CN209502964U - A kind of automatic high temperature and high pressure gas reaction nano metal composite material prepares furnace - Google Patents
A kind of automatic high temperature and high pressure gas reaction nano metal composite material prepares furnace Download PDFInfo
- Publication number
- CN209502964U CN209502964U CN201822216090.4U CN201822216090U CN209502964U CN 209502964 U CN209502964 U CN 209502964U CN 201822216090 U CN201822216090 U CN 201822216090U CN 209502964 U CN209502964 U CN 209502964U
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- Prior art keywords
- high temperature
- pressure
- valve
- sealing flange
- steel pipe
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- 238000006243 chemical reaction Methods 0.000 title claims abstract description 21
- 239000002905 metal composite material Substances 0.000 title claims abstract description 14
- 238000007789 sealing Methods 0.000 claims abstract description 42
- 229910000851 Alloy steel Inorganic materials 0.000 claims abstract description 24
- 239000002184 metal Substances 0.000 claims abstract description 24
- 229910052751 metal Inorganic materials 0.000 claims abstract description 24
- 238000010438 heat treatment Methods 0.000 claims abstract description 14
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims abstract description 9
- 238000001816 cooling Methods 0.000 claims abstract description 9
- 229910052802 copper Inorganic materials 0.000 claims abstract description 9
- 239000010949 copper Substances 0.000 claims abstract description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 9
- 239000010935 stainless steel Substances 0.000 claims description 10
- 229910001220 stainless steel Inorganic materials 0.000 claims description 10
- 238000003780 insertion Methods 0.000 claims description 3
- 230000037431 insertion Effects 0.000 claims description 3
- 210000000038 chest Anatomy 0.000 claims description 2
- 239000000463 material Substances 0.000 abstract description 8
- 239000002131 composite material Substances 0.000 abstract description 6
- 239000002086 nanomaterial Substances 0.000 abstract description 2
- 238000003786 synthesis reaction Methods 0.000 abstract description 2
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 abstract 1
- 239000010931 gold Substances 0.000 abstract 1
- 229910052737 gold Inorganic materials 0.000 abstract 1
- 239000007789 gas Substances 0.000 description 17
- 239000007769 metal material Substances 0.000 description 5
- 238000000034 method Methods 0.000 description 4
- 230000001681 protective effect Effects 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 238000009833 condensation Methods 0.000 description 2
- 230000005494 condensation Effects 0.000 description 2
- 239000002114 nanocomposite Substances 0.000 description 2
- 239000012495 reaction gas Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 238000007792 addition Methods 0.000 description 1
- 229910045601 alloy Inorganic materials 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 235000019628 coolness Nutrition 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000010304 firing Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 229920002994 synthetic fiber Polymers 0.000 description 1
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- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The utility model discloses a kind of automatic high temperature and high pressure gas reaction nano metal composite material and prepares furnace, air inlet needle-valve is covered including double card, automatic pressure relief valve, pressure gauge, pressure sensor, first sealing flange, red copper sealing ring, high temperature alloy steel pipe, response sample boat, water cooling fixed frame, heating furnace and metal plate furnace body, the two sides of the metal plate furnace body are symmetrically installed with two water cooling fixed frames, the metal plate furnace body is internally provided with heating furnace, the high temperature alloy steel pipe runs through metal plate furnace body and heating furnace, and the inside of the high temperature alloy steel pipe is fixedly connected with response sample boat, the both ends of the high temperature alloy steel pipe pass through red copper sealing ring and are tightly connected respectively with the first sealing flange and the second sealing flange, the bottom of first sealing flange is fixedly connected with automatic pressure relief valve, this prepares furnace, nano material and gold Belong to material and lower high-pressure synthesis reaction is protected by high temperature and high pressure gas, obtains high quality composite material.
Description
Technical field
The utility model relates to metal nanometer composite material synthetic reaction equipment technical fields, and in particular to a kind of automatic height
Warm high pressure gas reaction nano metal composite material prepares furnace.
Background technique
Synthetic material is done at this stage using being hot-press equipment, and pressurization up and down, fires certain temperature in closed cavity
The mode pressed when burning arrives composite material, and the determination of this technique is that Impact direction is up and down, to obtain quality of materials
Apparent defect.And it cannot achieve some gas source reaction under high pressure tests during the test.
Utility model content
In order to overcome above-mentioned technical problem, the purpose of this utility model is to provide a kind of automatic high temperature and high pressure gas is anti-
It answers nano metal composite material to prepare furnace, protects lower high-pressure synthesis anti-by high temperature and high pressure gas nano material and metal material
It answers, obtains high quality composite material.
The purpose of this utility model can be achieved through the following technical solutions:
A kind of automatic high temperature and high pressure gas reaction nano metal composite material prepares furnace, including double card set air inlet needle-valve,
Check valve, automatic pressure relief valve, pressure gauge, pressure sensor, the first sealing flange, red copper sealing ring, high temperature alloy steel pipe, reaction
Example boat, water cooling fixed frame, pressure safety valve, pressure security needle-valve, the second sealing flange, exhaust valve, heating furnace and metal plate
Furnace body, the two sides of the metal plate furnace body are symmetrically installed with two water cooling fixed frames, and the metal plate furnace body is internally provided with heating furnace
Thorax, the high temperature alloy steel pipe runs through metal plate furnace body and heating furnace, and the inside of the high temperature alloy steel pipe is fixedly connected
There is response sample boat, it is close with the first sealing flange and second respectively that the both ends of the high temperature alloy steel pipe pass through red copper sealing ring
Flange seal connection is sealed, is fixedly connected with pressure sensor at the top of first sealing flange, first sealing flange
Bottom is fixedly connected with automatic pressure relief valve, the one end of first sealing flange far from high temperature alloy steel pipe and internal screw thread stainless steel
One interface of threeway is connected by pipeline, and the top interface of the internal screw thread Stainless steel tee is connect with pressure gauge, the interior spiral shell
Line Stainless steel tee is connect far from an interface of pipeline with check valve, and the side of the check valve is equipped with double card set air inlet needle
Valve, double card set air inlet needle-valve one end offer double card set air inlet, pass through pipeline at the top of second sealing flange
It is connect with pressure safety valve and pressure security needle-valve, the bottom of second sealing flange is connect by pipeline with exhaust valve.
As a further solution of the present invention: the side of the metal plate furnace body is fixedly connected with control system switch,
The side insertion of the control system switch is equipped with temperature control display screen, and the pressure sensor is electrically connected control system switch
Input terminal, the output end of the control system switch is electrically connected temperature control display screen.
As a further solution of the present invention: the pressure safety valve and pressure security needle-valve are installed in an angle of 90 degrees.
The utility model has the beneficial effects that this equipment prepares the composite material of high quality by the way of high temperature and pressure,
Using high temperature alloy steel pipe as closed carrying sample chamber, both ends are equipped with CF sealing flange as disassembly dress and take sample, configure
It is constant as temperature to be equipped with temperature control system as guaranteeing that chamber pressure is stable for pressure sensor control system；Sample is placed high
On response sample boat in temperature alloy steel pipe, heat and be passed through protective gas a to level pressure, while entering cavity by gas
Interior Pintsch process reaction and the intracorporal metal material of chamber react under high pressure-temperature, prepare the nano composite of high quality
Material；The nano metal material capability and performance reacted at high temperature under high pressure simultaneously is excellent, so that the metal nano for obtaining high quality is multiple
Condensation material；
The device of gas source synthetic reaction under effective solution high temperature and pressure, efficiently solves gas reaction at high temperature under high pressure
Prepare the nano metal composite material of high quality；Solution cannot realize chemical vapor in high temperature and pressure in the prior art
The problem of reaction, provides effective means to prepare the nano metal composite material of high quality.
Detailed description of the invention
The utility model will be further described below with reference to the accompanying drawings.
Fig. 1 is the utility model reacting furnace the schematic diagram of the section structure.
In figure: 1, double card covers air inlet needle-valve；2, check valve；3, automatic pressure relief valve；4, pressure gauge；5, pressure sensor；
6, the first sealing flange；7, red copper sealing ring；8, high temperature alloy steel pipe；9, response sample boat；10, water cooling fixed frame；11, pressure
Safety valve；12, pressure security needle-valve；13, the second sealing flange；14, exhaust valve；15, heating furnace；16, metal plate furnace body；17,
Temperature control display screen；18, control system switch；19, double card covers air inlet；20, internal screw thread Stainless steel tee.
Specific embodiment
Below in conjunction with the utility model embodiment, the technical scheme in the embodiment of the utility model is carried out clear, complete
Site preparation description, it is clear that the described embodiments are only a part of the embodiments of the utility model, instead of all the embodiments.
Based on the embodiments of the present invention, obtained by those of ordinary skill in the art without making creative efforts
All other embodiment, fall within the protection scope of the utility model.
Refering to Figure 1, a kind of automatic high temperature and high pressure gas reaction nano metal composite material prepares furnace, including double card
Cover air inlet needle-valve 1, check valve 2, automatic pressure relief valve 3, pressure gauge 4, pressure sensor 5, the first sealing flange 6, red copper sealing
Circle 7, high temperature alloy steel pipe 8, response sample boat 9, water cooling fixed frame 10, pressure safety valve 11, pressure security needle-valve 12, second are close
Envelope flange 13, exhaust valve 14, heating furnace 15 and metal plate furnace body 16, the two sides of metal plate furnace body 16 are symmetrically installed with two water coolings and fix
Frame 10, metal plate furnace body 16 are internally provided with heating furnace 15, and high temperature alloy steel pipe 8 runs through metal plate furnace body 16 and heating furnace
15, and the inside of high temperature alloy steel pipe 8 is fixedly connected with response sample boat 9, it is close that the both ends of high temperature alloy steel pipe 8 pass through red copper
Seal 7 is tightly connected with the first sealing flange 6 and the second sealing flange 13 respectively, and the top of the first sealing flange 6 is fixedly connected
There is pressure sensor 5, the bottom of the first sealing flange 6 is fixedly connected with automatic pressure relief valve 3, and the first sealing flange 6 is far from high temperature
One end of alloy pipe 8 is connect with an interface of internal screw thread Stainless steel tee 20 by pipeline, internal screw thread Stainless steel tee 20
Top interface is connect with pressure gauge 4, and internal screw thread Stainless steel tee 20 is connect far from an interface of pipeline with check valve 2, check valve 2
Side be equipped with double card set air inlet needle-valve 1, double card set 1 one end of air inlet needle-valve offer double card set air inlet 19, second
The top of sealing flange 13 is connect by pipeline with pressure safety valve 11 and pressure security needle-valve 12, the bottom of the second sealing flange 13
Portion is connect by pipeline with exhaust valve 14.
The side of metal plate furnace body 16 is fixedly connected with control system switch 18, the model MAM- of control system switch 18
200, the side insertion of control system switch 18 is equipped with temperature control display screen 17, and pressure sensor 5 is electrically connected control system and opens
18 input terminal is closed, the output end of control system switch 18 is electrically connected temperature control display screen 17, high degree of automation, convenient for control
Pressure and temperature is constant；Pressure safety valve 11 and pressure security needle-valve 12 are installed in an angle of 90 degrees, are easy to use.
Working principle of the utility model is: opening the second sealing flange 13 is put into reacting metal sample to response sample boat 9
Position is vacuumized by opening exhaust valve 14, covers air inlet needle-valve 1 by double card and double card covers air inlet 19 and is passed through gas, lead to
It crosses heating furnace 15 and 25-1200 DEG C is heated to high temperature alloy steel pipe 8, pressure reaches 0-80MPa, and firing reaction temperature is 0-
1200 DEG C, air inlet needle-valve 1 and double card set air inlet 19 are covered from double card and is passed through reaction gas by check valve 2,25-1200 DEG C adds
Hot time 0-10000 hours, reaction gas is then cut off, protective gas nitrogen is passed through and is cooled to room temperature, take out sample.
The utility model has the advantages that this equipment prepares the composite material of high quality by the way of high temperature and pressure, using high temperature alloy
Steel pipe 8 is used as closed carrying sample chamber, and both ends are equipped with CF sealing flange as disassembly dress and take sample, pressure sensor 5
It is constant as temperature to be equipped with PID programming temperature control system as guaranteeing that chamber pressure is stable for control system；Sample is placed high
On response sample boat 9 in temperature alloy steel pipe 8, heats and be passed through protective gas to 0-80MPa, while cavity is entered by gas
Interior Pintsch process reaction and the intracorporal metal material of chamber react under high pressure-temperature, prepare the nano composite of high quality
Material；The nano metal material capability and performance reacted at high temperature under high pressure simultaneously is excellent, so that the metal nano for obtaining high quality is multiple
Condensation material；
The device of gas source synthetic reaction under effective solution high temperature and pressure, efficiently solves gas reaction at high temperature under high pressure
Prepare the nano metal composite material of high quality；Solution cannot realize chemical vapor in high temperature and pressure in the prior art
The problem of reaction, provides effective means to prepare the nano metal composite material of high quality.
In the description of this specification, the description of reference term " one embodiment ", " example ", " specific example " etc. means
Particular features, structures, materials, or characteristics described in conjunction with this embodiment or example are contained at least one of the utility model
In embodiment or example.In the present specification, schematic expression of the above terms be not necessarily referring to identical embodiment or
Example.Moreover, particular features, structures, materials, or characteristics described can be in any one or more embodiment or examples
In can be combined in any suitable manner.
Above content is only to examples for clearly illustrating the present invention and explanation, affiliated those skilled in the art couple
Described specific embodiment does various modifications or additions or is substituted in a similar manner, without departing from practical new
Type or beyond the scope defined by this claim, all should belong to the protection range of the utility model.
Claims (3)
1. a kind of automatic high temperature and high pressure gas reaction nano metal composite material prepares furnace, which is characterized in that packed into including double card
Port needle-valve (1), check valve (2), automatic pressure relief valve (3), pressure gauge (4), pressure sensor (5), the first sealing flange (6),
Red copper sealing ring (7), high temperature alloy steel pipe (8), response sample boat (9), water cooling fixed frame (10), pressure safety valve (11), pressure
The safe needle-valve of power (12), the second sealing flange (13), exhaust valve (14), heating furnace (15) and metal plate furnace body (16), the metal plate
The two sides of golden furnace body (16) are symmetrically installed with two water cooling fixed frames (10), and the metal plate furnace body (16) is internally provided with heating furnace
Thorax (15), the high temperature alloy steel pipe (8) run through metal plate furnace body (16) and heating furnace (15), and the high temperature alloy steel pipe
(8) inside is fixedly connected with response sample boat (9), and the both ends of the high temperature alloy steel pipe (8) pass through red copper sealing ring (7)
It is tightly connected respectively with the first sealing flange (6) and the second sealing flange (13), the top of first sealing flange (6) is fixed
It being connected with pressure sensor (5), the bottom of first sealing flange (6) is fixedly connected with automatic pressure relief valve (3), and described first
One interface of sealing flange (6) one end and internal screw thread Stainless steel tee (20) far from high temperature alloy steel pipe (8) is connected by pipeline
It connects, the top interface of the internal screw thread Stainless steel tee (20) is connect with pressure gauge (4), the internal screw thread Stainless steel tee (20)
An interface far from pipeline is connect with check valve (2), and the side of the check valve (2) is equipped with double card set air inlet needle-valve (1),
Double card set air inlet needle-valve (1) one end offers double card set air inlet (19), the top of second sealing flange (13)
It is connect by pipeline with pressure safety valve (11) and pressure security needle-valve (12), the bottom of second sealing flange (13) passes through
Pipeline is connect with exhaust valve (14).
2. a kind of automatic high temperature and high pressure gas reaction nano metal composite material according to claim 1 prepares furnace, special
Sign is that the side of the metal plate furnace body (16) is fixedly connected with control system switch (18), the control system switch (18)
Side insertion be equipped with temperature control display screen (17), the pressure sensor (5) is electrically connected the defeated of control system switch (18)
Enter end, the output end of the control system switch (18) is electrically connected temperature control display screen (17).
3. a kind of automatic high temperature and high pressure gas reaction nano metal composite material according to claim 1 prepares furnace, special
Sign is that the pressure safety valve (11) and pressure security needle-valve (12) are installed in an angle of 90 degrees.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201822216090.4U CN209502964U (en) | 2018-12-27 | 2018-12-27 | A kind of automatic high temperature and high pressure gas reaction nano metal composite material prepares furnace |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201822216090.4U CN209502964U (en) | 2018-12-27 | 2018-12-27 | A kind of automatic high temperature and high pressure gas reaction nano metal composite material prepares furnace |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN209502964U true CN209502964U (en) | 2019-10-18 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201822216090.4U Expired - Fee Related CN209502964U (en) | 2018-12-27 | 2018-12-27 | A kind of automatic high temperature and high pressure gas reaction nano metal composite material prepares furnace |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN209502964U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109570494A (en) * | 2018-12-27 | 2019-04-05 | 合肥百思新材料研究院有限公司 | A kind of automatic high temperature and high pressure gas reaction nano metal composite material prepares furnace |
-
2018
- 2018-12-27 CN CN201822216090.4U patent/CN209502964U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109570494A (en) * | 2018-12-27 | 2019-04-05 | 合肥百思新材料研究院有限公司 | A kind of automatic high temperature and high pressure gas reaction nano metal composite material prepares furnace |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20230116 Address after: 238000 101, Baisi Group office building, northwest corner of the intersection of Heping Avenue and Xiuhu Road, Chaohu Economic Development Zone, Hefei, Anhui Province Patentee after: Hefei Baisi Intelligent Equipment Co.,Ltd. Address before: 238000 northwest corner of the intersection of Heping Avenue and Xiuhu Road, Chaohu Economic Development Zone, Hefei City, Anhui Province Patentee before: HEFEI BAISI NEW MATERIALS RESEARCH INSTITUTE Co.,Ltd. |
|
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20191018 |