CN209475629U - A kind of efficient, stable crystalline device - Google Patents

A kind of efficient, stable crystalline device Download PDF

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Publication number
CN209475629U
CN209475629U CN201920132115.4U CN201920132115U CN209475629U CN 209475629 U CN209475629 U CN 209475629U CN 201920132115 U CN201920132115 U CN 201920132115U CN 209475629 U CN209475629 U CN 209475629U
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China
Prior art keywords
ontology
storage bin
chamber
side wall
scraper plate
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CN201920132115.4U
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Chinese (zh)
Inventor
冯树海
耿洪军
赵修全
胡建涛
冯树军
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WEIFANG DAYOU BIOLOGICAL CHEMICAL CO LTD
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WEIFANG DAYOU BIOLOGICAL CHEMICAL CO LTD
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Priority to CN201920132115.4U priority Critical patent/CN209475629U/en
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Abstract

The utility model discloses a kind of efficient, stable crystalline device, including ontology, agitating shaft is provided in the ontology, the agitating shaft is driven by motor and rotated, and is provided with filter in the ontology, the inner cavity of ontology is divided into stir chamber and feed back chamber by the filter;Drain spout is provided on the filter, the drain spout is sector, the drain spout connection stir chamber and feed back chamber;It is provided with storage bin below the drain spout, the storage bin is located at that feed back is intracavitary, and the storage bin includes the two storage bin side walls and storage bin bottom wall being connected.The utility model can achieve efficient, stable crystalline effect;Crystalline particle size is uniform simultaneously, and product quality is high;Sealing effect is good, and after stirred crystallization is completed, fast and easy, exhaustive is discharged in crystalline particle, and can be adjusted according to the needs the discharge rate of particle;Residual on the side wall and bottom wall of crystallizer without feed liquid or little crystallization particle.

Description

A kind of efficient, stable crystalline device
Technical field
The utility model relates to a kind of crystallizers, specifically, are related to a kind of efficient, stable crystalline device, belong to crystallization and set Standby technical field.
Background technique
There are many type of crystallizer, in such a way that solution obtains hypersaturated state, press the type of flow, is more by mode of operation etc. The crystallizer of kind mode.At present it is existing by the way of hypersaturated state in, mostly use stirring feed liquid, feed liquid made to reach saturation State can be crystalline particle precipitation, however, there are more problems for existing crystallizer, for example, the knot that existing crystallizer obtains Brilliant particle diameter is inhomogenous, cannot guarantee the quality of product;Also the crystallizer having cannot rationally control crystalline particle in outlet The discharge rate made, using being inconvenient;Some crystalline rates are low, unstable, are not convenient to use.
In summary, the existing technology has inconveniences and defects in actual use, so it is necessary to be improved.
Utility model content
The technical problems to be solved in the utility model be against the above deficiency, provide it is a kind of efficiently, stable crystalline device, can be with Achieve the effect that efficient, stable crystalline;Crystalline particle size is uniform simultaneously, and product quality is high;Sealing effect is good, works as stirred crystallization After completion, fast and easy, exhaustive is discharged in crystalline particle, and can be adjusted according to the needs the discharge rate of particle;Crystallizer Residual on side wall and bottom wall without feed liquid or little crystallization particle.
In order to solve the above technical problems, the utility model uses following technical scheme: a kind of efficient, stable crystalline device, packet Include ontology, be provided with agitating shaft in the ontology, the agitating shaft is driven by motor and is rotated, be provided in the ontology every The inner cavity of ontology is divided into stir chamber and feed back chamber by net, the filter;
Drain spout is provided on the filter, the drain spout is sector, the drain spout connection stir chamber and feed back chamber; It is provided with storage bin below the drain spout, the storage bin is located at that feed back is intracavitary, and the storage bin includes two and is connected Storage bin side wall and storage bin bottom wall are provided with several positive six sides on the two storage bin side walls and storage bin bottom wall being connected Shape through-hole, the storage bin bottom wall tilt down setting, and the included angle B between the storage bin bottom wall and storage bin side wall is 110°;Included angle A between the storage bin bottom wall and the side wall of ontology is 70 °, is provided with crystallization below the side wall of the ontology Discharge port, the storage bin are connected to crystallization discharge port;
The bottom of the agitating shaft is provided with feed back chamber scraper plate, and it is intracavitary that the feed back chamber scraper plate is located at feed back, the stirring It is additionally provided with stir chamber scraper plate on axis, the stir chamber scraper plate is located at the bottom of stir chamber, and the stir chamber scraper plate is close to filter It is arranged, side wall scraper plate is provided on the stir chamber scraper plate, the side wall of the side wall scraper plate close to ontology is arranged, and the side wall is scraped Multiple rotatable stirring blades are provided between plate and agitating shaft;
Be provided with baffle chamber on the side wall of the ontology of the crystallization discharge outlet, the baffle is intracavitary be provided with can on move down The radian of dynamic discharge port baffle, the discharge port baffle is identical as the radian of ontology.
A kind of prioritization scheme, the crystallization discharge port are connected with crystallization discharge nozzle, are provided with band on the crystallization discharge nozzle The through-hole of internal screw thread is provided with bolt in the through-hole, and external screw thread is provided on the bolt and is matched with the internal screw thread of through-hole It closes.
Further, the bottom of bolt is provided with spherical link block, is provided with connecting rod in the crystallization discharge nozzle, described One end of connecting rod is fixedly connected with the lower part of discharge port baffle and the other end is provided with spherical accommodating chamber, and the spherical shape accommodating chamber is same In the spherical link block of splendid attire.
Further, multiple roller balls are additionally provided in the spherical accommodating chamber, the roller ball is located at spherical link block Between the inner wall of spherical accommodating chamber.
Further, sealing ring is provided with above the spherical link block.
Further, gasket is set on the side wall of the baffle chamber.
Further, one end connection agitating shaft of the feed back chamber scraper plate and the matching of the bottom wall shape of the other end and ontology It closes.
Further, the bottom of the ontology is provided with feed liquid circulation outlet, is provided with feed liquid at the top of the ontology and follows Ring import, feed inlet, the feed liquid circulation export and are provided with circulating line between feed liquid circulation import, on the circulating line It is provided with product pump.
Further, the stirring blade includes the first blade and the second blade, between second blade of the first blade Angle be 150 °.
Further, the upper edge of second blade and the first blade is arcuate structure.
The utility model after the above technical solution is adopted, compared with prior art, has the advantage that
The crystallizer of the utility model can achieve efficient, stable crystalline effect;Crystalline particle size is uniform simultaneously, Product quality is high;Sealing effect is good, after stirred crystallization is completed, crystalline particle discharge fast and easy, and exhaustive, and can root According to the discharge rate for needing to adjust particle;Residual on the side wall and bottom wall of crystallizer without feed liquid or little crystallization particle.
The utility model is described in detail with reference to the accompanying drawings and examples.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the utility model crystallizer;
Fig. 2 is the structural schematic diagram of filter;
Fig. 3 is the structural schematic diagram of storage bin side wall;
Fig. 4 is the structural schematic diagram of storage bin;
Fig. 5 is the structural schematic diagram that discharge port baffle moves up;
Fig. 6 is the structural schematic diagram that discharge port baffle moves down;
Fig. 7 is the attachment structure schematic diagram of connecting rod and bolt;
Fig. 8 is the structural schematic diagram of stirring blade;
In figure,
1- ontology, 2- agitating shaft, 3- motor, 4- feed back chamber scraper plate, 5- feed back chamber, 6- storage bin, 7- filter, 8- stirring Chamber, the outlet of 9- feed liquid circulation, 10- feed liquid circulation import, 11- circulating line, 12- product pump, 13- feed inlet, 14- paddle Piece, the first blade of 15-, the second blade of 16-, 17- storage bin bottom wall, 18- drain spout, 19- storage bin side wall, 20- crystallization discharging Mouthful, 21- baffle chamber, 22- discharge port baffle, 23- connecting rod, 24- bolt, 25- spherical shape link block, 26- spherical shape accommodating chamber, 27- Roller ball, 28- sealing ring, 29- gasket, 30- stirring scratch board, 31- side wall scraper plate.
Specific embodiment
For a clearer understanding of the technical features, objectives and effects of the utility model, now compareing Detailed description of the invention Specific embodiment of the present utility model.
A kind of efficient, the stable crystalline device of embodiment 1
As shown in figures 1-8, the utility model provide it is a kind of efficiently, stable crystalline device include ontology 1, set in the ontology 1 It is equipped with agitating shaft 2, the agitating shaft 2 drives rotation by motor 3.
Filter 7 is provided in the ontology 1, the inner cavity of ontology 1 is divided into stir chamber 8 and feed back chamber 5 by the filter 7.
Drain spout 18 is provided on the filter 7, the drain spout 18 is sector, and the drain spout 18 is connected to stir chamber 8 With feed back chamber 5.
Storage bin 6 is provided with below the drain spout 18, the storage bin 6 is located in feed back chamber 5.
The storage bin 6 includes the two storage bin side walls 19 and storage bin bottom wall 17 being connected.Two storages being connected Be provided with several regular hexagon through-holes on feed bin side wall 19 and storage bin bottom wall 17, through-hole for filter feed liquid and not up at The little particle of product crystalline particle diameter.
The storage bin bottom wall 17 tilts down setting, the angle between the storage bin bottom wall 17 and storage bin side wall 19 B is 110 °;Included angle A between the storage bin bottom wall 17 and the side wall of ontology 1 is 70 °.
Crystallization discharge port 20 is provided with below the side wall of the ontology 1, the storage bin 6 is connected to crystallization discharge port 20.
It is provided with baffle chamber 21 on the side wall of ontology 1 at the crystallization discharge port 20, is provided in the baffle chamber 21 The radian of discharge port baffle 22 moving up and down, the discharge port baffle 22 is identical as the radian of ontology 1.
The crystallization discharge port 20 is connected with crystallization discharge nozzle, is provided on the crystallization discharge nozzle tapped logical Hole is provided with bolt 24 in the through-hole, and the bottom of bolt 24 is provided with spherical link block 25, is provided on the bolt 24 outer It screw thread and is matched with the internal screw thread of through-hole.
Connecting rod 23 is provided in the crystallization discharge nozzle, one end of the connecting rod 23 is fixedly connected with discharge port baffle 22 Lower part and the other end be provided with spherical accommodating chamber 26, the spherical shape accommodating chamber 26 is same as containing spherical link block 25, the ball Multiple roller balls 27 are additionally provided in shape accommodating chamber 26, the roller ball 27 is located at spherical link block 25 and spherical accommodating chamber 26 Between inner wall.
The top of the spherical shape link block 25 is provided with sealing ring 28, can be to avoid feed liquid or not up to finished product crystallization The little particle of grain diameter enters spherical accommodating chamber 26.
When rotating bolt 24, spherical link block 25 is rotated while being driven in spherical accommodating chamber 26 and moved down in connecting rod 23 It is dynamic, and then discharge port baffle 22 is driven to move up and down, turn on or off crystallization discharge port 20.
Gasket 29 can be arranged in leakproofness in order to further increase on the side wall of baffle chamber 21.Avoid feed liquid Or the little particle of not up to finished product crystalline particle diameter enters baffle chamber 21.
The bottom of the ontology 1 is provided with feed liquid circulation outlet 9, and the top of the ontology 1 is provided with feed liquid circulation import 10, feed inlet 13 are provided with circulating line 11, the circulation pipe between the feed liquid circulation outlet 9 and feed liquid circulation import 10 Product pump 12 is provided on road 11.
The bottom of the agitating shaft 2 is provided with feed back chamber scraper plate 4, and the feed back chamber scraper plate 4 is located in feed back chamber 5, described One end connection agitating shaft 2 and the other end of feed back chamber scraper plate 4 are matched with the bottom wall shape of ontology 1, are same as the bottom wall of ontology 1 On feed liquid or not up to finished product crystalline particle diameter little particle scrape and drive into feed liquid circulation outlet 9, to In the stir chamber 8 for being again introduced into ontology 1 after into circulating line 11, product pump 12, feed liquid circulation import 10.
Stir chamber scraper plate 30 is additionally provided on the agitating shaft 2, the stir chamber scraper plate 30 is located at the bottom of stir chamber 8, The stir chamber scraper plate 30 is arranged close to filter 7, for by feed liquid or the little particle of not up to finished product crystalline particle diameter from It is scraped on filter 7, is also used to be up in the bulky grain push-in storage bin 6 of finished product crystalline particle diameter.
Side wall scraper plate 31 is provided on the stir chamber scraper plate 30, the side wall of the side wall scraper plate 31 close to ontology 1 is arranged, Multiple rotatable stirring blades 14 are provided between the side wall scraper plate 31 and agitating shaft 2.Side wall scraper plate 31 can scrape this The little particle of feed liquid or not up to finished product crystalline particle diameter on the side wall of body 1, avoids cohering.
The stirring blade 14 includes the first blade 15 and the second blade 16, between 15 second blade 16 of the first blade Angle be 150 °.
The upper edge of first blade 15 and the second blade 16 is arcuate structure.When motor 3 drives agitating shaft 2 to rotate When, stirring blade 14 rotates and feed liquid is driven to rotate, and accelerates feed liquid crystallization.
The utility model uses feed liquid circulation formula, can achieve efficient, stable crystalline effect;Crystalline particle size simultaneously Uniform, product quality is high;Sealing effect is good, after stirred crystallization is completed, crystalline particle discharge fast and easy, and exhaustive, and It can be adjusted according to the needs the discharge rate of particle;Residual on the side wall and bottom wall of crystallizer without feed liquid or little crystallization particle.
The above is the citing of the utility model preferred forms, wherein the part that do not address in detail is this field The common knowledge of those of ordinary skill.The protection scope of the utility model is based on the contents of the claims, any to be based on this reality The equivalent transformation carried out with novel technical inspiration, is also within the protection scope of the utility model.

Claims (10)

1. a kind of efficient, stable crystalline device, it is characterised in that: including ontology (1), is provided with agitating shaft in the ontology (1) (2), the agitating shaft (2) drives rotation by motor (3), is provided with filter (7) in the ontology (1), and the filter (7) will The inner cavity of ontology (1) is divided into stir chamber (8) and feed back chamber (5);
It is provided with drain spout (18) on the filter (7), the drain spout (18) is sector, drain spout (18) the connection stirring Chamber (8) and feed back chamber (5);It is provided with storage bin (6) below the drain spout (18), the storage bin (6) is located at feed back chamber (5) Interior, the storage bin (6) includes the two storage bin side walls (19) and storage bin bottom wall (17) being connected, two storages being connected Several regular hexagon through-holes are provided on feed bin side wall (19) and storage bin bottom wall (17), the storage bin bottom wall (17) is downward It is obliquely installed, the included angle B between the storage bin bottom wall (17) and storage bin side wall (19) is 110 °;The storage bin bottom wall (17) included angle A between the side wall of ontology (1) is 70 °, is provided with crystallization discharge port below the side wall of the ontology (1) (20), the storage bin (6) is connected to crystallization discharge port (20);
The bottom of the agitating shaft (2) is provided with feed back chamber scraper plate (4), and the feed back chamber scraper plate (4) is located in feed back chamber (5), It being additionally provided with stir chamber scraper plate (30) on the agitating shaft (2), the stir chamber scraper plate (30) is located at the bottom of stir chamber (8), The stir chamber scraper plate (30) is arranged close to filter (7), is provided with side wall scraper plate (31) on the stir chamber scraper plate (30), described Side wall scraper plate (31) close to ontology (1) side wall be arranged, be provided between the side wall scraper plate (31) and agitating shaft (2) it is multiple can The stirring blade (14) of rotation;
It is provided with baffle chamber (21) on the side wall of ontology (1) at crystallization discharge port (20), is set in the baffle chamber (21) It is equipped with discharge port baffle (22) moving up and down, the radian of the discharge port baffle (22) is identical as the radian of ontology (1).
2. a kind of efficient, stable crystalline device as described in claim 1, it is characterised in that: crystallization discharge port (20) connection There is crystallization discharge nozzle, is provided with tapped through-hole on the crystallization discharge nozzle, bolt (24), institute are provided in the through-hole It states and is provided with external screw thread on bolt (24) and is matched with the internal screw thread of through-hole.
3. a kind of efficient, stable crystalline device as claimed in claim 2, it is characterised in that: the bottom of bolt (24) is provided with ball Shape link block (25) is provided with connecting rod (23) in the crystallization discharge nozzle, and one end of the connecting rod (23) is fixedly connected out The lower part of material mouth baffle (22) and the other end is provided with spherical accommodating chamber (26), the spherical shape accommodating chamber (26) is same as containing spherical Link block (25).
4. a kind of efficient, stable crystalline device as claimed in claim 3, it is characterised in that: in the spherical shape accommodating chamber (26) also Be provided with multiple roller balls (27), the roller ball (27) be located at spherical link block (25) and spherical shape accommodating chamber (26) inner wall it Between.
5. it is as claimed in claim 3 a kind of efficiently, stable crystalline device, it is characterised in that: the spherical shape link block (25) it is upper Side is provided with sealing ring (28).
6. a kind of efficient, stable crystalline device as described in claim 1, it is characterised in that: on the side wall of the baffle chamber (21) It is arranged gasket (29).
7. a kind of efficient, stable crystalline device as described in claim 1, it is characterised in that: one end of the feed back chamber scraper plate (4) It connects agitating shaft (2) and the other end is matched with the bottom wall shape of ontology (1).
8. a kind of efficient, stable crystalline device as described in claim 1, it is characterised in that: the bottom of the ontology (1) is provided with Feed liquid circulation exports (9), is provided with feed liquid circulation import (10), feed inlet (13) at the top of the ontology (1), the feed liquid is followed It is provided with circulating line (11) between ring outlet (9) and feed liquid circulation import (10), is provided with object on the circulating line (11) Material pump (12).
9. it is as described in claim 1 a kind of efficiently, stable crystalline device, it is characterised in that: the stirring blade (14) includes the One blade (15) and the second blade (16), the angle between (15) second blade (16) of the first blade is 150 °.
10. a kind of efficient, stable crystalline device as claimed in claim 9, it is characterised in that: second blade (16) and first The upper edge of blade (15) is arcuate structure.
CN201920132115.4U 2019-01-25 2019-01-25 A kind of efficient, stable crystalline device Active CN209475629U (en)

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CN201920132115.4U CN209475629U (en) 2019-01-25 2019-01-25 A kind of efficient, stable crystalline device

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Application Number Priority Date Filing Date Title
CN201920132115.4U CN209475629U (en) 2019-01-25 2019-01-25 A kind of efficient, stable crystalline device

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112569628A (en) * 2020-12-09 2021-03-30 湖北富奕达电子科技有限公司 Crystallization reaction kettle for aluminum dihydrogen phosphate directly outputting internally crystallized particles

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112569628A (en) * 2020-12-09 2021-03-30 湖北富奕达电子科技有限公司 Crystallization reaction kettle for aluminum dihydrogen phosphate directly outputting internally crystallized particles

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