facilities of phase double emulsion gel in a kind of DHA algal oil is high Download PDF

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CN209549439U
CN209549439U CN201822006645.2U CN201822006645U CN209549439U CN 209549439 U CN209549439 U CN 209549439U CN 201822006645 U CN201822006645 U CN 201822006645U CN 209549439 U CN209549439 U CN 209549439U
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magnetic ball
ball impact
impact chamber
micro
phase
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邹立强
刘伟
谢安琪
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Jianqixing Life Sciences Shanghai Co ltd
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Nanchang University
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Abstract

The utility model provides the preparation facilities of phase double emulsion gel in a kind of DHA algal oil height, including oily phase feed inlet, micro- magnetic ball impact chamber, magnetic ball impact chamber, discharge port and the first, second water phase injection port;The oil phase feed inlet, the first water phase injection port are connected to the side of micro- magnetic ball impact chamber respectively, and the other side of micro- magnetic ball impact chamber is connected to the magnetic ball impact chamber, and the second water phase injection port is connected to the magnetic ball impact chamber;Micro- magnetic ball impact chamber and magnetic ball impact chamber are all set in alternating magnetic field, and micro- magnetic ball impact chamber and the intracavitary portion of magnetic ball impact are equipped with several magnetic balls.The utility model can realize the continuous preparation of phase " w/o/w " double emulsion gel in DHA algal oil height, product stability is good, it also can obviously improve the unstable phenomenons such as bleed, the condensate oil in high fat liquor storage, DHA algal oil is locked in internal cavities, reduction system oxygen content promotes product stability performance.

Description

The preparation facilities of phase double emulsion gel in a kind of DHA algal oil is high
Technical field
The utility model belongs to double emulsion technical field, and in particular to phase double emulsion gel in a kind of DHA algal oil is high Preparation facilities.
Background technique
Double emulsion is the highly structural fluid that more droplet is wrapped in a kind of dispersed phase drop, is broadly divided into W/O/ W type and O/W/O type.Double emulsion can be used as carrier, is isolated, protected and controlled release to drug, active constituent, in agriculture The industries such as industry, food, medical treatment and cosmetics have obtained extensive utilization.
High Internal Phase Emulsion refers to a kind of lotion of the dispersed phase volume fraction 74% or more.The body of dispersed phase in ordinary emulsion Fraction is generally 30-40%, highest to reach 50%.Dispersed phase drop is dispersed in continuous phase with mutual disjunct spherical shape. If continuing growing the volume fraction of dispersed phase, when the tightly packed spherical shape at interconnection of dispersed phase drop, at this time Dispersed phase volume fraction is 74%.Dispersed phase volume fraction is further increased, will occur to squeeze mutually between drop, Zhi Daokong Between maximum saturation, formed High Internal Phase Emulsion.
The preparation process of double emulsion and High Internal Phase Emulsion is more mature, however, being restricted by many factors, phase in height Double emulsion is also difficult to prepare, and crucial core equipment is also badly in need of developing.
Utility model content
For phase double emulsion in current height preparation it is more difficult the problems such as, the utility model is provided in a kind of DHA algal oil height The preparation facilities of phase double emulsion gel.
The utility model discloses a kind of preparation facilities of phase double emulsion gel in DHA algal oil height, including oil mutually to feed Mouth, micro- magnetic ball impact chamber, magnetic ball impact chamber, discharge port and the first, second water phase injection port;The oil phase feed inlet, first Water phase injection port is connected to the side of micro- magnetic ball impact chamber respectively, the other side of micro- magnetic ball impact chamber and the magnetic ball Impact cavity connection, the second water phase injection port are connected to the magnetic ball impact chamber;Micro- magnetic ball impact chamber and magnetic ball impact Chamber is all set in alternating magnetic field, and micro- magnetic ball impact chamber and the intracavitary portion of magnetic ball impact are equipped with several magnetic balls.
The diameter of the intracavitary magnetic ball of micro- magnetic ball impact is equal;The magnetic ball that the intracavitary portion of the magnetic ball impact is placed be two kinds not Same diameter.
Compared with prior art, the beneficial effects of the utility model are shown:
1, the utility model is crosslinked whey protein isolate by calcium carbonate-gluconolactone, is aided with dynamic magnetic ball impact skill Art prepares lotion, so that the oil phase content of double emulsion can achieve 90% or more, much higher than common High Internal Phase Emulsion, together When reduce the dosage of surfactant, avoid lamination of the lotion in storage, stability is more preferable.
2, phase gel emulsion has tridimensional network in the DHA algal oil height of the utility model preparation, can obviously improve height The unstable phenomenons such as bleed, condensate oil in fat liquor storage, DHA algal oil are locked in internal cavities, reduce system oxygen content, Performance for stability is promoted, also controllable DHA algal oil Targeting delivery and the release for slowing down flavor substance.Green-tea extract is anti-oxidant Ability can slow down by force DHA algal oil oxidation, and green tea faint scent can good cover algae oil fishy smell.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the preparation facilities of phase double emulsion gel in a kind of DHA algal oil height in the utility model.
Specific embodiment:
In order to which the above objects, features, and advantages of the utility model are more clearly understood, with reference to the accompanying drawing and The utility model is described in further detail for embodiment.It should be clear that these examples are merely to illustrate the utility model still It is not limited only to the scope of the utility model.
The utility model discloses a kind of preparation facilities of phase double emulsion gel in DHA algal oil height, including oil mutually to feed Mouth 1, micro- magnetic ball impact chamber 2, magnetic ball impact chamber 3, discharge port 4 and the first, second water phase injection port 5,6;The oil is mutually fed Mouthful the 1, first water phase injection port 5 is connected to the side of micro- magnetic ball impact chamber 2 respectively, micro- magnetic ball impact chamber 2 it is another Side is connected to the magnetic ball impact chamber 3, and the second water phase injection port 6 is connected to the magnetic ball impact chamber 3;Micro- magnetic ball is hit It hits chamber 2 and magnetic ball impact chamber 3 is all set in alternating magnetic field, if being equipped with inside micro- magnetic ball impact chamber 2 and magnetic ball impact chamber 3 Dry magnetic ball, oily phase feed liquid enter micro- magnetic ball impact chamber 2 by oily phase injection port 1, and aqueous phase liquid is entered micro- by the first water phase feed inlet 5 Magnetic ball impact chamber 2.Under the action of alternating magnetic field, magnetic ball inside micro- magnetic ball impact chamber 2 is high with aqueous phase liquid and oily phase feed liquid Frequency collides, and achievees the effect that grease merges, obtains lotion;Aqueous phase liquid can be hit by the second water phase feed inlet 6 into magnetic ball later Chamber 3 is hit, is mixed in 3 inside of magnetic ball impact chamber with the lotion flowed out in micro- magnetic ball impact chamber 2, while in the work for adding alternating magnetic field outside With lower mutual shock, after oil water mixture double emulsions, is flowed out from discharging pipeline 4, cream is crosslinked by calcium carbonate-gluconolactone Clear protein isolate is aided with dynamic magnetic ball impact technology to prepare lotion, so that the oil phase content of double emulsion can achieve 90% More than, much higher than common High Internal Phase Emulsion, while reducing the dosage of surfactant, avoids lotion in storage Lamination, stability is more preferable.
The diameter of magnetic ball is equal in micro- magnetic ball impact chamber 2;The magnetic ball placed inside the magnetic ball impact chamber 3 is two kinds Different-diameter can make the more uniform of material impacting, and the oil phase content of oil water mixture double emulsion can be made far high In common High Internal Phase Emulsion.
Embodiment 1
(1) pre-process: by 5kg gelatin, 0.2kg green-tea extract is dissolved in 100kg water, 500rpm stirring and dissolving, is adjusted PH to 6 is saved, is obtained as aqueous phase liquid A;By 5kg whey protein isolate, 534g glucolactone and 150g dissolution of calcium carbonate in In 100kg drinking water, 500rpm is stirred to being completely dissolved, and then heats 30min at 85 DEG C, obtains aqueous phase liquid B;
(2) preparation of substance lotion: oil is obtained after 150kg DHA algal oil and the mixing of 3kg polyglycereol poly ricinoleate Phase feed liquid is imported under 70MPa high pressure in the oily phase injection port 1 of dynamic magnetic ball impact device, while aqueous phase liquid A is in 70MPa It is imported under pressure from the first water phase injection port 5;Magnetic ball, water phase material under the action of alternating magnetic field, inside micro- magnetic ball impact chamber 2 Liquid A and the oily mutual high frequency of phase feed liquid are hit, and are achieved the effect that grease merges, are obtained colostric fluid;
(3) preparation of double emulsion: using and import aqueous phase liquid B from the second water phase injection port 6 in 70MPa high pressure, In Under the action of alternating magnetic field, magnetic ball, aqueous phase liquid B and colostric fluid inside magnetic ball impact chamber 3 are hit mutually, from discharging pipeline 4 Cooling after export, product is detected.
Embodiment 2
(1) pre-process: by 5kg gelatin, 0.2kg green-tea extract is dissolved in 100kg water, 500rpm stirring and dissolving, is adjusted PH to 6 is saved, is obtained as aqueous phase liquid A;By 5kg whey protein isolate, 534g glucolactone and 150g dissolution of calcium carbonate in In 100kg drinking water, 500rpm is stirred to being completely dissolved, and then heats 30min at 85 DEG C, obtains aqueous phase liquid B;
(2) preparation of substance lotion: oil is obtained after 150kg DHA algal oil and the mixing of 3kg polyglycereol poly ricinoleate Phase feed liquid is passed through at dynamic high-pressure Microfluidizer together after mixing aqueous phase liquid A, aqueous phase liquid B and oily phase feed liquid Reason, processing pressure 70MPa are detected after gained feed liquid is cooling.
Embodiment 3
(1) pre-process: by 5kg gelatin, 0.2kg green-tea extract is dissolved in 100kg water, 500rpm stirring and dissolving, is adjusted PH to 6 is saved, is obtained as aqueous phase liquid A;5kg whey protein isolate is dissolved in 100kg drinking water, 500rpm is stirred to complete Dissolution, then heats 30min at 85 DEG C, obtains aqueous phase liquid B;
(2) preparation of substance lotion: after 150kg DHA algal oil and the mixing of 3kg polyglycereol poly ricinoleate, in 60- It is imported under 80MPa high pressure in the oily phase injection port 1 of dynamic magnetic ball impact device, while 50kg aqueous phase liquid A is pressed in 60-80MPa It is imported under power from the first water phase injection port 5;Magnetic ball, aqueous phase liquid under the action of alternating magnetic field, inside micro- magnetic ball impact chamber 2 A and the oily mutual high frequency of phase feed liquid are hit, and are achieved the effect that grease merges, are obtained colostric fluid;
(3) preparation of double emulsion: using and import aqueous phase liquid B from the second water phase injection port 6 in 70MPa high pressure, In Under the action of alternating magnetic field, magnetic ball, aqueous phase liquid B and colostric fluid inside magnetic ball impact chamber 3 are hit mutually, from discharging pipeline 4 Cooling after export, product is detected.
Phase " w/o/w " type double emulsion gel sensory evaluation scores table in table 1 DHA algal oil height
2 Analyses Methods for Sensory Evaluation Results of table
3 physical and chemical property determining result of table
Learnt by the interpretation of result of table 2, table 3 and Fig. 1: the sample of embodiment 1 is a more perfect product.With implementation Example 1 is compared, and embodiment 2 prepares High Internal Phase Emulsion using traditional dynamic high-pressure Microfluidizer, and product cut size is larger, is easy There is the flocculation or aggregation of drop, stability, hardness, elastic force is all weaker, and the situation of bleed or condensate oil is more apparent;In embodiment 3 In, product does not use calcium carbonate-gluconolactone crosslinking whey protein isolate to stablize in height to lotion, steady only with emulsifier Determine lotion, the complete bleed of products obtained therefrom, condensate oil, hardness, elastic force is all poor.Product is common algae oil double emulsion in embodiment 4, Stability is preferable.The product of embodiment 1 can keep original state after long-term storage, not be in the presence of bleed or condensate oil, and Emulsion droplet partial size is smaller, is evenly distributed, and has been maximally maintained the original nutritive value of product.The result shows that passing through carbon Sour calcium-gluconolactone is crosslinked whey protein isolate, is aided with dynamic magnetic ball impact device, can prepare phase " w/o/ in DHA algal oil height W " type double emulsion gel.
The above description is only the embodiments of the present invention, and therefore it does not limit the scope of the patent of the utility model, needs Illustrate term " on ", "lower", "left", "right" " top ", " bottom ", "vertical", "horizontal", "inner", "outside" such as occur Deng, indicated by orientation or positional relationship be based on the orientation or positional relationship shown in the drawings, be merely for convenience of description this Utility model and simplified description, rather than the device or element of indication or suggestion meaning must have a particular orientation, with specific Orientation construction and operation, therefore should not be understood as limiting the present invention.In addition, such as there is term " first ", " Two ", " third " is used for descriptive purposes only and cannot be understood as indicating or suggesting relative importance.In the description of the utility model In, it should be noted that unless otherwise clearly defined and limited, such as there is term " installation ", " connected ", " connection " should be done extensively Reason and good sense solution may be a detachable connection for example, it may be being fixedly connected, or the connection of one;It can be mechanical connection, It can be electrical connection;It can be directly connected, the company inside two elements can also be can be indirectly connected through an intermediary It is logical.For the ordinary skill in the art, above-mentioned term in the present invention specific can be understood with concrete condition Meaning, equivalents made by using the description of the utility model and the drawings are applied directly or indirectly in relevant Technical field is also included in the patent protection scope of the utility model.

Claims (2)

1. the preparation facilities of phase double emulsion gel in a kind of DHA algal oil height, it is characterised in that:
Including oily phase feed inlet (1), micro- magnetic ball impact chamber (2), magnetic ball impact chamber (3), discharge port (4) and the first, second water Phase injection port (5,6);
The oil phase feed inlet (1), the first water phase injection port (5) are connected to the side of micro- magnetic ball impact chamber (2) respectively, institute The other side for stating micro- magnetic ball impact chamber (2) is connected to the magnetic ball impact chamber (3), the second water phase injection port (6) with it is described Magnetic ball impact chamber (3) connection;
Micro- magnetic ball impact chamber (2) and magnetic ball impact chamber (3) are all set in alternating magnetic field, micro- magnetic ball impact chamber (2) It is internal equipped with several magnetic balls with magnetic ball impact chamber (3).
2. the preparation facilities of phase double emulsion gel in a kind of DHA algal oil height as described in claim 1, it is characterised in that: institute The diameter for stating micro- interior magnetic ball of magnetic ball impact chamber (2) is equal;The magnetic ball placed inside the magnetic ball impact chamber (3) is that two kinds of differences are straight Diameter.
CN201822006645.2U 2018-11-30 2018-11-30 The preparation facilities of phase double emulsion gel in a kind of DHA algal oil is high Active CN209549439U (en)

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Address before: 200000 Room 201, floor 2, building 13, No. 1218, Huateng Road, Huaxin Town, Qingpu District, Shanghai

Patentee before: Shanghai Fengsheng Health Technology Co.,Ltd.