CN209333250U - A kind of organic synthesis extraction equipment - Google Patents

A kind of organic synthesis extraction equipment Download PDF

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Publication number
CN209333250U
CN209333250U CN201822166813.4U CN201822166813U CN209333250U CN 209333250 U CN209333250 U CN 209333250U CN 201822166813 U CN201822166813 U CN 201822166813U CN 209333250 U CN209333250 U CN 209333250U
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CN
China
Prior art keywords
wall
bull stick
tank body
organic synthesis
extraction equipment
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201822166813.4U
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Chinese (zh)
Inventor
贾贞
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Dezhou University
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Dezhou University
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Filing date
Publication date
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Priority to CN201822166813.4U priority Critical patent/CN209333250U/en
Application granted granted Critical
Publication of CN209333250U publication Critical patent/CN209333250U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model discloses a kind of organic synthesis extraction equipments, including pedestal, the top exterior walls quadrangle of the pedestal is provided with bracket, and the other end of bracket is provided with the same tank body, the top exterior walls of the tank body are provided with rotating electric machine, and the output shaft of rotating electric machine is connected with the first bull stick by shaft coupling, the outer wall of first bull stick has been equidistantly positioned the first stirring rod, the inner wall of the tank body is provided with concave block close to one end two sides of bottom, and the inner wall of two concave blocks passes through bearing and is rotatably connected to same second bull stick, the outer wall of second bull stick is symmetrically connected with the second stirring rod by bolt, second bull stick and the first bull stick opposite side are provided with conical tooth, and it is intermeshed between two conical tooths.The utility model can adequately be stirred by the first stirring rod and the second stirring rod, there is the benefit for accelerating extraction efficiency, convenient for being rinsed after the completion of extraction to inner tank wall.

Description

A kind of organic synthesis extraction equipment
Technical field
The utility model relates to technical field of organic synthesis more particularly to a kind of organic synthesis extraction equipments.
Background technique
Extraction is to make substance from one using substance solubility or difference of distribution coefficient in two kinds of immiscible solvents It is transferred in another solvent in kind solvent.Extraction is to be used to purify the means with purifying compound in Organic Chemistry Laboratory One of.By extraction, required substance can be extracted from solid or liquid mixture.Extraction does not cause extracted substance The change of chemical component, so extracting operation is a physical process.
During organic synthesis, extraction equipment can be usually used, but existing organic synthesis-extraction device is most Structure is relatively simple, and extraction efficiency is not high, and after the completion of extraction, is not easy to clean inner tank wall, actually use There are certain inconveniences in journey.
Utility model content
Purpose of the utility model is to solve disadvantages existing in the prior art, and a kind of organic synthesis proposed is used Extraction equipment.
To achieve the goals above, the utility model adopts the technical scheme that
The top exterior walls quadrangle of a kind of organic synthesis extraction equipment, including pedestal, the pedestal is provided with bracket, and The other end of bracket is provided with the same tank body, and the top exterior walls of the tank body are provided with rotating electric machine, and rotating electric machine Output shaft is connected with the first bull stick by shaft coupling, and the outer wall of first bull stick has been equidistantly positioned the first stirring rod, described The inner wall of tank body is provided with concave block close to one end two sides of bottom, and the inner wall of two concave blocks is rotatably connected to by bearing Same second bull stick, the outer wall of second bull stick are symmetrically connected with the second stirring rod by bolt, second bull stick and First bull stick opposite side is provided with conical tooth, and is intermeshed between two conical tooths, the bottom outer wall two of the tank body Side is provided with installing port, and the inner wall of two installing ports is respectively arranged with feeder pipe and drainpipe, the feeder pipe and drainpipe Outer wall be connected through a screw thread the first sealing valve and the second sealing valve respectively.
Preferably, the tank body includes lagging casing and inner panel, and the opposite side of inner panel is provided with mounting groove.
Preferably, the inner wall of the mounting groove is provided with resistance heating wire, and inner panel is equal close to the side of resistance heating wire It is provided with heat-conducting plate.
Preferably, the side outer wall of the heat-conducting plate has been equidistantly positioned convex block, and the side of tank body is provided with feed inlet, into The inner wall of material mouth is provided with loading hopper.
Preferably, the top exterior walls of the pedestal are provided with water tank, and water tank is located at the underface of drainpipe, the top of pedestal Portion's outer wall is provided with water pump close to the side of water tank.
Preferably, the input terminal of the water pump is connected with water tank, and the output end of water pump is provided with water supplying pipe.
Preferably, the inner wall of the tank body is provided with annular conduit close to the one end at top, and the side of annular conduit with Water supplying pipe is connected, and the surrounding outer wall of annular conduit is equidistant to be provided with hole for water spraying, and the side outer wall of tank body is provided with observation window.
Compared with prior art, the utility model provides a kind of organic synthesis extraction equipment, has following beneficial to effect Fruit:
1. the organic synthesis extraction equipment can drive the first bull stick by conical tooth by the rotating electric machine of setting It with the second bar rotation, is adequately stirred by the first stirring rod and the second stirring rod, there is the benefit for accelerating extraction efficiency.
2. the organic synthesis extraction equipment can be heated, energy by the resistance heating wire of setting by heat-conducting plate The efficiency for enough further increasing extraction can increase the heat-conducting area of heat-conducting plate, raising is led by being provided with convex block in heat-conducting plate The heating conduction of hot plate.
3. the organic synthesis extraction equipment is convenient for after the completion of extraction, to inner tank wall by the annular conduit of setting It is rinsed, and circulation flushing is realized by drainpipe, there is saving water resource, increase the benefit of device practicability.
It is not directed to part in the device to be the same as those in the prior art or can be realized by using the prior art, the utility model It can be improved the efficiency of extraction, inner tank wall can be rinsed after the completion of extraction.
Detailed description of the invention
Fig. 1 be the utility model proposes a kind of organic synthesis extraction equipment overall structure diagram;
Fig. 2 be the utility model proposes a kind of organic synthesis extraction equipment tank body schematic cross-sectional view;
Fig. 3 be the utility model proposes a kind of organic synthesis extraction equipment annular conduit structural schematic diagram.
In figure: 1- pedestal, 2- feeder pipe, the second sealing valve of 3-, 4- water tank, 5- water pump, 6- water supplying pipe, 7- drainpipe, 8- Bracket, 9- conical tooth, the first bull stick of 10-, 11- annular conduit, 12- hole for water spraying, 13- rotating electric machine, 14- loading hopper, 15- first Stirring rod, the second bull stick of 16-, the second stirring rod of 17-, 18- tank body, the first sealing valve of 19-, 20- inner panel, 21- lagging casing, 22- convex block, 23- heat-conducting plate, 24- resistance heating wire.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole Embodiment.
In the description of the present invention, it should be understood that term " on ", "lower", "front", "rear", "left", "right", The orientation or positional relationship of the instructions such as "top", "bottom", "inner", "outside" is to be based on the orientation or positional relationship shown in the drawings, and is only For ease of description the utility model and simplify description, rather than the device or element of indication or suggestion meaning must have it is specific Orientation, be constructed and operated in a specific orientation, therefore should not be understood as limiting the present invention.
Referring to Fig.1-3, it welds the top exterior walls quadrangle of a kind of organic synthesis extraction equipment, including pedestal 1, pedestal 1 There is bracket 8, and the other end of bracket 8 is welded with the same tank body 18, the top exterior walls of tank body 18 have been bolted rotation Rotating motor 13, and the output shaft of rotating electric machine 13 is connected with the first bull stick 10 by shaft coupling, the outer wall of the first bull stick 10 is equidistant From the first stirring rod 15 has been bolted, the inner wall of tank body 18 has been bolted recessed close to one end two sides of bottom Block, and the inner wall of two concave blocks passes through bearing and is rotatably connected to same second bull stick 16, the outer wall of the second bull stick 16 passes through Bolt is symmetrically connected with the second stirring rod 17, and the second bull stick 16 and 10 opposite side of the first bull stick pass through screw and be fixed with taper Tooth 9, and be intermeshed between two conical tooths 9, start rotating electric machine 13,10 He of the first bull stick can be driven by conical tooth 9 The rotation of second bull stick 16, is adequately stirred by the first stirring rod 15 and the second stirring rod 17, accelerates rate of extraction, tank body 18 bottom outer wall two sides are provided with installing port, and the inner wall of two installing ports has been bolted feeder pipe 2 and row respectively The outer wall of water pipe 7, feeder pipe 2 and drainpipe 7 has been connected through a screw thread the first sealing valve 19 and the second sealing valve 3 respectively.
In the utility model, tank body 18 includes lagging casing 21 and inner panel 20, and the opposite side of inner panel 20 is provided with peace Tankage.
The inner wall of mounting groove is fixed with resistance heating wire 24 by screw, and inner panel 20 is close to the side of resistance heating wire 24 It is bolted heat-conducting plate 23, start-up resistor heater strip 24 can be heated by heat-conducting plate 23, be further increased The efficiency of extraction.
The side outer wall of heat-conducting plate 23 is equidistant to be welded with convex block 22, can by being provided with convex block 22 in heat-conducting plate 23 Increase the heat-conducting area of heat-conducting plate 23, improves the heating conduction of heat-conducting plate 23, and the side of tank body 18 is provided with feed inlet, feed inlet Inner wall loading hopper 14 is fixed with by screw.
The top exterior walls of pedestal 1 are fixed with water tank 4 by screw, and water tank 4 is located at the underface of drainpipe 7, pedestal 1 Top exterior walls have been bolted water pump 5 close to the side of water tank 4.
The input terminal of water pump 5 is connected with water tank 4, and the output end of water pump 5 is fixed with water supplying pipe 6 by screw.
The inner wall of tank body 18 has been bolted annular conduit 11, and the side of annular conduit 11 close to the one end at top It is connected with water supplying pipe 6, starting water pump 5 can be rinsed 18 inner wall of tank body by annular conduit 11, and the second sealing is opened Valve 3 realizes circulation flushing by drainpipe 7, and the surrounding outer wall of annular conduit 11 is equidistant to be provided with hole for water spraying 12, the one of tank body 18 Side outer wall is provided with observation window.
Working principle: in use, solution and extractant are added into tank body 18 by loading hopper 14, start rotating electric machine 13, drive the first bull stick 10 and the second bull stick 16 to rotate by conical tooth 9, by the first stirring rod 15 and the second stirring rod 17 into Row adequately stirring, accelerates rate of extraction, and start-up resistor heater strip 24 is heated by heat-conducting plate 23, further increases extraction Efficiency, after the completion of stirring, close rotating electric machine 13, be layered solution left standstill, and by observation window observe, extraction completion Afterwards, starting water pump 5 is rinsed 18 inner wall of tank body by annular conduit 11, opens the second sealing valve 3, real by drainpipe 7 Existing circulation flushing.
The preferable specific embodiment of the above, only the utility model, but the protection scope of the utility model is not It is confined to this, anyone skilled in the art is within the technical scope disclosed by the utility model, practical according to this Novel technical solution and its utility model design are subject to equivalent substitution or change, should all cover the protection model in the utility model Within enclosing.

Claims (7)

1. a kind of organic synthesis extraction equipment, including pedestal (1), which is characterized in that the top exterior walls quadrangle of the pedestal (1) It is provided with bracket (8), and the other end of bracket (8) is provided with the same tank body (18), outside the top of the tank body (18) Wall is provided with rotating electric machine (13), and the output shaft of rotating electric machine (13) is connected with the first bull stick (10) by shaft coupling, described The outer wall of first bull stick (10) has been equidistantly positioned the first stirring rod (15), the one end of the inner wall of the tank body (18) close to bottom Two sides are provided with concave block, and the inner wall of two concave blocks passes through bearing and is rotatably connected to same second bull stick (16), described The outer wall of second bull stick (16) is symmetrically connected with the second stirring rod (17) by bolt, second bull stick (16) and the first bull stick (10) opposite side is provided with conical tooth (9), and is intermeshed between two conical tooths (9), the bottom of the tank body (18) Outer wall two sides are provided with installing port, and the inner wall of two installing ports is respectively arranged with feeder pipe (2) and drainpipe (7), under described The outer wall of expects pipe (2) and drainpipe (7) has been connected through a screw thread the first sealing valve (19) and the second sealing valve (3) respectively.
2. a kind of organic synthesis extraction equipment according to claim 1, which is characterized in that the tank body (18) includes protecting Warm shell (21) and inner panel (20), and the opposite side of inner panel (20) is provided with mounting groove.
3. a kind of organic synthesis extraction equipment according to claim 2, which is characterized in that the inner wall of the mounting groove is set It is equipped with resistance heating wire (24), and inner panel (20) is provided with heat-conducting plate (23) close to the side of resistance heating wire (24).
4. a kind of organic synthesis extraction equipment according to claim 3, which is characterized in that the one of the heat-conducting plate (23) Side outer wall has been equidistantly positioned convex block (22), and the side of tank body (18) is provided with feed inlet, and the inner wall of feed inlet is provided with charging It struggles against (14).
5. a kind of organic synthesis extraction equipment according to claim 4, which is characterized in that the top of the pedestal (1) Outer wall is provided with water tank (4), and water tank (4) is located at the underface of drainpipe (7), and the top exterior walls of pedestal (1) are close to water tank (4) Side be provided with water pump (5).
6. a kind of organic synthesis extraction equipment according to claim 5, which is characterized in that the input of the water pump (5) End is connected with water tank (4), and the output end of water pump (5) is provided with water supplying pipe (6).
7. a kind of organic synthesis extraction equipment according to claim 6, which is characterized in that the inner wall of the tank body (18) One end close to top is provided with annular conduit (11), and the side of annular conduit (11) is connected with water supplying pipe (6), annular water The surrounding outer wall of pipe (11) is equidistant to be provided with hole for water spraying (12), and the side outer wall of tank body (18) is provided with observation window.
CN201822166813.4U 2018-12-24 2018-12-24 A kind of organic synthesis extraction equipment Expired - Fee Related CN209333250U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201822166813.4U CN209333250U (en) 2018-12-24 2018-12-24 A kind of organic synthesis extraction equipment

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201822166813.4U CN209333250U (en) 2018-12-24 2018-12-24 A kind of organic synthesis extraction equipment

Publications (1)

Publication Number Publication Date
CN209333250U true CN209333250U (en) 2019-09-03

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201822166813.4U Expired - Fee Related CN209333250U (en) 2018-12-24 2018-12-24 A kind of organic synthesis extraction equipment

Country Status (1)

Country Link
CN (1) CN209333250U (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111036116A (en) * 2019-12-16 2020-04-21 株洲蓝海包装有限公司 Liquid laundry is compounding device for lapping
CN111778105A (en) * 2020-06-21 2020-10-16 曹国行 Plant essential oil extraction processingequipment
CN112044112A (en) * 2020-07-27 2020-12-08 董金玉 Chinese-medicinal material extraction equipment
CN113750568A (en) * 2021-09-26 2021-12-07 臻顺(南京)工业设备有限公司 Extraction barrel convenient to clean and cleaning method thereof

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111036116A (en) * 2019-12-16 2020-04-21 株洲蓝海包装有限公司 Liquid laundry is compounding device for lapping
CN111778105A (en) * 2020-06-21 2020-10-16 曹国行 Plant essential oil extraction processingequipment
CN112044112A (en) * 2020-07-27 2020-12-08 董金玉 Chinese-medicinal material extraction equipment
CN113750568A (en) * 2021-09-26 2021-12-07 臻顺(南京)工业设备有限公司 Extraction barrel convenient to clean and cleaning method thereof

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CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20190903

Termination date: 20201224