CN209500856U - A kind of diaminodiphenyl ether distillation crystallization apparatus - Google Patents
A kind of diaminodiphenyl ether distillation crystallization apparatus Download PDFInfo
- Publication number
- CN209500856U CN209500856U CN201822195015.4U CN201822195015U CN209500856U CN 209500856 U CN209500856 U CN 209500856U CN 201822195015 U CN201822195015 U CN 201822195015U CN 209500856 U CN209500856 U CN 209500856U
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- arc panel
- diaminodiphenyl ether
- heated seats
- outer tube
- rubber sleeve
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Abstract
The utility model discloses a kind of diaminodiphenyl ether distillation crystallization apparatus, including main body, it further include gathering device and support device, the main body includes support frame and heated seats, the gathering device includes rubber sleeve, the rubber sleeve is located at the inside of heated seats, the inner surface of the rubber sleeve is connected with aluminium foil, arc panel is fixedly connected at the top of the rubber sleeve, guide post is respectively connected on the inside of the both ends of the arc panel, one end of the arc panel is connected with adjusting bolt, is connected with fixing bearing one between adjusting bolt and the arc panel；Rubber sleeve etc. is mounted with by design, heat is gathered when may be implemented in use device, it is easy to use personnel intuitively to observe the crystallization progress of evaporative flask simultaneously, solves existing diaminodiphenyl ether distillation crystallization apparatus, since heated seats being sealed using sealing cover, the problem of when using sealing cover, user of service can not intuitively observe the crystallization effect of evaporative flask by sealing cover, may influence crystallization effect.
Description
Technical field
The utility model belongs to crystallization apparatus technical field, and in particular to a kind of diaminodiphenyl ether distillation crystallization apparatus.
Background technique
Diaminodiphenyl ether is a kind of organic chemical, abbreviation ODA, chemical formula C12H12N2O.
Existing diaminodiphenyl ether distillation crystallization apparatus is using sealing due to sealing heated seats using sealing cover
Gai Shi, user of service possibly can not intuitively be observed the crystallization effect of evaporative flask by sealing cover, may influence crystallization effect very
To the problem for leading to evaporative flask breakage, thus it is proposed that a kind of diaminodiphenyl ether distillation crystallization apparatus.
Utility model content
The purpose of this utility model is to provide a kind of diaminodiphenyl ether distillation crystallization apparatus, to solve above-mentioned background skill
Existing diaminodiphenyl ether distillation crystallization apparatus is proposed in art, due to sealing heated seats using sealing cover, is using sealing
Gai Shi, user of service possibly can not intuitively be observed the crystallization effect of evaporative flask by sealing cover, may influence crystallization effect very
To the problem for leading to evaporative flask breakage.
To achieve the above object, the utility model provides the following technical solutions: a kind of diaminodiphenyl ether distillation crystallization dress
It sets, including main body, further includes gathering device and support device, the main body includes support frame and heated seats, the gathering device
Including rubber sleeve, the rubber sleeve is located at the inside of heated seats, and the inner surface of the rubber sleeve is connected with aluminium foil, the rubber sleeve
Top be fixedly connected with arc panel, guide post, one end connection of the arc panel are respectively connected on the inside of the both ends of the arc panel
There is adjusting bolt, is connected with fixing bearing one between adjusting bolt and the arc panel.
Preferably, the support device includes outer tube sleeve, and the outer tube sleeve is located at the side of support frame, the outer tube sleeve
Inner surface is connected with retention bead, and rotation ring is connected with above the outer tube sleeve, is connected between rotation ring and the outer tube sleeve solid
Dead axle holds two, and inner tube set is connected on the inside of the outer tube sleeve, and the top of said inner tube set is fixedly connected with supporting block.
Preferably, the main body further includes test tube and receiving flask and evaporative flask, and the side of support frame as described above is connected with test tube,
The bottom of the test tube is connected with receiving flask, and the side of support frame as described above is connected with heated seats, the inside connection of the heated seats
There is evaporative flask.
Preferably, the inside of the arc panel offers limit hole, and in the guide post and arc panel on the inside of the heated seats
The guide hole of side, which corresponds to each other, to be fixed.
Preferably, anti-skid chequer is offered on the outside of the adjusting bolt, and pass through between adjusting bolt and the arc panel
Fixing bearing one is flexibly connected.
Preferably, the retention bead is an integral structure with outer tube sleeve, and the inner surface and inner tube set of the rotation ring
Outer surface offer screw thread.
Compared with prior art, the utility model has the beneficial effects that
(1) it is mounted with rubber sleeve being located on the inside of heated seats etc., it can be achieved that gathering heat in use device by design
Hold together, convenient for preventing the wasting of resources caused by heat losses, while personnel easy to use intuitively observe the crystallization progress of evaporative flask,
It solves existing diaminodiphenyl ether distillation crystallization apparatus, due to sealing heated seats using sealing cover, is using sealing cover
When, user of service can not intuitively observe the crystallization effect of evaporative flask, the problem of may influencing crystallization effect by sealing cover.
(2) outer tube sleeve etc. being located at below receiving flask is mounted with by design, support can be provided for receiving flask, convenient for increasing
Stability when receiving flask uses solves existing diaminodiphenyl ether distillation crystallization apparatus, due to being not provided with outer tube sleeve
If equal devices cause the connecting portion of test tube and receiving flask burden larger, may cause receiving flask fill with liquid in receiving flask
Loosen the problem of even falling off.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the utility model；
Fig. 2 is the top view of the utility model heated seats；
Fig. 3 is the side view of the utility model rubber sleeve；
Fig. 4 is the side view of the utility model outer tube sleeve.
In figure: 1, test tube；2, receiving flask；3, outer tube sleeve；4, support frame；5, heated seats；6, evaporative flask；7, bolt is adjusted；
8, guide post；9, rubber sleeve；10, arc panel；11, fixing bearing one；12, aluminium foil；13, supporting block；14, inner tube set；15, ring is revolved；
16, fixing bearing two；17, retention bead.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model
Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole
Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work
Every other embodiment obtained, fall within the protection scope of the utility model.
Fig. 1-Fig. 4 is please referred to, the utility model provides a kind of technical solution: a kind of diaminodiphenyl ether distillation crystallization dress
It sets, including main body, further includes gathering device and support device, main body includes support frame 4 and heated seats 5, and gathering device includes rubber
Gum cover 9, rubber sleeve 9 are located at the inside of heated seats 5, and the inner surface of rubber sleeve 9 is connected with aluminium foil 12, and the top of rubber sleeve 9 is fixed
It is connected with arc panel 10, guide post 8 is respectively connected on the inside of the both ends of arc panel 10, one end of arc panel 10, which is connected with, adjusts bolt 7,
It adjusts to be connected together between bolt 7 and arc panel 10 and has fixing bearing 1, be mounted with to be located at 5 inside of heated seats by designing
Rubber sleeves 9 etc. are, it can be achieved that gather heat in use device, convenient for preventing the wasting of resources caused by heat losses, while just
The crystallization progress of evaporative flask 6 is intuitively observed in user of service, solves existing diaminodiphenyl ether distillation crystallization apparatus, by
In being sealed heated seats 5 using sealing cover, when using sealing cover, user of service, which can not intuitively be observed by sealing cover, evaporates
The crystallization effect of bottle 6, the problem of crystallization effect may be influenced.
For the ease of guaranteeing the normal use of support device, in the present embodiment, it is preferred that support device includes outer tube sleeve 3,
Outer tube sleeve 3 is located at the side of support frame 4, and the inner surface of outer tube sleeve 3 is connected with retention bead 17, and the top of outer tube sleeve 3 is connected with
Ring 15 is revolved, revolves and is connected with fixing bearing 2 16 between ring 15 and outer tube sleeve 3, the inside of outer tube sleeve 3 is connected with inner tube set 14, inner tube
The top of set 14 is fixedly connected with supporting block 13, can be to receive by designing the outer tube sleeve 3 etc. for being mounted with to be located at below receiving flask 2
Collect bottle 2 and support is provided, convenient for increasing stability when receiving flask 2 uses, solves existing diaminodiphenyl ether distillation crystallization
If device causes the connection of test tube 1 Yu receiving flask 2 fill with liquid in receiving flask 2 due to being not provided with the devices such as outer tube sleeve 3
Position burden is larger, may cause the problem of receiving flask 2 is loosened or even fallen off.
For the ease of guaranteeing the normal use of main body, in the present embodiment, it is preferred that main body further includes test tube 1 and receiving flask 2
With evaporative flask 6, the side of support frame 4 is connected with test tube 1, and the bottom of test tube 1 is connected with receiving flask 2, the side connection of support frame 4
There are heated seats 5, the inside of heated seats 5 is connected with evaporative flask 6.
For the ease of preventing arc panel 10 from rotating, in the present embodiment, it is preferred that the inside of arc panel 10 offers limit
Hole, and the guide post 8 of 5 inside of heated seats corresponds to each other fixation with the guide hole of 10 inside of arc panel.
Bolt 7 is adjusted for the ease of preferably using, in the present embodiment, it is preferred that the outside of adjusting bolt 7 offers anti-
Sliding line, and adjust and be flexibly connected between bolt 7 and arc panel 10 by fixing bearing 1.
For the ease of adjusting inner tube set 14, in the present embodiment, it is preferred that retention bead 17 is integral type with outer tube sleeve 3
Structure, and the inner surface of rotation ring 15 and the outer surface of inner tube set 14 offer screw thread.
The working principle and process for using of the utility model: the device by the heating wire of 5 inside of heated seats in use, added
Heat can be evaporated purification to the liquid of 6 inside of evaporative flask, when needing to gather heat, screw the adjusting bolt 7 of two sides, by
It is connected with fixing bearing 1 between bolt 7 and arc panel 10 in adjusting, therefore can prevent arc panel 10 from following 7 turns of bolt of adjusting
Dynamic, when screwing adjusting bolt 7 at this time, adjusting bolt 7 can drive rubber sleeve 9 mobile to the center of circle of heated seats 5, the rubber of two sides
9 top of set is gathered inwardly, and the heat that 9 bottom heating wire of rubber sleeve can be made to issue more is concentrated, and needs to support receiving flask 2
When, ring 15 is screwed, the screw thread for revolving 14 outside of screw thread and inner tube set of 15 inner wall of ring interacts, and inner tube set 14 can be made to drive
Supporting block 13 moves up, until contacting with receiving flask 2, provides support for receiving flask 2.
While there has been shown and described that the embodiments of the present invention, for the ordinary skill in the art,
It is understood that these embodiments can be carried out with a variety of variations in the case where not departing from the principles of the present invention and spirit, repaired
Change, replacement and variant, the scope of the utility model is defined by the appended claims and the equivalents thereof.
Claims (6)
- The crystallization apparatus 1. a kind of diaminodiphenyl ether distils, including main body, it is characterised in that: further include gathering device and support dress It sets, the main body includes support frame (4) and heated seats (5), and the gathering device includes rubber sleeve (9), rubber sleeve (9) position Inner surface in the inside of heated seats (5), the rubber sleeve (9) is connected with aluminium foil (12), and the top of the rubber sleeve (9) is fixed It is connected with arc panel (10), is respectively connected with guide post (8) on the inside of the both ends of the arc panel (10), one end of the arc panel (10) It is connected with and adjusts bolt (7), be connected with fixing bearing one (11) between the adjusting bolt (7) and arc panel (10).
- The crystallization apparatus 2. a kind of diaminodiphenyl ether according to claim 1 distils, it is characterised in that: the support device Including outer tube sleeve (3), the outer tube sleeve (3) is located at the side of support frame (4), and the inner surface connection of the outer tube sleeve (3) is limited Position is raised (17), and rotation ring (15) is connected with above the outer tube sleeve (3), is connected between the rotation ring (15) and outer tube sleeve (3) There is fixing bearing two (16), is connected with inner tube set (14) on the inside of the outer tube sleeve (3), the top of said inner tube set (14) is fixed It is connected with supporting block (13).
- The crystallization apparatus 3. a kind of diaminodiphenyl ether according to claim 1 distils, it is characterised in that: the main body is also wrapped Test tube (1) and receiving flask (2) and evaporative flask (6) are included, the side of support frame as described above (4) is connected with test tube (1), the test tube (1) Bottom be connected with receiving flask (2), the side of support frame as described above (4) is connected with heated seats (5), the inside of the heated seats (5) It is connected with evaporative flask (6).
- The crystallization apparatus 4. a kind of diaminodiphenyl ether according to claim 3 distils, it is characterised in that: the arc panel (10) inside offers limit hole, and the guide post (8) on the inside of the heated seats (5) and the guide hole on the inside of arc panel (10) are mutual It is corresponding to fix.
- The crystallization apparatus 5. a kind of diaminodiphenyl ether according to claim 1 distils, it is characterised in that: the adjusting bolt (7) anti-skid chequer is offered on the outside of, and passes through fixing bearing one (11) activity between the adjusting bolt (7) and arc panel (10) Connection.
- The crystallization apparatus 6. a kind of diaminodiphenyl ether according to claim 2 distils, it is characterised in that: the retention bead (17) it is an integral structure with outer tube sleeve (3), and the inner surface of rotation ring (15) and the outer surface of inner tube set (14) are opened Equipped with screw thread.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201822195015.4U CN209500856U (en) | 2018-12-26 | 2018-12-26 | A kind of diaminodiphenyl ether distillation crystallization apparatus |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201822195015.4U CN209500856U (en) | 2018-12-26 | 2018-12-26 | A kind of diaminodiphenyl ether distillation crystallization apparatus |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN209500856U true CN209500856U (en) | 2019-10-18 |
Family
ID=68197199
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201822195015.4U Active CN209500856U (en) | 2018-12-26 | 2018-12-26 | A kind of diaminodiphenyl ether distillation crystallization apparatus |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN209500856U (en) |
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2018
- 2018-12-26 CN CN201822195015.4U patent/CN209500856U/en active Active
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