CN209466173U - A kind of hydrothermal synthesis reaction kettle handler - Google Patents

A kind of hydrothermal synthesis reaction kettle handler Download PDF

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Publication number
CN209466173U
CN209466173U CN201920112280.3U CN201920112280U CN209466173U CN 209466173 U CN209466173 U CN 209466173U CN 201920112280 U CN201920112280 U CN 201920112280U CN 209466173 U CN209466173 U CN 209466173U
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China
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reaction kettle
removable disk
hydrothermal synthesis
synthesis reaction
bearing
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CN201920112280.3U
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Chinese (zh)
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于跃
卜志杰
陈军伟
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Rizhao Zhongbang Electronic Co Ltd
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Rizhao Zhongbang Electronic Co Ltd
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Abstract

The utility model discloses a kind of hydrothermal synthesis reaction kettle handlers, including bracket, it is equipped with workbench on the bracket, removable disk is equipped on workbench, it is equipped with handling hole on the upper surface of the removable disk, bearing is equipped on the excircle of the removable disk, is equipped with bearing block on the working platform, it is fixedly connected with automatic rotating device in the bottom of the removable disk, is equipped in the lower section of the bracket and tramples bar.The utility model structure is simple, easy to use, can solve the problem of hydrothermal synthesis reaction kettle disassembling operations difficulty;The outer surface of reaction kettle is protected to be not damaged during dismounting equipped with elastic silica gel gasket;It is equipped with automatic rotating device in the lower section of removable disk, can uniformly be acted on power on reaction kettle, so that the outer surface uniform force of reaction kettle, will not damage screw thread, save trouble and labor is high-efficient;It with small portable, does not take up space and cheap, and can flexibly install, advantage easy to use.

Description

A kind of hydrothermal synthesis reaction kettle handler
Technical field
The utility model relates to a kind of handlers, more particularly, to a kind of hydrothermal synthesis reaction kettle handler.
Background technique
Hydrothermal synthesis reaction kettle is also known as polymerization reaction kettle, high-pressure digestion tank, hydrothermal reaction kettle, Pressure solution bullet, digester etc., It is using strong acid in tank body or highly basic and high temperature high pressure enclosed environment achievees the purpose that rapid-digestion indissoluble substance.Outer tank by Stainless steel is process, and the polytetrafluoroethylene (PTFE) Raw material processing of Lining Selection naivety forms.Hydrothermal reaction kettle is in certain temperature, pressure It selects suitable solvent solution as reaction system under the conditions of power, makes those in atmospheric conditions using the solvent solution of high temperature and pressure Under the dissolution of insoluble or indissoluble substance, or reaction generates the dissolved product of the substance, and the temperature official post by controlling solution occurs Convection current separates grown crystal to form hypersaturated state.It can be used for preparation, compound synthesis, the crystal growth etc. of nano material Aspect also can be used in low dose of anabolic reaction, be the extremely common small-sized reaction kettle of colleges and universities.Main working process is that indissoluble is mixed It closes substance to put within the liner, after liner is placed in hydrothermal synthesis reaction kettle, hydrothermal synthesis reaction kettle is placed in homogeneous reactor, is pressed It is warming up to required reaction temperature according to defined heating rate, carries out heating dissolution.
In scientific experiment, it is often necessary to use container of the various reaction kettles as chemical reaction.Reaction kettle is a kind of close The container closed can be made of materials such as glass, metal or enamel, have the function such as sealing, pressure-bearing, heating, cooling, stirring, ventilation Can, required reaction environment is provided for chemical reaction.And common reaction kettle mainly has glass reaction kettle, hydro-thermal to close in laboratory At reaction kettle and various miniature or miniature high pressure reaction still etc..Since most of reaction kettle is pressure-bearing or vacuum equipment, dissolution Hydrothermal synthesis reaction kettle sealing thermal insulation is needed in the process, so reaction kettle opening will tighten, and to be twisted after the completion of dissolving by heating It opens.In order to realize sealing and can dismantle repeatedly, flange arrangement is generallyd use between autoclave body and kettle cover or helicitic texture is connected It connects, in order to guarantee leakproofness and intensity, generally requires biggish torque and tighten each bolt, also need after the completion of reaction larger Torque dismantle each bolt.When usual each reaction kettle manufacturer design, user is needed to provide the fixtures such as bench vice for oneself for reaction kettle It is fixed, play the role of by means of power, to be dismantled repeatedly when user-friendly.However for many chemical laboratories, It is limited by conditions such as spaces, in laboratory, installation is heavy, take up space and inaesthetic bench vice is often unrealistic;And every time When operation is tightened and unscrewed, it will operate and be lot more time to tighten and unscrew, waste time, working efficiency is low.
Summary of the invention
In order to overcome the above-mentioned deficiencies of the prior art, the utility model provides a kind of hydrothermal synthesis reaction kettle handling dress It sets, the utility model adopts the following technical solutions: a kind of hydrothermal synthesis reaction kettle handler, including bracket, in the branch Frame is equipped with workbench, is equipped with removable disk on the working platform, and handling hole is equipped on the upper surface of the removable disk, Main fixed reactor bottom, realizes reaction kettle quick despatch, bearing is equipped on the excircle of the removable disk, in the work Make platform and be equipped with the bearing block to match with the bearing, the outer ring of bearing and bearing block are fixed on workbench, bearing Inner ring rotated together with removable disk, automatic rotating device is fixedly connected in the bottom of the removable disk, by rotating automatically The rotation of device carrys out band dynamic bearing and removable disk rotates, to drive the lower rotation of reaction kettle, Lai Shixian reaction kettle is tightened With unscrew, the screw thread uniform force on such reaction kettle, will not be caused because of artificial rotation screw thread it is firmly uneven, to damage The case where screw thread, occurs, and is equipped in the lower section of the bracket and tramples bar, and during handling, staff slams that trample bar auxiliary Help fixed reaction kettle.
Preferably, it is equipped with elastomeric pad on the side wall of the handling hole, the outer surface of such reaction kettle and handling hole Side wall does not need directly to contact, and the rotary force of automatic rotating device can uniformly be transmitted to the outer of reaction kettle by elastomeric pad On surface, the side wall of the outer surface and handling hole that avoid reaction kettle directly contacts generation and rubs, the outer surface of injury response kettle, To influence the service life of reaction kettle, while the rotary force of automatic rotating device can be uniformly transmitted to the outer of reaction kettle On surface, it ensure that the screw thread of reaction kettle is not damaged.
Preferably, the elastomeric pad be silicagel pad, silicagel pad have silica gel characteristic, have certain tension, flexibility, Excellent insulating properties, pressure resistance, high temperature resistant is low temperature resistant, and chemical property stabilization, Environmental Safety, free from extraneous odour, food grade silicone pad have Non-toxic and tasteless, not soluble in water and any solvent is a kind of green product of high activity, can preferably protect reaction kettle in this way, Unnecessary damage or damage will not be generated.
Preferably, the automatic rotating device is rotating electric machine, is rotated by rotating electric machine and drives handling disc spins, thus Realize the installation and removal of reaction kettle, rotating electric machine is the rotating electromagnetic machinery for relying on electromagnetic induction principle and running, for real The mutual conversion of existing mechanical energy and electric energy being screwed and being unscrewed using the screw thread of rotating electric machine control reaction kettle, uniform force, no The screw thread of meeting injury response kettle, guarantees the service life of reaction kettle.
Preferably, the rotating electric machine is positive reverse rotation motor, and in this way when installation, rotating electric machine is rotated forward, will Screw thread on reaction kettle screws, and when disassembly, the screw thread on reaction kettle is unscrewed, installed in this way by rotating electric machine reversion Or when disassembly, it is only necessary to by the basis rest to handling hole of reaction kettle, then by the rotating forward of lower rotating electrical machine or Reversal switch, it is simple and convenient, it operates well not easy to make mistakes.
It is further preferred that the handling hole is adjustable type handling hole, it is equipped in the handling hole convenient for adjusting handling The adjusting block of pore size is equipped with groove on the two sidewalls of the removable disk, and the both ends of the adjusting block are slided in the groove It is dynamic, the installing and dismounting work of the reaction kettle of sizes can be met simultaneously in this way, replace different dresses again without staff Disk is unloaded, the working time is saved, improves working efficiency, elastomeric pad is equipped on the inner sidewall of the adjusting block, it in this way can be more The outer surface for protecting reaction kettle well, when disassembly or installation, the outer surface of handling hole and reaction kettle will not be because of direct Contact generates friction, and the outer surface of reaction kettle will not generate unnecessary damage or damage, set on the outside of the adjusting block There is the fastening screw of secured adjusted block, after adjusting block is slided into suitable position, fixed adjusting block by fastening screw, Move it no longer.
Compared with prior art, the utility model has the beneficial effects that 1, the utility model structure is simple, it is easy to use, It can solve the problem of the disassembling operations difficulty of hydrothermal synthesis reaction kettle;2, it is protected during dismounting equipped with elastic silica gel gasket The outer surface of shield reaction kettle is not damaged or damages;3, it is equipped with automatic rotating device in the lower section of removable disk, it can be uniform Power is acted on reaction kettle so that the outer surface uniform force of reaction kettle, will not damage screw thread, save trouble and labor is high-efficient; 4, there is small portable, do not take up space and cheap, and can flexibly install, advantage easy to use.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the utility model.
Fig. 2 is the top view of the utility model.
Fig. 3 is the cross-sectional view of the workbench of the utility model.
Fig. 4 is the top view of the removable disk of the utility model.
Fig. 5 is the cross-sectional view of the removable disk of the utility model.
Wherein: 1. brackets, 2. workbenches, 3. trample bar, 4. removable disks, 5. handling holes, 6. automatic rotating devices, 7. axis It holds, 8. bearing blocks, 9. elastomeric pads, 10. adjusting blocks, 11. grooves, 12. fastening screws.
Specific embodiment
The utility model is further described below by non-limiting embodiment and in conjunction with attached drawing:
1-3 gives the first embodiment of the utility model in figure: a kind of hydrothermal synthesis reaction kettle handler, packet Bracket 1 is included, workbench 2 is equipped on the bracket 1, removable disk 4 is equipped on the workbench 2, in the removable disk 4 Upper surface be equipped with handling hole 5, mainly fix reactor bottom, realize reaction kettle quick despatch, in the outer of the removable disk 4 Circumference is equipped with bearing 7, is equipped with the bearing block 8 that matches with the bearing 7 on the workbench 2, the outer ring of bearing 7 and Bearing block 8 is fixed on workbench 2, and inner ring and the removable disk 4 of bearing 7 rotate together, and is fixed in the bottom of the removable disk 4 It is connected with automatic rotating device 6, is rotated by the rotation of automatic rotating device 6 come band dynamic bearing 7 and removable disk 5, to drive The lower rotation of reaction kettle, Lai Shixian reaction kettle are tightened and are unscrewed, the screw thread uniform force on such reaction kettle, will not be because of Artificial rotation screw thread causes firmly unevenly, so that the case where damaging screw thread generation, is equipped in the lower section of the bracket 1 and tramples bar 3, during handling, staff, which slams, to trample bar 3 reaction kettle is auxiliarily fixed.
Elastomeric pad 9, the outer surface of such reaction kettle and the side wall of handling hole 5 are equipped on the side wall of the handling hole 5 It does not need directly to contact, the rotary force of automatic rotating device 6 can uniformly be transmitted to the appearance of reaction kettle by elastomeric pad 9 On face, the side wall of the outer surface and handling hole 5 that avoid reaction kettle directly contacts generation and rubs, the outer surface of injury response kettle, To influence the service life of reaction kettle, while the rotary force of automatic rotating device 6 can be uniformly transmitted to reaction kettle On outer surface, it ensure that the screw thread of reaction kettle is not damaged.
The elastomeric pad 9 is silicagel pad, and silicagel pad has the characteristic of silica gel, there is certain tension, flexibility, excellent Insulating properties, pressure resistance, high temperature resistant is low temperature resistant, chemical property stabilization, Environmental Safety, free from extraneous odour, and food grade silicone pad has nontoxic nothing Taste, not soluble in water and any solvent are a kind of green products of high activity, can preferably protect reaction kettle in this way, will not produce Raw unnecessary damage or damage.
The automatic rotating device 6 is rotating electric machine, is rotated by rotating electric machine and removable disk 4 is driven to rotate, to realize The installation and removal of reaction kettle, rotating electric machine is the rotating electromagnetic machinery for relying on electromagnetic induction principle and running, for realizing machine Tool can control screwing and unscrewing for the screw thread of reaction kettle using rotating electric machine, uniform force will not damage with the mutual conversion of electric energy The screw thread of traumatic response kettle guarantees the service life of reaction kettle.
The rotating electric machine is positive reverse rotation motor, and in this way when installation, rotating electric machine is rotated forward, will be on reaction kettle Screw thread screw, disassembly when, rotating electric machine reversion, the screw thread on reaction kettle is unscrewed, in this way install or dismantle When, it is only necessary to it in the basis rest of reaction kettle to handling hole 5, will then press rotating forward or the reversal switch of lower rotating electrical machine , it is simple and convenient, it operates well not easy to make mistakes.
1-5 gives second of embodiment of the utility model in figure: a kind of hydrothermal synthesis reaction kettle handler, packet Bracket 1 is included, workbench 2 is equipped on the bracket 1, removable disk 4 is equipped on the workbench 2, in the removable disk 4 Upper surface be equipped with handling hole 5, mainly fix reactor bottom, realize reaction kettle quick despatch, in the outer of the removable disk 4 Circumference is equipped with bearing 7, is equipped with the bearing block 8 that matches with the bearing 7 on the workbench 2, the outer ring of bearing 7 and Bearing block 8 is fixed on workbench 2, and inner ring and the removable disk 4 of bearing 7 rotate together, and is fixed in the bottom of the removable disk 4 It is connected with automatic rotating device 6, is rotated by the rotation of automatic rotating device 6 come band dynamic bearing 7 and removable disk 5, to drive The lower rotation of reaction kettle, Lai Shixian reaction kettle are tightened and are unscrewed, the screw thread uniform force on such reaction kettle, will not be because of Artificial rotation screw thread causes firmly unevenly, so that the case where damaging screw thread generation, is equipped in the lower section of the bracket 1 and tramples bar 3, during handling, staff, which slams, to trample bar 3 reaction kettle is auxiliarily fixed.
Elastomeric pad 9, the outer surface of such reaction kettle and the side wall of handling hole 5 are equipped on the side wall of the handling hole 5 It does not need directly to contact, the rotary force of automatic rotating device 6 can uniformly be transmitted to the appearance of reaction kettle by elastomeric pad 9 On face, the side wall of the outer surface and handling hole 5 that avoid reaction kettle directly contacts generation and rubs, the outer surface of injury response kettle, To influence the service life of reaction kettle, while the rotary force of automatic rotating device 6 can be uniformly transmitted to reaction kettle On outer surface, it ensure that the screw thread of reaction kettle is not damaged.
The elastomeric pad 9 is silicagel pad, and silicagel pad has the characteristic of silica gel, there is certain tension, flexibility, excellent Insulating properties, pressure resistance, high temperature resistant is low temperature resistant, chemical property stabilization, Environmental Safety, free from extraneous odour, and food grade silicone pad has nontoxic nothing Taste, not soluble in water and any solvent are a kind of green products of high activity, can preferably protect reaction kettle in this way, will not produce Raw unnecessary damage or damage.
The automatic rotating device 6 is rotating electric machine, is rotated by rotating electric machine and removable disk 4 is driven to rotate, to realize The installation and removal of reaction kettle, rotating electric machine is the rotating electromagnetic machinery for relying on electromagnetic induction principle and running, for realizing machine Tool can control screwing and unscrewing for the screw thread of reaction kettle using rotating electric machine, uniform force will not damage with the mutual conversion of electric energy The screw thread of traumatic response kettle guarantees the service life of reaction kettle.
The rotating electric machine is positive reverse rotation motor, and in this way when installation, rotating electric machine is rotated forward, will be on reaction kettle Screw thread screw, disassembly when, rotating electric machine reversion, the screw thread on reaction kettle is unscrewed, in this way install or dismantle When, it is only necessary to it in the basis rest of reaction kettle to handling hole 5, will then press rotating forward or the reversal switch of lower rotating electrical machine , it is simple and convenient, it operates well not easy to make mistakes.
The handling hole 5 is adjustable type handling hole, is equipped in the handling hole 5 convenient for adjusting the tune of 5 size of handling hole Locking nub 10, is equipped with groove 11 on the two sidewalls of the removable disk 4, and the both ends of the adjusting block 10 are sliding in the groove 11 It is dynamic, the installing and dismounting work of the reaction kettle of sizes can be met simultaneously in this way, replace different dresses again without staff Disk 4 is unloaded, the working time is saved, improves working efficiency, elastomeric pad 9 is equipped on the inner sidewall of the adjusting block 10, in this way may be used Preferably to protect the outer surface of reaction kettle, when disassembly or installation, the outer surface of handling hole 5 and reaction kettle will not be because of Directly contact generates friction, and the outer surface of reaction kettle will not generate unnecessary damage or damage, in the adjusting block 10 The fastening screw 12 that outside is equipped with secured adjusted block 10 passes through fastening screw after adjusting block 10 is slided into suitable position 12 is fixed by adjusting block 10, moves it no longer.
Above-described embodiment elaborates the utility model.Certainly, above description is not the limit to the utility model System, the utility model are also not limited to above-mentioned example, and related technical personnel are made in the essential scope of the utility model Variation, remodeling, addition are reduced, replacement, also belong to the protection scope of the utility model.

Claims (6)

1. a kind of hydrothermal synthesis reaction kettle handler, it is characterised in that: flat equipped with work on the bracket including bracket Platform is equipped with removable disk on the working platform, handling hole is equipped on the upper surface of the removable disk, in the removable disk Excircle is equipped with bearing, the bearing block to match with the bearing is equipped on the working platform, in the removable disk Bottom is fixedly connected with automatic rotating device, is equipped in the lower section of the bracket and tramples bar.
2. hydrothermal synthesis reaction kettle handler according to claim 1, it is characterised in that: in the side wall of the handling hole It is equipped with elastomeric pad.
3. hydrothermal synthesis reaction kettle handler according to claim 2, it is characterised in that: the elastomeric pad is silica gel Pad.
4. hydrothermal synthesis reaction kettle handler according to claim 1, it is characterised in that: the automatic rotating device is Rotating electric machine.
5. hydrothermal synthesis reaction kettle handler according to claim 4, it is characterised in that: the rotating electric machine is positive and negative Rotate rotating motor.
6. hydrothermal synthesis reaction kettle handler according to claim 1, it is characterised in that: the handling hole is adjustable type Handling hole is equipped with convenient for adjusting the adjusting block of handling pore size in the handling hole, sets on the two sidewalls of the removable disk Fluted, the both ends of the adjusting block are slided in the groove, and elastomeric pad is equipped on the inner sidewall of the adjusting block, The outside of the adjusting block is equipped with the fastening screw of secured adjusted block.
CN201920112280.3U 2019-01-23 2019-01-23 A kind of hydrothermal synthesis reaction kettle handler Active CN209466173U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201920112280.3U CN209466173U (en) 2019-01-23 2019-01-23 A kind of hydrothermal synthesis reaction kettle handler

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201920112280.3U CN209466173U (en) 2019-01-23 2019-01-23 A kind of hydrothermal synthesis reaction kettle handler

Publications (1)

Publication Number Publication Date
CN209466173U true CN209466173U (en) 2019-10-08

Family

ID=68092472

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201920112280.3U Active CN209466173U (en) 2019-01-23 2019-01-23 A kind of hydrothermal synthesis reaction kettle handler

Country Status (1)

Country Link
CN (1) CN209466173U (en)

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