CN209393154U - Gu a kind of liquid-liquid/gas generator - Google Patents
Gu a kind of liquid-liquid/gas generator Download PDFInfo
- Publication number
- CN209393154U CN209393154U CN201822247748.8U CN201822247748U CN209393154U CN 209393154 U CN209393154 U CN 209393154U CN 201822247748 U CN201822247748 U CN 201822247748U CN 209393154 U CN209393154 U CN 209393154U
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- Prior art keywords
- liquid
- kettle
- sealing pipe
- gas
- partition
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/30—Hydrogen technology
- Y02E60/36—Hydrogen production from non-carbon containing sources, e.g. by water electrolysis
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Abstract
Gu the utility model discloses a kind of liquid-liquid/gas generator, including low level kettle (1), high-order kettle (8) and dropping funel (10).High position kettle (8) top be it is spherical open, spherical bottom is provided with partition, partition aperture and inserted with connecting tube between kettle (2) and liquid sealing pipe (4)；The junction of partition and pipeline seals；Liquid sealing pipe (4) upper end opening, lower end is closed, and side wall is located at partition lower end and is provided with liquid droping port (6)；The high position kettle (8) is placed in low level kettle (1) upper end, and the two is tightly connected；Dropping funel (10) is inserted into liquid sealing pipe (4), is sealed at liquid sealing pipe (11) suitable for reading.Device provided by the utility model realizes liquid-liquid reactions and liquid-solid reaction gas and takes the automatic control of gas velocity degree, also complies with the principle of " using with the opening, with Guan Suiting ".Drug can be effectively saved, the generation and stopping of reaction are controlled, it can the adding liquid drug into device at any time.
Description
Technical field
The utility model belongs to chemical field, in particular to liquid-liquid and liquid-solid contact gas generator.
Background technique
Kipp gas generator (Kipp's apparatus), is a kind of gas generator, also known as Qi Shi gas generator or hydrogen
Gas generator.It is Dutch scientist's Pietrus Jack's Bath open it is general (Petrus Jacobus Kipp, 1808~
1864) utility model, and with the name of his surname.It is commonly used in the experiment of solid particle and liquid reactions to produce gas
Body.Typical experiment is exactly to utilize dilute sulfuric acid and zinc granule hydrogen making.It can save drug, control the generation and stopping of reaction,
Can the adding liquid drug into device at any time, meet the principle of " using with the opening, with Guan Suiting ".But liquid and liquid reactions are produced
Gas cannot use kipp gas generator；When blocks of solid dissolves quickly in the reaction, kipp gas generator can not be used.
Utility model content
In order to solve the above technical problems, the utility model provide one kind can liquid and solid reaction gas, also can liquid
With liquid reactions gas, the gas generator that " can be used with the opening, with Guan Suiting ".
The technical scheme that the utility model is provided is as follows:
Gu a kind of liquid-liquid/gas generator, including low level kettle (1), high-order kettle (8) and dropping funel (10).
High position kettle (8) top be it is spherical open, spherical bottom is provided with partition, partition aperture and inserted with connecting between kettle
Take over (2) and liquid sealing pipe (4)；The junction of partition and pipeline seals.
Liquid sealing pipe (4) upper end opening, lower end is closed, and side wall is located at partition lower end and is provided with liquid droping port (6).
The high position kettle (8) is placed in low level kettle (1) upper end, and the two is tightly connected；Dropping funel (10) is inserted into liquid sealing pipe
(4) it in, is sealed at liquid sealing pipe (11) suitable for reading.
Specifically, the low level kettle (1) is made of spherical epicoele and hemispheric cavity of resorption；Epicoele upper end opening, up and down
Chamber junction enables epicoele bottom to place admittedly to formation gap between connecting tube between contract and kettle (2) and liquid sealing pipe (4)
Body raw material, cavity of resorption bottom are closed.Epicoele side wall is provided with gas vent (5)；Cavity of resorption is provided with Butterworth Hatch (3).
Specifically, connecting tube (2), liquid sealing pipe (4) are integrally formed between the partition and kettle.
Specifically, connecting tube (2) and liquid sealing pipe (4) are inserted into low level kettle (1) cavity of resorption between the kettle of the high position kettle (8).
Device provided by the utility model can be used for liquid liquid gas and liquid gas admittedly processed.
One, liquid liquid jia bombardier is rapid:
(1) cap covers Butterworth Hatch (3) are used, gas vent (7) accesses the gas-guide tube with air valve (7), closes liquid-dropping valve (9)
With air valve (7)；
(2) in two kinds of material liquids of preparing gas, a kind of material liquid that price is more expensive is selected to be added in addition funnel；
(3) after observing liquid-dropping valve (10) no leakage, the lower material liquid of another price is added to high-order kettle (8)
In；
(4) it observes that high-low position kettle has liquid level difference, when liquid level difference does not change over time, opens air valve (7)；
(5) it after the material liquid in high-order kettle (8) all flows into low level kettle (1), closes air valve (7)；
(6) liquid-dropping valve (9) are opened, prepares gas；
(7) air valve (7) are opened and takes gas.
Two, liquid jia bombardier admittedly processed is rapid:
(1) low level kettle (1) epicoele is added in solid material, with cap covers Butterworth Hatch (3), it is gentle closes liquid-dropping valve (9)
Valve (7)；
(2) liquid charging stock is added in high-order kettle (8)；
(3) it observes that high-low position kettle has liquid level difference, when liquid level difference does not change over time, opens air valve (7)；
(4) after the material liquid in high-order kettle (8) all flows into low level kettle (1), air valve (7) gas processed is closed；
(5) air valve (7) are opened and takes gas.
The reactive liquid solution rate controlling principle of device provided by the utility model:
When preparing gas, open liquid-dropping valve (9), reaction solution starts haptoreaction.When just having opened liquid-dropping valve (9), dropping liquid is pushed away
Power is maximum, is equal to the head of liquid of dropping funel (10) liquid level liquid sealing pipe (4) liquid level at liquid droping port (6), liquid droping speed is most
Fastly, gas processed is fastest.As the gas produced gathers in low level kettle ullage, air pressure is gradually increased in kettle, and liquid is passed through
Connecting tube (2) presses to high-order kettle (8) between kettle, and is gradually reduced dropwise addition motive force, and rate of addition slows down, and gas velocity degree processed slows down；
When liquid level liquid sealing pipe (4) liquid at liquid droping port (6) on air pressure=high-low position kettle hydraulic pressure difference=dropping funel (10) of low level kettle
When the hydraulic pressure difference in face, it is zero that motive force, which is added dropwise, is added dropwise and stops, and gas processed stops.
When demand gas, air valve (7) can be opened at any time and takes gas.When just having opened air valve (7), the interior pressure of low level kettle (1) is maximum,
Take gas fastest, with the taking-up of gas, (1) air pressure of low level kettle is reduced, and is made to take the reduction of gas velocity degree, is also made dropwise addition motive force extensive
Redoubling increases, and is added dropwise and restores and speed increases, and gas processed restores and speed increases, and quickly reaches balance, gas processed with take gas velocity degree phase
Deng.Hereafter, gas constant airspeed is taken, if increasing air valve (7) aperture, when just starting, the interior pressure of low level kettle (1) is maximum, takes gas velocity degree
Most fast, with the taking-up of increment gas, (1) air pressure of low level kettle is reduced, and makes to take the reduction of gas velocity degree, also makes that motive force increase is added dropwise,
Rate of addition is accelerated, and gas velocity degree processed increases, and quickly reaches balance, gas processed is equal with gas velocity degree is taken, hereafter, biggish to take gas velocity degree
It is constant.Take gas velocity degree that can be adjusted at any time with air valve (7).
The design of liquid sealing pipe (4) can be effectively isolated two kinds of reaction solutions, and the two is mixed in reaction without a large amount of, in turn
The separation and mixing for repeating to realize two kinds of reaction solutions by the pressure that gas generates may be implemented.In addition to this, liquid droping port 6 can also
The enough pressure generated by gas realizes the control of liquid droping speed.Liquid sealing pipe (4) can be realized above two technical effect in turn
Realize " the using with the opening, with Guan Suiting " of reactive liquid solution.
The utility model has the beneficial effects that
Device provided by the utility model realizes liquid-liquid reactions and liquid-solid reaction gas and takes the automatic control of gas velocity degree
System, also complies with the principle of " using with the opening, with Guan Suiting ".Drug can be effectively saved, the generation and stopping of reaction are controlled, it can be with
When into device adding liquid drug.
Detailed description of the invention
Gu Fig. 1 is a kind of liquid-liquid/gas generator schematic diagram；
Appended drawing reference: 1- low level kettle；Connecting tube between 2- kettle；3- Butterworth Hatch；4- liquid sealing pipe；5- gas vent；6- liquid droping port；
7- air valve；8- high position kettle；9- liquid-dropping valve；10- dropping funel；11- is suitable for reading；12- top opening；13- minim pipette.
Specific embodiment
The utility model is illustrated combined with specific embodiments below, the content of the utility model is completely without being limited thereto.
Embodiment 1
Fig. 1 shows the utility model and provides the structure of device.
Gu a kind of liquid-liquid/gas generator, including low level kettle 1, high-order kettle 8 and dropping funel 10.
High-order 8 top of kettle be it is spherical open, spherical bottom is provided with partition, partition aperture and inserted with connecting tube 2 between kettle
With liquid sealing pipe 4；The junction of partition and pipeline seals.Preferably, connecting tube 2, liquid sealing pipe 4 are integrally formed between partition and kettle.
4 upper end opening of liquid sealing pipe, lower end is closed, and side wall is located at partition lower end and is provided with liquid droping port 6.
High-order kettle 8 is placed in 1 upper end of low level kettle, and the two is tightly connected.Preferably, the two ground connects.Between the kettle of high-order kettle 8
Connecting tube 2 and liquid sealing pipe 4 are inserted into the cavity of resorption of low level kettle 1.Dropping funel 10 is inserted into liquid sealing pipe 4, at liquid sealing pipe suitable for reading 11
Sealing can be connect at this with dropping funel 10 by the way of ground, seal gasket/set also can be used and be sealed.It is excellent
Choosing, it is connected at top opening 12 for ground.
Low level kettle 1 is made of spherical epicoele and hemispheric cavity of resorption.Epicoele upper end opening, upper and lower cavity junction are inwardly received
Gap is formed between contracting and kettle between connecting tube 2 and liquid sealing pipe 4 for placing solid material, cavity of resorption bottom is closed.Epicoele side wall is opened
There is gas vent 5；Cavity of resorption is provided with Butterworth Hatch 3.
Application Example 1
Prepare ammonia
1) that saturated solution is made in diffluent ammonium hydrogen carbonate is spare；
2) cap covers Butterworth Hatch 3 is used, liquid-dropping valve 9 and air valve 7 are closed；
3) 20% sodium hydroxide solution is added in addition funnel 10；
4) after observing and confirming 9 no leakage of liquid-dropping valve, the ammonium hydrogen carbonate saturated solution got ready is added in high-order kettle 8；
5) liquid level difference for observing high-low position kettle when liquid level difference does not change over time, i.e., after air tight, opens air valve 7；
6) after the ammonium hydrogen carbonate saturated solution in high-order kettle 8 all flows into low level kettle 1, air valve 7 is closed；
7) liquid-dropping valve 9 is opened, preparing gas is stand-by；
8) when demand gas, air valve 7 can be opened at any time and takes gas.
Application Example 2
Prepare carbon dioxide
1) that saturated solution is made in diffluent ammonium hydrogen carbonate is spare；
2) cap covers Butterworth Hatch 3 is used, liquid-dropping valve 9 and air valve 7 are closed；
3) 98% concentrated sulfuric acid is added in addition funnel 10；
4) after observing and confirming 9 no leakage of liquid-dropping valve, the ammonium hydrogen carbonate saturated solution got ready is added in high-order kettle 8；
5) liquid level difference for observing high-low position kettle when liquid level difference does not change over time, i.e., after air tight, opens air valve 7；
6) after the ammonium hydrogen carbonate saturated solution in high-order kettle 8 all flows into low level kettle 1, air valve 7 is closed；
7) liquid-dropping valve 9 is opened, preparing gas is stand-by；
8) when demand gas, air valve 7 can be opened at any time and takes gas.
Application Example 3
Prepare hydrogen sulfide
1) that saturated solution is made in diffluent vulcanized sodium is spare；
2) cap covers Butterworth Hatch 3 is used, liquid-dropping valve 9 and air valve 7 are closed；
3) 98% concentrated sulfuric acid is added in addition funnel 10；
4) after observing and confirming 9 no leakage of liquid-dropping valve, the vulcanized sodium saturated solution got ready is added in high-order kettle 8；
5) liquid level difference of high-low position kettle is observed, and confirms that liquid level difference does not change over time, i.e., after air tight, opens air valve
7；
6) after the vulcanized sodium saturated solution in high-order kettle 8 all flows into low level kettle 1, air valve 7 is closed；
7) liquid-dropping valve 9 is opened, preparing gas is stand-by；
8) when demand gas, air valve 7 can be opened at any time and takes gas.
Application Example 4
Prepare hydrogen
1) zinc granule is added to 1 epicoele of low level kettle；
2) cap covers Butterworth Hatch 3 is used, liquid-dropping valve 9 and air valve 7 are closed；
3) dilute hydrochloric acid is added in high-order kettle 8；
4) it observes that high-low position kettle has liquid level difference, when liquid level difference does not change over time, i.e., after air tight, opens air valve 7；
5) after the acid solution in high-order kettle 8 all flows into low level kettle 1, the gas processed of air valve 7 is closed；
6) it opens air valve 7 and takes gas.
The above is only the preferred embodiment of the utility model, it is noted that for the common skill of the art
For art personnel, without deviating from the technical principle of the utility model, several improvements and modifications can also be made, these change
It also should be regarded as the protection scope of the utility model into modification.
Claims (4)
1. Gu a kind of liquid-liquid/gas generator, it is characterised in that:
Including low level kettle (1), high-order kettle (8) and dropping funel (10)；
High position kettle (8) top be it is spherical open, spherical bottom is provided with partition, partition aperture and inserted with connecting tube between kettle
(2) and liquid sealing pipe (4)；The junction of partition and pipeline seals；
Liquid sealing pipe (4) upper end opening, lower end is closed, and side wall is located at partition lower end and is provided with liquid droping port (6)；
The high position kettle (8) is placed in low level kettle (1) upper end, and the two is tightly connected；Dropping funel (10) is inserted into liquid sealing pipe (4)
In, it is sealed at liquid sealing pipe (11) suitable for reading.
2. Gu liquid-liquid/gas generator according to claim 1, it is characterised in that: the low level kettle (1) is by spherical shape
Epicoele and hemispheric cavity of resorption composition；Epicoele upper end opening, upper and lower cavity junction is to connecting tube between contract and kettle (2) and fluid-tight
Gap is formed between pipe (4), cavity of resorption bottom is closed；Epicoele side wall is provided with gas vent (5)；Cavity of resorption is provided with Butterworth Hatch (3).
3. Gu liquid-liquid/gas generator according to claim 1, it is characterised in that: connecting tube between the partition and kettle
(2), liquid sealing pipe (4) is integrally formed.
4. Gu liquid-liquid/gas generator according to claim 1 or 2, it is characterised in that: between the kettle of the high position kettle (8)
Connecting tube (2) and liquid sealing pipe (4) are inserted into low level kettle (1) cavity of resorption.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201822247748.8U CN209393154U (en) | 2018-12-29 | 2018-12-29 | Gu a kind of liquid-liquid/gas generator |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201822247748.8U CN209393154U (en) | 2018-12-29 | 2018-12-29 | Gu a kind of liquid-liquid/gas generator |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN209393154U true CN209393154U (en) | 2019-09-17 |
Family
ID=67897043
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201822247748.8U Expired - Fee Related CN209393154U (en) | 2018-12-29 | 2018-12-29 | Gu a kind of liquid-liquid/gas generator |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN209393154U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109464966A (en) * | 2018-12-29 | 2019-03-15 | 黄冈师范学院 | Gu a kind of liquid-liquid/gas generator |
-
2018
- 2018-12-29 CN CN201822247748.8U patent/CN209393154U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109464966A (en) * | 2018-12-29 | 2019-03-15 | 黄冈师范学院 | Gu a kind of liquid-liquid/gas generator |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20190917 Termination date: 20211229 |