CN209348619U - A kind of Organometallic Chemistry apparatus for photoreaction - Google Patents
A kind of Organometallic Chemistry apparatus for photoreaction Download PDFInfo
- Publication number
- CN209348619U CN209348619U CN201822278921.0U CN201822278921U CN209348619U CN 209348619 U CN209348619 U CN 209348619U CN 201822278921 U CN201822278921 U CN 201822278921U CN 209348619 U CN209348619 U CN 209348619U
- Authority
- CN
- China
- Prior art keywords
- fixedly installed
- reaction vessel
- organometallic chemistry
- reserve tank
- reaction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Landscapes
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The utility model relates to technical field of organic chemistry, and disclose a kind of Organometallic Chemistry apparatus for photoreaction, including pedestal, reaction vessel is fixedly installed at the top of the pedestal, the bottom of the reaction vessel is fixedly installed with the inside positioned at pedestal and extends to the drain pipe of chassis left side.The Organometallic Chemistry apparatus for photoreaction, the inside of liquid reserve tank can be marked off to two liquid storage spaces by partition, so as to back up two kinds of differential responses objects, when needing the inside of the reaction vessel to carry out Organometallic Chemistry light reaction to add new reactant, rotate liquid reserve tank, so that corresponding through-hole turns to the left side of plup inlet, then control valve is opened, so that the reactant inside liquid reserve tank passes sequentially through through-hole and plup inlet enters the inside of reaction vessel and reacted, it is easy to operate, it is easy to use, not only make the result of reaction more accurate, also assure the safety of staff.
Description
Technical field
The utility model relates to technical field of organic chemistry, specially a kind of Organometallic Chemistry apparatus for photoreaction.
Background technique
Organic reaction is related to the chemical reaction of organic compound, is the basis of organic synthesis, several fundamental reaction types
For substitution reaction, addition reaction, elimination reaction, pericyclic reaction, rearrangement reaction and redox reaction, Organometallic Chemistry reaction
As it is related to metal-organic chemical reaction, metallic compound is to contain one or more metal-carbon key in molecule
Or the compound of metal-hydrogen key, the specific type that not can be carried out of general organic chemistry reaction change, it sometimes can excuse me chemistry side
Method realizes that as Organometallic Chemistry light reaction, Organometallic Chemistry light reaction needs to use dedicated reaction unit.
Organometallic Reac- tion should carry out in the environment of anhydrous and oxygen-free, and existing Organometallic Chemistry apparatus for photoreaction exists
It needs to open lid when new reactant being added in reaction process, thus influence whether the air-tightness of reaction environment, it not only can be right
Reaction result affects, and can also have some potential safety problems, so it is anti-to propose a kind of Organometallic Chemistry light
Answer device.
Utility model content
(1) the technical issues of solving
In view of the deficiencies of the prior art, the utility model provides a kind of Organometallic Chemistry apparatus for photoreaction, has just
In add reactant the advantages that, solves existing Organometallic Chemistry apparatus for photoreaction and new reaction is added during the reaction
It needs to open lid when object, to influence whether the air-tightness of reaction environment, can not only affect to reaction result,
Can also there are problems that some potential safety problems.
(2) technical solution
To realize the above-mentioned purpose convenient for addition reactant, the utility model provided the following technical solutions: a kind of metal has
Chemical machine apparatus for photoreaction, including pedestal are fixedly installed with reaction vessel, the bottom of the reaction vessel at the top of the pedestal
It is fixedly installed with the inside positioned at pedestal and extends to the drain pipe of chassis left side, be fixedly installed with and be located at the top of the pedestal
The lamp holder of reaction vessel interior is fixedly installed with ultraviolet radiator, the fixed peace in the inside of the reaction vessel at the top of the lamp holder
Equipped with the cloche being located at outside ultraviolet radiator, feeding pipe, the top of the pedestal are fixedly installed at the top of the reaction vessel
Portion is fixedly installed with the mounting base on the right side of reaction vessel, and the internal activity of the mounting base is equipped with shaft, the shaft
Outside be socketed with axle sleeve, the movable plate being fixedly installed at the top of the shaft at the top of mounting base, the movable plate
Top is fixedly installed with liquid reserve tank, and the outside of the liquid reserve tank is fixedly installed with the sealing plate at the top of movable plate, described anti-
The inner wall right side opening of container is answered to be equipped with the plup inlet being through to inside mounting base, the inside of the sealing plate is fixedly installed with control
Valve, the inside of the liquid reserve tank are fixedly installed with partition, and there are two liquid-in pipe, two institutes for the top fixed installation of the liquid reserve tank
The relatively uniform side for stating liquid-in pipe is fixed with exhaust tube, and the inside of the reaction vessel is fixedly installed with water cooling tube, feeding pipe
Left side is fixedly installed with exhaust pipe.
Preferably, the inside of the sealing plate offers through-hole, and the quantity of through-hole is two, and two through-holes are uniformly distributed in
The left and right sides of sealing plate.
Preferably, the quantity of the control valve is two, and two control valves are uniformly distributed in the inside of two through-holes.
Preferably, valve, the quantity of valve are provided at the top of the opposite side of two liquid-in pipes and exhaust tube
It is four.
Preferably, the bottom of the shaft is provided with the limit plate inside mounting base, and limit plate is located at the bottom of axle sleeve
Portion, the diameter of limit plate are greater than the diameter of axle sleeve.
Preferably, the two sides up and down of the sealing plate are provided with sealing strip, sealing strip shape in a ring, the quantity of sealing strip
It is two.
(3) beneficial effect
Compared with prior art, the utility model provides a kind of Organometallic Chemistry apparatus for photoreaction, and having following has
Beneficial effect:
1, the inside of liquid reserve tank can be marked off two liquid storage skies by partition by the Organometallic Chemistry apparatus for photoreaction
Between, so as to back up two kinds of differential responses objects, when needs are the reaction vessel for carrying out Organometallic Chemistry light reaction
When new reactant is added in inside, liquid reserve tank is rotated, so that corresponding through-hole turns to the left side of plup inlet, then opens control
Valve, so that the reactant inside liquid reserve tank passes sequentially through through-hole and plup inlet enters the inside of reaction vessel and reacted,
It is easy to operate, it is easy to use, not only make the result of reaction more accurate, it is ensured that the safety of staff.
2, the Organometallic Chemistry apparatus for photoreaction can be controlled separately two kinds by two through-holes and two control valves
Reactant enters the inside of reaction vessel, increases operability when reaction, and the use for the staff that is more convenient for passes through shaft
It is more stable in rotation can to make shaft, movable plate, liquid reserve tank and sealing plate for the limit plate of bottom setting, and not
It will appear the case where shaft falls off, the sealing strip being arranged by two sides above and below sealing plate can effectively increase the reaction unit
Leakproofness, ensure that the stability of reaction, and stabilization when sealing plate rotation can be increased, so that logical inside sealing plate
Hole can accurately be docked with plup inlet, and then increase the stability of the reaction unit, open the corresponding valve of liquid-in pipe, so that
Spare reactant can be entered by liquid-in pipe, be then shut off the corresponding valve of liquid-in pipe, open the valve at the top of corresponding exhaust tube
Door can carry out pumping and inert gas replacement operation, be then shut off valve, so that the inside of liquid reserve tank is in anhydrous and oxygen-free environment,
To ensure that the accuracy of test.
Detailed description of the invention
FIG. 1 is a schematic structural view of the utility model；
Fig. 2 is the utility model liquid reserve tank top view；
Fig. 3 is the utility model liquid-in pipe left view.
In figure: 1 pedestal, 2 reaction vessels, 3 drain pipes, 4 lamp holders, 5 ultraviolet radiator, 6 cloches, 7 feeding pipes, 8 mounting bases,
9 shafts, 10 axle sleeves, 11 movable plates, 12 liquid reserve tanks, 13 sealing plates, 14 plup inlets, 15 control valves, 16 partitions, 17 liquid-in pipes, 18
Exhaust tube, 19 water cooling tubes, 20 exhaust pipes.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model
Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole
Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work
Every other embodiment obtained, fall within the protection scope of the utility model.
Fig. 1-3, a kind of Organometallic Chemistry apparatus for photoreaction, including pedestal 1 are please referred to, the top of pedestal 1 is fixedly mounted
There is reaction vessel 2, the bottom of reaction vessel 2 is fixedly installed with the inside positioned at pedestal 1 and extends to the drain pipe in 1 left side of pedestal
3, the top of pedestal 1 is fixedly installed with the lamp holder 4 inside reaction vessel 2, and the top of lamp holder 4 is fixedly installed with ultraviolet radiator
5, the inside of reaction vessel 2 is fixedly installed with the cloche 6 outside ultraviolet radiator 5, and the top of reaction vessel 2 is fixedly mounted
There is feeding pipe 7, the top of pedestal 1 is fixedly installed with the mounting base 8 positioned at 2 right side of reaction vessel, the internal activity peace of mounting base 8
Equipped with shaft 9, the outside of shaft 9 is socketed with axle sleeve 10, and the bottom of shaft 9 is provided with the limit plate inside mounting base 8, limit
Position plate is located at the bottom of axle sleeve 10, and the diameter of limit plate is greater than the diameter of axle sleeve 10, to enhance stabilization when shaft 9 rotates
Property, prevent shaft 9 from falling off, the top of shaft 9 is fixedly installed with the movable plate 11 positioned at 8 top of mounting base, the top of movable plate 11
Portion is fixedly installed with liquid reserve tank 12, and the outside of liquid reserve tank 12 is fixedly installed with the sealing plate 13 positioned at 11 top of movable plate, sealing
The inside of plate 13 offers through-hole, and the quantity of through-hole is two, and two through-holes are uniformly distributed in the left and right sides of sealing plate 13, use
Reactant inside liquid reserve tank 12 enters the inside of reaction vessel 2, and the two sides up and down of sealing plate 13 are provided with sealing strip, close
Shape, the quantity of sealing strip are two to strip of paper used for sealing in a ring, increase the leakproofness of the reaction unit, the inner wall right side of reaction vessel 2
The plup inlet 14 being through to inside mounting base 8 is offered, the inside of sealing plate 13 is fixedly installed with control valve 15, control valve 15
Quantity is two, and two control valves 15 are uniformly distributed in the inside of two through-holes, for controlling the flow velocity of through-hole internal-response object,
The inside of liquid reserve tank 12 is fixedly installed with partition 16, and there are two liquid-in pipes 17 for the top fixed installation of liquid reserve tank 12, and two enter liquid
The relatively uniform side of pipe 17 is fixed with exhaust tube 18, and the opposite side of two liquid-in pipes 17 and the top of exhaust tube 18 are provided with
Valve, the quantity of valve is four, for controlling the entrance of reactant and being evacuated to the inside of liquid reserve tank 12, reaction vessel
2 inside is fixedly installed with water cooling tube 19, and the left side of feeding pipe 7 is fixedly installed with exhaust pipe 20, for carrying out to reaction vessel 2
Pumping and inert gas replacement operation, guarantee the air-tightness inside reaction vessel 2, which leads to
The inside of liquid reserve tank 12 can be marked off in two liquid storage spaces by crossing partition 16, so as to back up two kinds of differential responses objects, when need
When adding new reactant for the inside for the reaction vessel 2 for carrying out Organometallic Chemistry light reaction, liquid reserve tank 12 is rotated,
So that corresponding through-hole turns to the left side of plup inlet 14, control valve 15 is then opened, so that anti-inside liquid reserve tank 12
The inside for answering object to pass sequentially through through-hole and plup inlet 14 into reaction vessel 2 is reacted, easy to operate, easy to use, not only
So that the result of reaction is more accurate, it is ensured that the safety of staff can be with by two through-holes and two control valves 15
The inside that two kinds of reactants enter reaction vessel 2 is controlled respectively, is increased operability when reaction, is more convenient for staff's
It uses, the limit plate being arranged by 9 bottom of shaft, shaft 9, movable plate 11, liquid reserve tank 12 and sealing plate 13 can be made to turn
It is more stable when dynamic, and be not in the case where shaft 9 falls off, the sealing strip being arranged by about 13 two sides of sealing plate,
The leakproofness that the reaction unit can effectively be increased ensure that the stability of reaction, and can increase the rotation of sealing plate 13
When stabilization, the through-hole inside sealing plate 13 is accurately docked with plup inlet 14, and then increase the reaction unit
Stability opens the corresponding valve of liquid-in pipe 17, spare reactant is entered by liquid-in pipe, is then shut off liquid-in pipe
17 corresponding valves, the valve for opening corresponding 18 top of exhaust tube can carry out pumping and inert gas replacement operation, be then shut off
Valve, so that the inside of liquid reserve tank 12 is in anhydrous and oxygen-free environment, to ensure that the accuracy of test.
In conclusion the Organometallic Chemistry apparatus for photoreaction, can be marked off the inside of liquid reserve tank 12 by partition 16
Two liquid storage spaces, so as to back up two kinds of differential responses objects, when needs are to carry out Organometallic Chemistry light reaction
When new reactant is added in the inside of reaction vessel 2, liquid reserve tank 12 is rotated, so that corresponding through-hole turns to a left side for plup inlet 14
Then control valve 15 is opened in side, so that the reactant inside liquid reserve tank 12 passes sequentially through through-hole and plup inlet 14 enters instead
The inside of container 2 is answered to be reacted, it is easy to operate, it is easy to use, not only make the result of reaction more accurate, it is ensured that work
The safety for making personnel can be controlled separately two kinds of reactants and enter reaction vessel 2 by two through-holes and two control valves 15
Inside increases operability when reaction, the use for the staff that is more convenient for, the limit plate being arranged by 9 bottom of shaft, can
It so that shaft 9, movable plate 11, liquid reserve tank 12 and sealing plate 13 are more stable in rotation, and is not in that shaft 9 is de-
The case where falling, the sealing strip being arranged by about 13 two sides of sealing plate, can effectively increase the leakproofness of the reaction unit, protect
The stability of reaction has been demonstrate,proved, and stabilization when sealing plate 13 rotates can be increased, so that through-hole inside sealing plate 13 can be with
It is accurately docked with plup inlet 14, and then increases the stability of the reaction unit, the corresponding valve of liquid-in pipe 17 is opened, so that standby
It can be entered by liquid-in pipe with reactant, be then shut off the corresponding valve of liquid-in pipe 17, open corresponding 18 top of exhaust tube
Valve can carry out pumping and inert gas replacement operation, valve is then shut off, so that the inside of liquid reserve tank 12 is in anhydrous and oxygen-free
Environment solves existing Organometallic Chemistry apparatus for photoreaction and adds during the reaction to ensure that the accuracy of test
It needs to open lid when entering new reactant, to influence whether the air-tightness of reaction environment, reaction result can not only be caused
Certain influence can also have some potential safety problems.
It should be noted that, in this document, relational terms such as first and second and the like are used merely to a reality
Body or operation are distinguished with another entity or operation, are deposited without necessarily requiring or implying between these entities or operation
In any actual relationship or order or sequence.Moreover, the terms "include", "comprise" or its any other variant are intended to
Non-exclusive inclusion, so that the process, method, article or equipment including a series of elements is not only wanted including those
Element, but also including other elements that are not explicitly listed, or further include for this process, method, article or equipment
Intrinsic element.In the absence of more restrictions, the element limited by sentence "including a ...", it is not excluded that
There is also other identical elements in process, method, article or equipment including the element.
While there has been shown and described that the embodiments of the present invention, for the ordinary skill in the art,
It is understood that these embodiments can be carried out with a variety of variations in the case where not departing from the principles of the present invention and spirit, repaired
Change, replacement and variant, the scope of the utility model is defined by the appended claims and the equivalents thereof.
Claims (6)
1. a kind of Organometallic Chemistry apparatus for photoreaction, including pedestal (1), it is characterised in that: the top of the pedestal (1) is fixed
It is equipped with reaction vessel (2), the bottom of the reaction vessel (2) is fixedly installed with the inside positioned at pedestal (1) and extends to bottom
Drain pipe (3) on the left of seat (1) is fixedly installed with the lamp holder (4) internal positioned at reaction vessel (2) at the top of the pedestal (1),
It is fixedly installed with ultraviolet radiator (5) at the top of the lamp holder (4), the inside of the reaction vessel (2), which is fixedly installed with, is located at purple
Outside line lamp (5) external cloche (6) is fixedly installed with feeding pipe (7) at the top of the reaction vessel (2), the pedestal (1)
Top be fixedly installed with the mounting base (8) on the right side of reaction vessel (2), the internal activity of the mounting base (8) is equipped with
The outside of shaft (9), the shaft (9) is socketed with axle sleeve (10), is fixedly installed at the top of the shaft (9) positioned at mounting base
(8) movable plate (11) at the top of is fixedly installed with liquid reserve tank (12) at the top of the movable plate (11), the liquid reserve tank (12)
Outside is fixedly installed with the sealing plate (13) at the top of movable plate (11), and the inner wall right side opening of the reaction vessel (2) is equipped with
It is through to the internal plup inlet (14) of mounting base (8), the inside of the sealing plate (13) is fixedly installed with control valve (15), described
The inside of liquid reserve tank (12) is fixedly installed with partition (16), and there are two liquid-in pipes for the top fixed installation of the liquid reserve tank (12)
(17), the relatively uniform side of two liquid-in pipes (17) is fixed with exhaust tube (18), and the inside of the reaction vessel (2) is fixed
It is equipped with water cooling tube (19), exhaust pipe (20) is fixedly installed on the left of feeding pipe (7).
2. a kind of Organometallic Chemistry apparatus for photoreaction according to claim 1, it is characterised in that: the sealing plate (13)
Inside offer through-hole, the quantity of through-hole is two, and two through-holes are uniformly distributed in the left and right sides of sealing plate (13).
3. a kind of Organometallic Chemistry apparatus for photoreaction according to claim 2, it is characterised in that: the control valve (15)
Quantity be two, two control valves (15) are uniformly distributed in the inside of two through-holes.
4. a kind of Organometallic Chemistry apparatus for photoreaction according to claim 1, it is characterised in that: two liquid-in pipes
(17) valve is provided at the top of opposite side and exhaust tube (18), the quantity of valve is four.
5. a kind of Organometallic Chemistry apparatus for photoreaction according to claim 1, it is characterised in that: the shaft (9)
Bottom is provided with the limit plate internal positioned at mounting base (8), and limit plate is located at the bottom of axle sleeve (10), and the diameter of limit plate is greater than
The diameter of axle sleeve (10).
6. a kind of Organometallic Chemistry apparatus for photoreaction according to claim 1, it is characterised in that: the sealing plate (13)
Two sides up and down be provided with sealing strip, shape, the quantity of sealing strip are two to sealing strip in a ring.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201822278921.0U CN209348619U (en) | 2018-12-24 | 2018-12-24 | A kind of Organometallic Chemistry apparatus for photoreaction |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201822278921.0U CN209348619U (en) | 2018-12-24 | 2018-12-24 | A kind of Organometallic Chemistry apparatus for photoreaction |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN209348619U true CN209348619U (en) | 2019-09-06 |
Family
ID=67802272
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201822278921.0U Expired - Fee Related CN209348619U (en) | 2018-12-24 | 2018-12-24 | A kind of Organometallic Chemistry apparatus for photoreaction |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN209348619U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110596004A (en) * | 2019-09-17 | 2019-12-20 | 天津大学 | Novel photoreactor and use method thereof |
-
2018
- 2018-12-24 CN CN201822278921.0U patent/CN209348619U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110596004A (en) * | 2019-09-17 | 2019-12-20 | 天津大学 | Novel photoreactor and use method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN209348619U (en) | A kind of Organometallic Chemistry apparatus for photoreaction | |
| CN106198196A (en) | A kind of environment simulator for Corrosion Fatigue Properties test | |
| CN213951020U (en) | Compost reaction system | |
| CN207440046U (en) | Deoxygenation liquid dispensing device | |
| CN212159500U (en) | Box-type pipe network biofilm growth simulation device | |
| CN214916344U (en) | A laboratory storage rack for depositing liquid sample | |
| CN216784511U (en) | Storage tank for storing hydrochloric acid | |
| CN211645199U (en) | Microorganism constant temperature culture ware | |
| CN214141779U (en) | Laboratory is with water treatment aeration reactor | |
| CN209651029U (en) | A kind of recyclable device of good airproof performance | |
| CN213913835U (en) | Chemical reagent storage device | |
| CN206601324U (en) | A kind of hydrogen induced cracking (HIC) HIC test chambers | |
| CN215353461U (en) | Parallel synthesis reaction instrument with efficient backflow function | |
| CN215446987U (en) | Low-temperature storage module | |
| CN218969210U (en) | Gas replacement device | |
| CN206027678U (en) | Simply install with photocatalysis in laboratory | |
| JP6339804B2 (en) | Incubator | |
| CN220894269U (en) | Leaching radon measuring device | |
| CN217977699U (en) | Kettle bottom temperature measurement discharging ball valve | |
| CN220181664U (en) | Bromination product storage tank | |
| CN205958431U (en) | Negative pressure draining system | |
| CN218232540U (en) | Auxiliary material exhaust device and auxiliary material conveying system of annular carburizing furnace for heat treatment | |
| CN204933492U (en) | Chemistry experiment box | |
| CN212254750U (en) | Multifunctional water quality fixative feeding box | |
| CN219326864U (en) | Electroplating agent adding device for electroplating pool processing |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20190906 Termination date: 20201224 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |