CN209393178U - New reactor for heterogeneous reaction system - Google Patents

New reactor for heterogeneous reaction system Download PDF

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Publication number
CN209393178U
CN209393178U CN201821946582.2U CN201821946582U CN209393178U CN 209393178 U CN209393178 U CN 209393178U CN 201821946582 U CN201821946582 U CN 201821946582U CN 209393178 U CN209393178 U CN 209393178U
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planetary
reaction system
stirring shaft
stirring
shaft
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罗军奇
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Hunan Kaiplatin Biopharmaceutical Co Ltd
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Hunan Kaiplatin Biopharmaceutical Co Ltd
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Abstract

The utility model relates to a kind of heterogeneous reaction system special utility reaction kettles, it includes autoclave body and the kettle cover that connect with autoclave body top flange dish, the kettle cover is equipped with agitating device, the agitating device includes driving device, agitating shaft, rotary disk, sun gear, multiple planetary gears and planet axis, gear ring, the driving device is installed on the top of kettle cover, the agitating shaft is connect through kettle cover with driving device, the other end protrudes into the bottom of autoclave body, the gear ring is fixed on the inner wall of kettle cover, the sun gear is installed on agitating shaft using key, multiple planetary gears are set between sun gear and gear ring and engage with the sun gear and gear ring, the rotary disk is installed on agitating shaft by bearing, and the rotary disk is located at the top of planetary gear, described planet axis one end is fixed and is fixedly connected after running through planetary gear with rotary disk, the other end protrudes into In autoclave body.The utility model has preferable mixing effect, and reduces wall built-up material to the greatest extent, improves process recovery ratio.

Description

非均相反应体系专用新型反应釜New reactor for heterogeneous reaction system

技术领域technical field

本实用新型涉及反应釜技术领域,尤其涉及一种非均相反应体系专用新型反应釜。The utility model relates to the technical field of reactors, in particular to a novel reactor dedicated to heterogeneous reaction systems.

背景技术Background technique

帕拉米韦生产过程中,部分反应步骤物料体系为非均相费用体系,这种非均相体系比较粘稠,而现有反应釜的搅拌装置为框式搅拌轴,框式搅拌轴主要适用于均相反应体系或粘稠度较小的反应体系,对于粘稠度较大的非均相反应体系存在搅拌不均匀,挂壁物料较多等问题,搅拌不均匀使产品的质量达不到质量标准要求,挂壁物料较多直接导致物料损耗多,导致工艺收率偏低。In the production process of peramivir, the material system of some reaction steps is a heterogeneous cost system, which is relatively viscous, and the stirring device of the existing reactor is a frame-type stirring shaft, which is mainly suitable for For homogeneous reaction systems or reaction systems with low viscosity, there are problems such as uneven stirring and more wall-hanging materials for heterogeneous reaction systems with high viscosity. Uneven stirring makes the quality of the product less than The quality standard requires that more wall-hanging materials directly lead to more material loss, resulting in low process yield.

实用新型内容Utility model content

针对现有技术的不足,本实用新型提供一种非均相反应体系专用新型反应釜,相比于传统框式搅拌轴具有较好的搅拌效果,且最大程度的减少了挂壁物料,提高了工艺收率。Aiming at the deficiencies of the prior art, the utility model provides a new type of reaction kettle dedicated to the heterogeneous reaction system, which has a better stirring effect compared with the traditional frame-type stirring shaft, and reduces the material hanging on the wall to the greatest extent, and improves the Process yield.

本实用新型解决其技术问题所采用的技术方案是:所述非均相反应体系专用新型反应釜包括釜体和与釜体顶部法兰盘连接的釜盖,所述釜盖上设有搅拌装置,所述搅拌装置包括驱动装置、搅拌轴、回转盘、太阳轮、多个行星轮和行星轴、齿圈,所述驱动装置安装于釜盖的顶部,所述搅拌轴贯穿釜盖与驱动装置连接,另一端伸入釜体的底部,所述齿圈固定于釜盖的内壁,所述太阳轮采用键安装于搅拌轴,多个所述行星轮设于太阳轮和齿圈之间且与所述太阳轮和齿圈啮合,所述回转盘通过轴承安装于搅拌轴,且所述回转盘位于行星轮的上方,所述行星轴一端固定并贯穿行星轮后与回转盘固定连接,另一端伸入釜体内。The technical scheme adopted by the utility model to solve the technical problem is: the special-purpose new reaction kettle for the heterogeneous reaction system includes a kettle body and a kettle cover connected with a flange plate on the top of the kettle body, and the kettle cover is provided with a stirring device , the stirring device includes a driving device, a stirring shaft, a rotary disk, a sun gear, a plurality of planetary gears and a planetary shaft, and a ring gear, and the driving device is installed on the top of the kettle cover, and the stirring shaft runs through the kettle cover and the driving device The other end extends into the bottom of the kettle body, the ring gear is fixed on the inner wall of the kettle cover, the sun gear is installed on the stirring shaft with a key, and a plurality of planetary gears are arranged between the sun gear and the ring gear and connected with the The sun gear is engaged with the ring gear, the rotary disc is installed on the stirring shaft through a bearing, and the rotary disc is located above the planetary gear, one end of the planetary shaft is fixed and connected to the rotary disc after passing through the planetary gear, and the other end into the kettle body.

在本实用新型提供的非均相反应体系专用新型反应釜的一种较佳实施例中,所述搅拌轴采用框式搅拌轴,且所述搅拌轴上还设有多个搅拌桨,所述搅拌桨的长度小于搅拌轴至行星轮之间的距离。In a preferred embodiment of the novel reactor dedicated to the heterogeneous reaction system provided by the utility model, the stirring shaft adopts a frame-type stirring shaft, and the stirring shaft is also provided with a plurality of stirring paddles. The length of the stirring paddle is less than the distance from the stirring shaft to the planetary wheel.

在本实用新型提供的非均相反应体系专用新型反应釜的一种较佳实施例中,所述搅拌桨呈多组设于搅拌轴的两侧。In a preferred embodiment of the novel reactor dedicated to the heterogeneous reaction system provided by the utility model, the stirring paddles are arranged in multiple groups on both sides of the stirring shaft.

在本实用新型提供的非均相反应体系专用新型反应釜的一种较佳实施例中,多个所述搅拌桨呈螺旋分布于搅拌轴。In a preferred embodiment of the novel reactor dedicated to the heterogeneous reaction system provided by the utility model, a plurality of the stirring blades are spirally distributed on the stirring shaft.

在本实用新型提供的非均相反应体系专用新型反应釜的一种较佳实施例中,所述行星轮设有均布于太阳轮圆周的2~4个。In a preferred embodiment of the novel reactor dedicated to the heterogeneous reaction system provided by the utility model, the planetary gears are provided with 2 to 4 planetary gears evenly distributed on the circumference of the sun gear.

在本实用新型提供的非均相反应体系专用新型反应釜的一种较佳实施例中,所述行星轴的长度小于搅拌轴的长度。In a preferred embodiment of the novel reactor dedicated to the heterogeneous reaction system provided by the utility model, the length of the planet shaft is shorter than the length of the stirring shaft.

在本实用新型提供的非均相反应体系专用新型反应釜的一种较佳实施例中,所述行星轴的底部设有螺旋叶,所述螺旋叶为左旋或右旋螺旋叶。In a preferred embodiment of the novel reactor dedicated to the heterogeneous reaction system provided by the utility model, the bottom of the planet shaft is provided with a helical leaf, and the helical leaf is a left-handed or right-handed helical leaf.

在本实用新型提供的非均相反应体系专用新型反应釜的一种较佳实施例中,所述行星轴上的螺旋叶的旋向相同或左旋螺旋叶、右旋螺旋叶间隔设置。In a preferred embodiment of the novel reactor dedicated to the heterogeneous reaction system provided by the utility model, the helical leaves on the planetary shaft have the same helical direction or the left-handed helical leaves and the right-handed helical leaves are arranged at intervals.

在本实用新型提供的非均相反应体系专用新型反应釜的一种较佳实施例中,所述釜体的顶部一侧设有进料口,底部设有出料口。In a preferred embodiment of the novel reactor dedicated to the heterogeneous reaction system provided by the utility model, a feed inlet is provided on one side of the top of the kettle body, and a discharge outlet is provided at the bottom.

与现有技术相比,本实用新型提供的非均相反应体系专用新型反应釜的有益效果是:本实用新型利用行星齿轮结构原理,通过搅拌轴上的太阳轮的转动带动行星轮及行星轴的转动,使行星轴自转的同时围绕太阳轮公转,搅拌轴将反应釜内部及底部的物料进行搅拌,而行星轴将反应釜筒壁的物料进行搅拌,保证了反应釜内物料的能充分进行搅拌,搅拌效果好、效率高,且行星轴对反应釜筒壁的搅拌还降低了非均相体系物料的挂壁率,提高了产品的工艺收率。Compared with the prior art, the beneficial effect of the new reactor dedicated to the heterogeneous reaction system provided by the utility model is: the utility model utilizes the principle of the planetary gear structure, and drives the planetary gear and the planetary shaft through the rotation of the sun gear on the stirring shaft The rotation of the planetary shaft makes the planetary shaft rotate around the sun gear at the same time. The stirring shaft stirs the materials inside and at the bottom of the reactor, and the planetary shaft stirs the materials on the wall of the reactor to ensure that the materials in the reactor can be fully processed. Stirring, the stirring effect is good and the efficiency is high, and the stirring of the planetary shaft to the wall of the reactor also reduces the wall hanging rate of the heterogeneous system material and improves the process yield of the product.

附图说明Description of drawings

为了更清楚地说明本实用新型实施例中的技术方案,下面将对实施例描述中所需要使用的附图作简单地介绍,显而易见地,下面描述中的附图仅仅是本实用新型的一些实施例,对于本领域普通技术人员来讲,在不付出创造性劳动的前提下,还可以根据这些附图获得其它的附图,其中:In order to more clearly illustrate the technical solutions in the embodiments of the present invention, the accompanying drawings that need to be used in the description of the embodiments will be briefly introduced below. Obviously, the accompanying drawings in the following description are only some implementations of the present invention. For example, for those of ordinary skill in the art, other drawings can also be obtained based on these drawings without creative work, wherein:

图1是本实用新型提供的非均相反应体系专用新型反应釜的结构示意图;Fig. 1 is the structural representation of the special-purpose novel reactor of heterogeneous reaction system that the utility model provides;

图2是图1提供的非均相反应体系专用新型反应釜的太阳轮和行星轮及齿圈的连接结构图。Fig. 2 is a connection structure diagram of the sun gear, the planetary gear and the ring gear of the new reactor dedicated to the heterogeneous reaction system provided in Fig. 1 .

具体实施方式Detailed ways

下面将结合本实用新型实施例中的附图,对本实用新型实施例中的技术方案进行清楚、完整地描述,显然,所描述的实施例仅是本实用新型的一部分实施例,而不是全部的实施例。基于本实用新型中的实施例,本领域普通技术人员在没有做出创造性劳动前提下所获得的所有其它实施例,都属于本实用新型保护的范围。The technical solutions in the embodiments of the present invention will be clearly and completely described below in conjunction with the accompanying drawings in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of them. Example. Based on the embodiments of the present utility model, all other embodiments obtained by persons of ordinary skill in the art without making creative efforts belong to the scope of protection of the present utility model.

请一并参阅图1及图2,所述非均相反应体系专用新型反应釜1包括釜体11和与釜体顶部法兰盘连接的釜盖12,所述釜盖12上设有搅拌装置13,所述搅拌装置13包括驱动装置131、搅拌轴132、回转盘133、太阳轮134、多个行星轮135和行星轴136、齿圈137,所述驱动装置13安装于釜盖12的顶部,一般地,驱动装置13由驱动电机和减速器组成,所述搅拌轴132贯穿釜盖12与驱动装置13连接,另一端伸入釜体11的底部,所述齿圈137固定于釜盖12的内壁,齿圈可采用焊接或过盈配合的方式进行固定,所述太阳轮134采用键安装于搅拌轴132,多个所述行星轮135设于太阳轮134和齿圈137之间且与所述太阳轮134和齿圈137啮合,所述回转盘133通过轴承安装于搅拌轴132,且所述回转盘133位于行星轮135的上方,所述行星轴136一端固定并贯穿行星轮135后与回转盘133固定连接,另一端伸入釜体11内,行星轴与行星轮采用键安装,行星轴与回转盘采轴承安装。Please refer to Fig. 1 and Fig. 2 together, the special-purpose novel reaction kettle 1 of described heterogeneous reaction system comprises kettle body 11 and the kettle lid 12 that is connected with the flange plate of kettle body top, described kettle lid 12 is provided with stirring device 13. The stirring device 13 includes a driving device 131, a stirring shaft 132, a rotary disk 133, a sun gear 134, a plurality of planetary gears 135, a planetary shaft 136, and a ring gear 137, and the driving device 13 is installed on the top of the kettle cover 12 , generally, the driving device 13 is composed of a driving motor and a reducer, the stirring shaft 132 is connected to the driving device 13 through the kettle cover 12, and the other end extends into the bottom of the kettle body 11, and the ring gear 137 is fixed on the kettle cover 12 The inner wall of the inner wall, the ring gear can be fixed by welding or interference fit, the sun gear 134 is mounted on the stirring shaft 132 with a key, and a plurality of planetary gears 135 are arranged between the sun gear 134 and the ring gear 137 and are connected with The sun gear 134 meshes with the ring gear 137, the rotary disc 133 is mounted on the stirring shaft 132 through a bearing, and the rotary disc 133 is located above the planetary gear 135, and one end of the planetary shaft 136 is fixed and runs through the rear of the planetary gear 135 It is fixedly connected with the rotary disk 133, and the other end stretches into the still body 11. The planetary shaft and the planetary wheel adopt keys to install, and the planetary shaft and the rotary disk adopt bearings to install.

在本实施例中,所述搅拌轴132采用框式搅拌轴,且所述搅拌轴上还设有多个搅拌桨1321,所述搅拌桨1321的长度小于搅拌轴至行星轮之间的距离,使搅拌轴在搅拌的过程中防止搅拌桨与行星轴的碰撞。In this embodiment, the stirring shaft 132 adopts a frame-type stirring shaft, and the stirring shaft is also provided with a plurality of stirring paddles 1321, and the length of the stirring paddles 1321 is less than the distance between the stirring shaft and the planetary wheel. Make the stirring shaft prevent the collision between the stirring paddle and the planetary shaft during the stirring process.

对本实施例的进一步改进,所述搅拌桨1321呈多组设于搅拌轴132的两侧,或多个所述搅拌桨1321呈螺旋分布于搅拌轴132。As a further improvement of this embodiment, the stirring paddles 1321 are arranged in multiple groups on both sides of the stirring shaft 132 , or a plurality of the stirring paddles 1321 are spirally distributed on the stirring shaft 132 .

在本实施例中,所述行星轮135设有均布于太阳轮134圆周的3个,当然也可以是2个、4个。In this embodiment, there are three planetary gears 135 evenly distributed on the circumference of the sun gear 134 , and of course there may be two or four planetary gears.

在本实施例中,所述行星轴136的长度小于搅拌轴132的长度,优选行星轴的长度使其在位于搅拌轴的搅拌框的上方。In this embodiment, the length of the planetary shaft 136 is shorter than the length of the stirring shaft 132 , preferably the length of the planetary shaft is such that it is located above the stirring frame of the stirring shaft.

对本实施例的进一步改进,所述行星轴136的底部设有螺旋叶1362,所述螺旋叶为左旋或右旋螺旋叶。As a further improvement to this embodiment, the bottom of the planetary shaft 136 is provided with a helical blade 1362, and the helical blade is left-handed or right-handed.

对本实施例的进一步改进,所述行星轴136上的螺旋叶1362的旋向相同或左旋螺旋叶、右旋螺旋叶间隔设置。As a further improvement to this embodiment, the helical blades 1362 on the planet shaft 136 have the same direction of rotation or the left-handed helical blades and the right-handed helical blades are arranged at intervals.

在本实施例中,所述釜体11的顶部一侧设有进料口111,底部设有出料口112,对于反应釜其它的接口也可设于釜体的侧壁,在此不做一一介绍,釜体上还可设有冷却或加热用的夹套,此为现有技术,在此不再赘述。In this embodiment, the top side of the kettle body 11 is provided with a feed inlet 111, and the bottom is provided with a discharge outlet 112. Other interfaces of the reactor can also be arranged on the side wall of the kettle body, which will not be described here. To introduce one by one, the kettle body can also be provided with a jacket for cooling or heating, which is a prior art and will not be repeated here.

以上所述仅为本实用新型的实施例,并非因此限制本实用新型的专利范围,凡是利用本实用新型说明书内容所作的等效结构或等效流程变换,或直接或间接运用在其它相关的技术领域,均同理包括在本实用新型的专利保护范围之内。The above descriptions are only examples of the present utility model, and are not intended to limit the patent scope of the present utility model. Any equivalent structure or equivalent process transformation made by using the content of the utility model description, or directly or indirectly used in other related technologies Fields are all included in the scope of patent protection of the utility model in the same way.

Claims (9)

1.一种非均相反应体系专用新型反应釜,其特征在于:包括釜体和与釜体顶部法兰盘连接的釜盖,所述釜盖上设有搅拌装置,所述搅拌装置包括驱动装置、搅拌轴、回转盘、太阳轮、多个行星轮和行星轴、齿圈,所述驱动装置安装于釜盖的顶部,所述搅拌轴贯穿釜盖与驱动装置连接,另一端伸入釜体的底部,所述齿圈固定于釜盖的内壁,所述太阳轮采用键安装于搅拌轴,多个所述行星轮设于太阳轮和齿圈之间且与所述太阳轮和齿圈啮合,所述回转盘通过轴承安装于搅拌轴,且所述回转盘位于行星轮的上方,所述行星轴一端固定并贯穿行星轮后与回转盘固定连接,另一端伸入釜体内。1. A special novel reactor for a heterogeneous reaction system, characterized in that: it comprises a still body and a still cover connected with a flange on the top of the still body, the still cover is provided with a stirring device, and the stirring device includes a drive Device, stirring shaft, rotary disc, sun gear, multiple planetary gears and planetary shafts, ring gear, the driving device is installed on the top of the kettle cover, the stirring shaft passes through the kettle cover and is connected to the driving device, and the other end extends into the kettle The bottom of the body, the ring gear is fixed on the inner wall of the kettle cover, the sun gear is installed on the stirring shaft with a key, and a plurality of the planetary gears are arranged between the sun gear and the ring gear and connected with the sun gear and the ring gear Mesh, the rotary disc is installed on the stirring shaft through bearings, and the rotary disc is located above the planetary gear, one end of the planetary shaft is fixed and connected with the rotary disc after passing through the planetary gear, and the other end extends into the kettle body. 2.根据权利要求1所述的非均相反应体系专用新型反应釜,其特征在于:所述搅拌轴采用框式搅拌轴,且所述搅拌轴上还设有多个搅拌桨,所述搅拌桨的长度小于搅拌轴至行星轮之间的距离。2. The special novel reactor for heterogeneous reaction system according to claim 1, characterized in that: the stirring shaft adopts a frame-type stirring shaft, and the stirring shaft is also provided with a plurality of stirring paddles, and the stirring shaft The length of the paddle is less than the distance from the stirring shaft to the planetary wheel. 3.根据权利要求2所述的非均相反应体系专用新型反应釜,其特征在于:所述搅拌桨呈多组设于搅拌轴的两侧。3. The special-purpose novel reactor for heterogeneous reaction system according to claim 2, characterized in that: said stirring paddles are arranged in multiple groups on both sides of the stirring shaft. 4.根据权利要求2所述的非均相反应体系专用新型反应釜,其特征在于:多个所述搅拌桨呈螺旋分布于搅拌轴。4. The special-purpose novel reactor for heterogeneous reaction system according to claim 2, characterized in that: a plurality of said stirring blades are spirally distributed on the stirring shaft. 5.根据权利要求1所述的非均相反应体系专用新型反应釜,其特征在于:所述行星轮设有均布于太阳轮圆周的2~4个。5. The new reactor for heterogeneous reaction system according to claim 1, characterized in that: said planetary gears are provided with 2 to 4 planetary gears evenly distributed on the circumference of the sun gear. 6.根据权利要求1或2所述的非均相反应体系专用新型反应釜,其特征在于:所述行星轴的长度小于搅拌轴的长度。6. The special-purpose novel reactor for heterogeneous reaction system according to claim 1 or 2, characterized in that: the length of the planetary shaft is less than the length of the stirring shaft. 7.根据权利要求6所述的非均相反应体系专用新型反应釜,其特征在于:所述行星轴的底部设有螺旋叶,所述螺旋叶为左旋或右旋螺旋叶。7. The special-purpose new reaction kettle for heterogeneous reaction system according to claim 6, characterized in that: the bottom of the planet shaft is provided with a helical leaf, and the helical leaf is a left-handed or right-handed helical leaf. 8.根据权利要求7所述的非均相反应体系专用新型反应釜,其特征在于:所述行星轴上的螺旋叶的旋向相同或左旋螺旋叶、右旋螺旋叶间隔设置。8. The new reaction kettle for heterogeneous reaction system according to claim 7, characterized in that: the helical leaves on the planetary shaft have the same direction of rotation or the left-handed helical leaves and right-handed helical leaves are arranged at intervals. 9.根据权利要求1所述的非均相反应体系专用新型反应釜,其特征在于:所述釜体的顶部一侧设有进料口,底部设有出料口。9. The special-purpose novel reaction kettle for heterogeneous reaction system according to claim 1, characterized in that: the top side of the kettle body is provided with a feed inlet, and the bottom is provided with a discharge outlet.
CN201821946582.2U 2018-11-23 2018-11-23 New reactor for heterogeneous reaction system Expired - Fee Related CN209393178U (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110947352A (en) * 2019-12-09 2020-04-03 安徽亿昊新材料科技有限公司 Macromolecular material reation kettle and production facility
CN112090107A (en) * 2020-09-21 2020-12-18 怀化市恒渝新材料有限公司 Purification crystallization kettle for preparing photoinitiator
CN115178221A (en) * 2022-09-07 2022-10-14 胜利油田方圆化工有限公司 Oil field oil recovery chemical auxiliary raw materials mixes reation kettle

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110947352A (en) * 2019-12-09 2020-04-03 安徽亿昊新材料科技有限公司 Macromolecular material reation kettle and production facility
CN112090107A (en) * 2020-09-21 2020-12-18 怀化市恒渝新材料有限公司 Purification crystallization kettle for preparing photoinitiator
CN115178221A (en) * 2022-09-07 2022-10-14 胜利油田方圆化工有限公司 Oil field oil recovery chemical auxiliary raw materials mixes reation kettle

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