CN209317682U - A kind of dedicated reaction kettle of liquid-solid reaction - Google Patents
A kind of dedicated reaction kettle of liquid-solid reaction Download PDFInfo
- Publication number
- CN209317682U CN209317682U CN201822237639.8U CN201822237639U CN209317682U CN 209317682 U CN209317682 U CN 209317682U CN 201822237639 U CN201822237639 U CN 201822237639U CN 209317682 U CN209317682 U CN 209317682U
- Authority
- CN
- China
- Prior art keywords
- blade
- autoclave body
- agitating unit
- helical
- ribbon type
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Landscapes
- Mixers Of The Rotary Stirring Type (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The utility model proposes a kind of dedicated reaction kettles of liquid-solid reaction, including heating tank, autoclave body, motor, agitating shaft, the first agitating unit, the second agitating unit and discharging structure；Autoclave body is set in heating tank, and the bottom surface of autoclave body is funnel structure；Agitating shaft is sequentially equipped with the first agitating unit and the second agitating unit from top to bottom；First agitating unit includes cross blade, U-shaped blade, the first helical-ribbon type blade and the second helical-ribbon type blade；Second agitating unit includes cross bar and several vertical bars for being welded in below cross bar, and the free end of vertical bar is inclined-plane, and the plane where each inclined-plane is parallel with funnel structure；The bottom end of autoclave body is fixedly connected with discharging structure, and discharging structure top is equipped with a partition, and discharging structure is divided into upper and bottom section by pull plate, and the inner wall of upper part is equipped with drain pipe.The included filtering of the utility model, drying and crushing function, and mixing effect is good, significantly reduces the loss of material.
Description
Technical field
The utility model belongs to chemical and medicine industry process units technical field, particularly relates to a kind of dedicated reaction of liquid-solid reaction
Kettle.
Background technique
There are mixing effect differences when carrying out a variety of liquid-solid reactions including spirolactone synthesis for existing reaction kettle
Defect, and need product being transferred to centrifugation apparatus after the reaction was completed and dry, followed by being dried, crushed etc.
Reason.So many processing needs carry out in different devices, and not only process is cumbersome, but also material loss is big.Therefore, have very much
Necessity improves the prior art, to solve above-mentioned shortcoming.
Utility model content
To solve the above the deficiencies in the prior art, the utility model proposes a kind of dedicated reaction kettles of liquid-solid reaction.
The technical solution of the utility model is achieved in that
A kind of dedicated reaction kettle of liquid-solid reaction, including heating tank, autoclave body, motor, agitating shaft, the first agitating unit,
Two agitating units and discharging structure；
Autoclave body is set in heating tank, and closed heating chamber is formed between the outer wall of autoclave body and the inner wall of heating tank, autoclave body
Top is equipped with liquid material feed inlet, exhaust outlet and solid material feed inlet, and the bottom end of autoclave body is funnel structure；
Motor is fixed on the top of autoclave body, and motor is by motor shaft and is set to the intracorporal stirring axis connection of kettle；
Agitating shaft is sequentially equipped with the first agitating unit and the second agitating unit from top to bottom；
First agitating unit includes cross blade, U-shaped blade, the first helical-ribbon type blade and the second helical-ribbon type blade, and first
Helical-ribbon type blade and the second helical-ribbon type blade are respectively welded in cross blade and U-shaped blade between farther away both ends, and first
Helical-ribbon type blade and the second helical-ribbon type blade are centrosymmetric, and are respectively provided with and stir in the middle part of cross blade and U shape blade
Mix the cross blade installation wheel hub and U-shaped blade installation wheel hub of axis connection；
Second agitating unit includes cross bar and several vertical bars for being welded in below cross bar, and the free end of vertical bar is oblique
Face, the plane where each inclined-plane is parallel with funnel structure, and the middle part of cross bar is equipped with for the second stirring with stirring axis connection
Unit installs wheel hub；
The bottom end of autoclave body is threaded with discharging structure, discharging structure end sealing, bottom end opening, close on the end face on top
Cloth liquid drain hole then forms a filter screen passed through for liquid material, one partition of discharging structure top, and partition is by discharging structure
It is divided into upper and bottom section, drain pipe is connected on upper part, one end that drain pipe is connect with upper part is equipped with valve body.
Preferably, the length of cross blade is identical as the opening width of U-shaped blade, the first helical-ribbon type blade and the second ribbon
The screw pitch of formula blade is identical.
It is further preferred that the diameter of 0.5-0.8 times of autoclave body of the length of cross blade, 1-1.5 times of screw pitch lateral leaf
The length of piece.
More preferably, outsides cover of electric machinery is equipped with motor cover.
Compared with prior art, the utility model structure is simple, design science, rationally distributed, carries filtering, drying and powder
Broken function, and mixing effect is good, reaction solution can be made to be sufficiently mixed, and helps to improve reaction effect, improves reaction yield, reduces
The loss of material.
Detailed description of the invention
In order to illustrate the embodiment of the utility model or the technical proposal in the existing technology more clearly, below will be to embodiment
Or attached drawing needed to be used in the description of the prior art is briefly described, it should be apparent that, the accompanying drawings in the following description is only
It is some embodiments of the utility model, for those of ordinary skill in the art, before not making the creative labor property
It puts, is also possible to obtain other drawings based on these drawings.
Fig. 1 is the structural schematic diagram of the utility model.
In figure: 1, heating tank；11, stabilizer blade；2, autoclave body；21, liquid material feed inlet；22, exhaust outlet；23, solid material
Feed inlet；24, funnel structure；3, motor；31, motor shaft；32, motor cover；4, agitating shaft；5, the first agitating unit；51, horizontal
To blade；511, cross blade installs wheel hub；52, U-shaped blade；521, U-shaped blade installs wheel hub；53, the first helical-ribbon type leaf
Piece；54, the second helical-ribbon type blade；6, the second agitating unit；61, cross bar；62, vertical bar；7, discharging structure；71, partition；72, it arranges
Liquid pipe.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model
Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole
Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without creative efforts
Every other embodiment obtained, fall within the protection scope of the utility model.
The dedicated reaction kettle of a kind of liquid-solid reaction as shown in Figure 1:, including heating tank 1, autoclave body 2, motor 3, agitating shaft 4,
One agitating unit 5, the second agitating unit 6 and discharging structure 7；
At least 2/3rds parts of autoclave body 2 are set in heating tank 1, and the bottom of heating tank 1 is equipped with stabilizer blade 11, autoclave body 2
Closed heating chamber is formed between outer wall and the inner wall of heating tank 1, the top of autoclave body 2 is equipped with liquid material feed inlet 21, exhaust
Mouth 22 and solid material feed inlet 23, the bottom end of autoclave body 2 are funnel structure 24；
Motor 3 is fixed on the top of autoclave body 2, and motor cover 32 is covered with outside motor 3, and motor 3 passes through motor shaft 31 and is set to
Agitating shaft 4 in autoclave body 1 connects；
Agitating shaft 4 is sequentially equipped with the first agitating unit 5 and the second agitating unit 6 from top to bottom；
First agitating unit 5 includes cross blade 51, U-shaped blade 52, the first helical-ribbon type blade 53 and the second helical-ribbon type leaf
Piece 54, the first helical-ribbon type blade 53 and the second helical-ribbon type blade 54 be respectively welded in cross blade 51 and 52 distance of U-shaped blade compared with
Between remote both ends, the first helical-ribbon type blade 53 and the second helical-ribbon type blade 54 are centrosymmetric, cross blade 51 and U-shaped blade
52 middle part is respectively provided with the cross blade installation wheel hub 511 connecting with agitating shaft 4 and U-shaped blade installation wheel hub 521,
It is bolted between cross blade installation wheel hub 511, U-shaped blade installation wheel hub 521 and agitating shaft 4；Cross blade 51
Length is identical as the opening width of U shape blade 52, and the first helical-ribbon type blade 53 is identical with the screw pitch of the second helical-ribbon type blade 54；
The diameter of 0.5-0.8 times of autoclave body of length 2 of cross blade 51, the length of 1-1.5 times of cross blade of screw pitch 51, first stirs
It mixes unit 5 and has both anchoring component and horizontal slurry structure, can satisfy stirring requirement when different viscosities, it can be in kettle in whipping process
Large range of Matter Transfer is formed in body 2, the first helical-ribbon type blade 53 and the second helical-ribbon type blade 54 can be upward material
It is promoted, to form macroscopic view flowing on a large scale in reaction kettle, the mixing effect of this reaction kettle is best under above-mentioned technical parameter；
Second agitating unit 6 includes cross bar 61 and several vertical bars 62 for being welded in 61 lower section of cross bar, the freedom of vertical bar 62
End is inclined-plane, and the plane where each inclined-plane is parallel with funnel structure 24, and the middle part of cross bar 61 is equipped with for connecting with agitating shaft 4
The the second agitating unit installation wheel hub connect, is bolted between the second agitating unit installation wheel hub and agitating shaft 4, has reacted
Autoclave body 2 is discharged via drain pipe 72 at rear liquid material, the solid material in autoclave body 2 is concentrated under the heat effect of heating tank 1,
Dry, the second agitating unit 6 can stir material in the process, prevent the drying process for agglomerating and accelerating material,
The free end of vertical bar 62 is inclined-plane, can also be crushed to material；
The bottom end of autoclave body 2 is threaded with discharging structure 7, and the free end of discharging structure 7 is arranged vacantly in stabilizer blade 11, out
Expect 7 end sealing of structure, bottom end opening, the liquid drain hole that gathers on the end face on top then forms one and is used for the mistake that liquid material passes through
Screen, 7 top of discharging structure are equipped with a partition 71, and discharging structure 7 is divided into upper and bottom section by partition 71, on upper part
It is connected with drain pipe 72, one end that drain pipe 72 is connect with upper part is equipped with valve body.
Working principle: the required liquid material of reaction is passed through liquid material feed inlet 21 with solid material respectively and consolidated
State material feed inlet 23 is added in autoclave body 2, opens heating tank 1 and motor 3 later, and motor 3 drives the rotation of agitating shaft 4 then to drive
First agitating unit 5 and the second agitating unit 6 are stirred, and to close heating tank 1 and motor 3 after reaction, pass through drain
Pipe (one end that drain pipe connect with upper cavity 71 equipped with solenoid valve or hand-operated valve) by the liquid material discharge after reaction, it is subsequent
It is continuous to open heating tank 1 and motor 3, product is dried and is crushed under stirring.Finally, unloading discharging structure 7
Collect solid material.
The above is only the preferred embodiment of the utility model only, is not intended to limit the utility model, all at this
Within the spirit and principle of utility model, any modification, equivalent replacement, improvement and so on should be included in the utility model
Protection scope within.
Claims (4)
1. a kind of dedicated reaction kettle of liquid-solid reaction, it is characterised in that: including heating tank (1), autoclave body (2), motor (3), stirring
Axis (4), the first agitating unit (5), the second agitating unit (6) and discharging structure (7)；
Autoclave body (2) is set in heating tank (1), forms closed heating between the outer wall of autoclave body (2) and the inner wall of heating tank (1)
The top of chamber, autoclave body (2) is equipped with liquid material feed inlet (21), exhaust outlet (22) and solid material feed inlet (23), autoclave body (2)
Bottom end be funnel structure (24)；
Motor (3) is fixed on the top of autoclave body (2), and motor (3) passes through motor shaft (31) and the agitating shaft in autoclave body (2)
(4) it connects；
Agitating shaft (4) is sequentially equipped with the first agitating unit (5) and the second agitating unit (6) from top to bottom；
First agitating unit (5) includes cross blade (51), U-shaped blade (52), the first helical-ribbon type blade (53) and the second ribbon
Formula blade (54), the first helical-ribbon type blade (53) and the second helical-ribbon type blade (54) are respectively welded in cross blade (51) and U-shaped
Between farther away both ends, the first helical-ribbon type blade (53) and the second helical-ribbon type blade (54) are centrosymmetric blade (52),
The cross blade installation wheel hub connecting with agitating shaft (4) is respectively provided in the middle part of cross blade (51) and U-shaped blade (52)
(511) and U-shaped blade installs wheel hub (521)；
Second agitating unit (6) includes cross bar (61) and several vertical bars (62) being welded in below cross bar (61), vertical bar (62)
Free end be inclined-plane, the plane where each inclined-plane is parallel with funnel structure (24), and the middle part of cross bar (61) is equipped with
The second agitating unit for connecting with agitating shaft (4) installs wheel hub；
The bottom end of autoclave body (2) is threaded with discharging structure (7), discharging structure (7) end sealing, bottom end opening, the top
End face on the liquid drain hole that gathers then form a filter screen passed through for liquid material, discharging structure (7) top be equipped with one every
Discharging structure (7) is divided into upper and bottom section, is connected with drain pipe on the upper part by plate (71), partition (71)
(72), one end that drain pipe (72) is connect with the upper part is equipped with valve body.
2. the dedicated reaction kettle of liquid-solid reaction according to claim 1, it is characterised in that: the length of cross blade (51) with
The opening width of U-shaped blade (52) is identical, and the first helical-ribbon type blade (53) is identical with the screw pitch of the second helical-ribbon type blade (54).
3. the dedicated reaction kettle of liquid-solid reaction according to claim 2, it is characterised in that: the length of cross blade (51)
The diameter of 0.5-0.8 times of autoclave body (2), the length of 1-1.5 times of cross blade of the screw pitch (51).
4. the dedicated reaction kettle of liquid-solid reaction according to claim 3, it is characterised in that: be covered with motor outside motor (3)
It covers (32).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201822237639.8U CN209317682U (en) | 2018-12-28 | 2018-12-28 | A kind of dedicated reaction kettle of liquid-solid reaction |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201822237639.8U CN209317682U (en) | 2018-12-28 | 2018-12-28 | A kind of dedicated reaction kettle of liquid-solid reaction |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN209317682U true CN209317682U (en) | 2019-08-30 |
Family
ID=67729583
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201822237639.8U Active CN209317682U (en) | 2018-12-28 | 2018-12-28 | A kind of dedicated reaction kettle of liquid-solid reaction |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN209317682U (en) |
-
2018
- 2018-12-28 CN CN201822237639.8U patent/CN209317682U/en active Active
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN209155729U (en) | A kind of agitating device for starch-based product production | |
| CN108905918A (en) | A kind of staggered form quickly mixes and convenient for quantitative chemical industry reaction kettle | |
| CN209566394U (en) | A kind of plastic melt equipment with filter structure | |
| CN206715715U (en) | One kind bakees syrup dedicated production agitating device | |
| CN207614845U (en) | A kind of multi-functional degumming retort | |
| CN209317682U (en) | A kind of dedicated reaction kettle of liquid-solid reaction | |
| CN203540408U (en) | Burdening agitation tank | |
| CN211026292U (en) | Reation kettle for fine chemistry industry | |
| CN108654476A (en) | Pharmaceutical engineering processing mixing equipment | |
| CN107159079A (en) | A kind of multi-functional chemical industry equipment for preparing industrial chemicals | |
| CN210993892U (en) | A agitating unit for instant agar production | |
| CN108311080A (en) | A kind of efficient chemical industry feed liquid centrifugation reaction kettle | |
| CN205182715U (en) | Smash chemical industry reation kettle that powder ground stirring to pieces | |
| CN108159944A (en) | A kind of efficient raw material of industry stirring humidifying pot that can be crushed | |
| CN209423538U (en) | A kind of feeding device of agent of non-phosphate degreasing blender | |
| CN209576650U (en) | A kind of hydrogen chloride detects filtering conveying device automatically | |
| CN208824479U (en) | A kind of centrifugal mixing reactor of chemical industry | |
| CN209116726U (en) | A kind of cone type bottom filtration type filter scrubbing-and-drying unit | |
| CN209722025U (en) | A kind of recover the oil uses profile control agent dispersion agent process units | |
| CN217490468U (en) | Degradable tableware production proportioning machine | |
| CN219559589U (en) | A reation kettle for separating free alcohol in lanolin | |
| CN201316617Y (en) | Barrel-roll type reaction pot | |
| CN211800197U (en) | Chemical raw material stirring device | |
| CN215783289U (en) | Polypeptide synthesis reaction tank | |
| CN109011694A (en) | A kind of novel energy-conserving composite stirring extraction tower |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CP01 | Change in the name or title of a patent holder |
Address after: 300380 Zhangjiawo Industrial Zone, Xiqing Economic Development Zone, Xiqing District, Tianjin Patentee after: Tianjin Xinyi Jinjin Pharmaceutical Co.,Ltd. Address before: 300380 Zhangjiawo Industrial Zone, Xiqing Economic Development Zone, Xiqing District, Tianjin Patentee before: TIANJIN JINJIN PHARMACEUTICAL Co.,Ltd. |
|
| CP01 | Change in the name or title of a patent holder |