CN209302740U - A kind of reactor tank convenient for cleaning producing thiophen acetyl chloride - Google Patents
A kind of reactor tank convenient for cleaning producing thiophen acetyl chloride Download PDFInfo
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- CN209302740U CN209302740U CN201821712052.1U CN201821712052U CN209302740U CN 209302740 U CN209302740 U CN 209302740U CN 201821712052 U CN201821712052 U CN 201821712052U CN 209302740 U CN209302740 U CN 209302740U
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- reactor tank
- motor
- fixed frame
- acetyl chloride
- side wall
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Abstract
The utility model relates to a kind of reactor tanks convenient for cleaning for producing thiophen acetyl chloride, including reactor tank, feed opening is fixedly installed at the top of reactor tank, fixed frame and water pipe, motor is movably equipped with above fixed frame, L connecting rod is hinged at the top of fixed frame, fixing sleeve is equipped with ring body on motor side wall, the annular trough body with the cooperation of L connecting rod is offered in ring body, the output shaft bottom activity of motor is protruded into inside reactor tank through fixed frame, spring is arranged on output shaft side wall between motor and fixed frame, multiple paddles are fixed on the output shaft side wall protruded into inside reactor tank, movable sleeve is equipped with sleeve on output shaft side wall, sleeve lateral wall is fixedly connected with rectangular box, bolt activity is threadedly coupled through sleeve and output shaft with nut;Technical solution provided by the utility model effectively compensates for existing production thiophen acetyl chloride inner tank wall existing for reactor tank and cleans inconvenience, stirring inconvenient defect when reaction.
Description
Technical field
The utility model relates to chemical production device technical fields, and in particular to a kind of to produce being convenient for for thiophen acetyl chloride
The reactor tank of cleaning.
Background technique
Thiophen acetyl chloride is kermesinus or brown liquid, 130-135 DEG C of boiling point (12kPa), relative density 1.303, refraction
Rate 1.5504,101 DEG C of flash-point, be a kind of medicine intermediate.
2- thiophen acetyl chloride is widely used in pharmaceutical industry, is broad spectrum antibiotic cefoxitin, cefaloridine, Cefoxitin
Intermediate, structural modification is carried out to 7 one amino-cephalo-alkanoic acid of cephalosporin mother nucleus (7 one ACA), the antibacterial that drug can be improved is living
Property.In recent years, external to develop many new cephalosporin antibiotics with 2 one thiophen acetyl chlorides again, there are Cefetrizole, cephalo Buddhist nun
Special sieve and furilazone etc..It is widely answered in addition, 2 one thiophen acetyl chlorides also have in pesticide, dyestuff and other field of fine chemical
With.
In publication number CN206152795U, publication date be on May 10th, 2017 utility model patent in disclose one
Kind is convenient for the chemical material homogeneous reactor tank of cleaning, including tank body and upper cover;Tank interior is set as homogeneous chamber, top open part
It is provided with upper cover;Cleaning device is provided on upper lid;Cleaning device is by gear box, the second motor, water inlet pipe and rotation spray tray
Composition;Internal layer homogeneous current divider and outer layer homogeneous current divider are provided in homogeneous chamber;Top of the tank is connected to one end of passage;
The other end of passage and the output end of air driven pump connect;The input terminal of air driven pump is connect with feed pipe;The utility model passes through
The tank body after using is cleaned in the setting of cleaning device, uses convenient for next time;It is equal by internal layer homogeneous current divider and outer layer
The reverse rotation of matter current divider carries out high-efficient homogeneous processing to the material in tank body, convenient for the reaction of material, improves work effect
Rate;By the setting of air driven pump, realizes that automatic feed, guarantee will not be revealed during transportation, reduce the waste of raw material.
But it is inconvenient usually to there is inner tank wall cleaning in the reactor tank of existing production thiophen acetyl chloride, and stirring is not when reaction
Just defect.
Utility model content
(1) the technical issues of solving
In view of the above problems, the anti-convenient for what is cleaned of thiophen acetyl chloride is produced the utility model proposes a kind of
Answer tank.Technical solution provided by the utility model can effectively compensate for drawbacks described above to a certain extent.
(2) technical solution
In order to achieve the above purpose, the following technical solution is employed for the utility model:
A kind of reactor tank convenient for cleaning producing thiophen acetyl chloride, including reactor tank, the reactor tank top are fixed
It is provided with feed opening, fixed frame and water pipe, motor is movably equipped with above the fixed frame, L company is hinged at the top of the fixed frame
Bar, fixing sleeve is equipped with ring body on the motor side wall, and the annular trough body with L connecting rod cooperation, institute are offered in the ring body
The output shaft bottom activity for stating motor is protruded into inside the reactor tank through the fixed frame, is located at the motor and the fixation
It is arranged with spring on the output shaft side wall between frame, fixation on the output shaft side wall inside the reactor tank is protruded into and sets
There are multiple paddles, movable sleeve is equipped with sleeve on the output shaft side wall, and the sleeve lateral wall is fixedly connected with rectangular box, spiral shell
Bolt activity is threadedly coupled through the sleeve and the output shaft with nut.
Preferably, the motor is servo motor, is fixedly installed with the pump housing, and the motor and the pump on the water pipe
Body is electrically connected with external power supply.
Preferably, the both ends of the spring are respectively fixedly connected at the top of the fixed frame and the motor bottom.
Preferably, the width of the rectangular box is equal with the diameter of the reactor tank.
Preferably, multiple through-holes are offered on the paddle, it is wide that the length of the paddle is less than the rectangular box
The half of degree.
Preferably, the reaction pot sidewall is equipped with door body and discharge nozzle, and the door body and the reactor tank are hinged, described
Piston is movably equipped in discharge nozzle.
Preferably, the rectangular box bottom is fixed with shaft, and the shaft passes through between pot bottom with described react
The embedded vertical grafting of bearing.
(3) beneficial effect
Due to using above-mentioned technical solution, the beneficial effects of the utility model are:
The utility model is by adjusting bolt and nut, and whether control rectangle framework rotates together with paddle, effectively
Reduce energy consumption;Rectangular box can effectively scrape reaction top tank structure, remove the object for being attached to reaction top tank structure in time
Material, effectively compensates for defect of the existing technology.
Detailed description of the invention
In order to illustrate the embodiment of the utility model or the technical proposal in the existing technology more clearly, below will be to embodiment
Or attached drawing needed to be used in the description of the prior art is briefly described, it should be apparent that, the accompanying drawings in the following description is only
It is some embodiments of the utility model, for those of ordinary skill in the art, in the premise not made the creative labor
Under, it is also possible to obtain other drawings based on these drawings.
Fig. 1 is the cross-sectional view of the utility model;
Fig. 2 is the portion A partial enlargement structural representation;
Fig. 3 is framework and its attachment structure schematic diagram;
Fig. 4 is the structural schematic diagram of fixed frame;
Wherein:
1, reactor tank;2, feed opening;3, fixed frame;4, motor;5, L connecting rod;6, ring body;7, output shaft;8, spring;9, it stirs
Mix leaf;10, sleeve;11, rectangular box;12, bolt;13, water pipe;14, the pump housing;15, discharge nozzle;16, shaft.
Specific embodiment
It is practical new below in conjunction with this to keep the objectives, technical solutions, and advantages of the embodiments of the present invention clearer
Type embodiment, the technical scheme in the utility model embodiment is clearly and completely described.Reality based on the utility model
Example is applied, every other embodiment obtained by those of ordinary skill in the art without making creative efforts all belongs to
In the range of the utility model protection.
A kind of reactor tank convenient for cleaning producing thiophen acetyl chloride, as shown in Figs 1-4: including reactor tank 1, reactor tank
1 top is fixedly installed feed opening 2, fixed frame 3 and water pipe 13, and motor 4 is movably equipped with above fixed frame 3, is cut with scissors at the top of fixed frame 3
It is connected to L connecting rod 5, fixing sleeve is equipped with ring body 6 on 4 side wall of motor, and the annular trough body cooperated with L connecting rod 5, motor are offered in ring body
47 bottom activity of output shaft is protruded into inside reactor tank 1 through fixed frame 3, the output shaft 7 between motor 4 and fixed frame 3
It is arranged with spring 8 on side wall, multiple paddles 9,7 side of output shaft are fixed on 7 side wall of output shaft protruded into inside reactor tank 1
Movable sleeve is equipped with sleeve 10 on wall, and 10 side wall of sleeve is fixedly connected with rectangular box 11, and bolt 12 is movable through sleeve 10 and defeated
Shaft 7 is threadedly coupled with nut.
Motor 4 is servo motor, is fixedly installed with the pump housing 14 on water pipe 13, and motor 4 and the pump housing 14 are and external power supply
It is electrically connected, the both ends of spring 8 are respectively fixedly connected in the top of fixed frame 3 and 4 bottom of motor, the width of rectangular box 11 and anti-
It answers the diameter of tank 1 equal, multiple through-holes is offered on paddle 9, the length of paddle 9 is less than two points of 11 width of rectangular box
One of, 1 side wall of reactor tank is equipped with door body and discharge nozzle 15, and door body and reactor tank 1 are hinged, is movably equipped with work in discharge nozzle 15
Plug, 11 bottom of rectangular box is fixed with shaft 16, passes through the vertical grafting of embedded bearing between shaft 16 and 1 bottom of reactor tank.
4 model EDSMT-2T130-040B of motor, the pump housing 14 select commercially available common water pump, and the two is connected in parallel on external power supply
On.
When being stirred to react liquid production thiophen acetyl chloride, door body is opened, nut is backed out, removes bolt 12, opens motor 4, electricity
Machine 4 only drives paddle 9 to rotate (rectangular box 11 is static), is stirred to reaction solution, offers on paddle 9 multiple logical
Hole reduces stirring resistance, improves stirring efficiency, reduces electric energy loss.
L connecting rod 5 is taken out out of annular trough body in ring body 6, upper and lower pushing motor 4, so that motor 4 is in the vertical direction
It moves reciprocatingly, paddle 9 up and down reciprocatingly stirs in reactor tank 1, strengthens mixing effect, effectively raises reaction speed
Rate.
Door body is opened, 12 activity of bolt is threadedly coupled through sleeve 10 and output shaft 7 with nut, door body is closed, opens
Water is pumped into reactor tank 1 by the pump housing 14, the pump housing 14, opens motor 4, and motor 4 drives rectangular box 11 to rotate, rectangular box 11
Width is equal with the diameter of reactor tank 1, in 11 rotation process of rectangular box, effectively scrapes the object in addition to inner tank wall attachment
Material, paddle 9 rotates, so that cleaning solution is more fully mixed, is conducive to clean reactor tank.By L connecting rod 5 from the ring in ring body 6
It is taken out in shape groove body, upper and lower pushing motor 4, so that motor 4 moves reciprocatingly in the vertical direction, rectangular box 11 is up and down reciprocatingly
Rotation, effectively scrape in addition to be attached to 1 inner wall of reactor tank material (in this way, need not be arranged the height of rectangular box 11 with react
The height of tank 1 is equal, and design is reasonable).
Above embodiments are only to illustrate the technical solution of the utility model, rather than its limitations;Although referring to aforementioned reality
Example is applied the utility model is described in detail, those skilled in the art should understand that: it still can be to preceding
Technical solution documented by each embodiment is stated to modify or equivalent replacement of some of the technical features;And these
It modifies or replaces, the spirit and model of various embodiments of the utility model technical solution that it does not separate the essence of the corresponding technical solution
It encloses.
Claims (7)
1. a kind of reactor tank convenient for cleaning for producing thiophen acetyl chloride, it is characterised in that: described anti-including reactor tank (1)
It answers and is fixedly installed feed opening (2), fixed frame (3) and water pipe (13) at the top of tank (1), be movably equipped with above the fixed frame (3)
Motor (4), fixed frame (3) top are hinged with L connecting rod (5), and fixing sleeve is equipped with ring body (6) on motor (4) side wall, institute
The annular trough body offered in ring body with the L connecting rod (5) cooperation is stated, output shaft (7) bottom activity of the motor (4) runs through
The fixed frame (3) protrudes into the reactor tank (1) inside, described defeated between the motor (4) and the fixed frame (3)
Spring (8) are arranged on shaft (7) side wall, protrudes on the internal output shaft (7) side wall of the reactor tank (1) and is fixed with
Multiple paddles (9), movable sleeve is equipped with sleeve (10), sleeve (10) side wall and rectangle frame on output shaft (7) side wall
Body (11) is fixedly connected, and bolt (12) activity is threadedly coupled through the sleeve (10) and the output shaft (7) with nut.
2. the reactor tank convenient for cleaning of production thiophen acetyl chloride according to claim 1, which is characterized in that the electricity
Machine (4) is servo motor, is fixedly installed with the pump housing (14) on the water pipe (13), and the motor (4) and the pump housing (14)
It is electrically connected with external power supply.
3. the reactor tank convenient for cleaning of production thiophen acetyl chloride according to claim 1, which is characterized in that the bullet
The both ends of spring (8) are respectively fixedly connected at the top of the fixed frame (3) and the motor (4) bottom.
4. the reactor tank convenient for cleaning of production thiophen acetyl chloride according to claim 1, which is characterized in that the square
The width of shape framework (11) is equal with the diameter of the reactor tank (1).
5. the reactor tank convenient for cleaning of production thiophen acetyl chloride according to claim 1, which is characterized in that described to stir
Mix and offer multiple through-holes on leaf (9), the length of the paddle (9) be less than the rectangular box (11) width two/
One.
6. the reactor tank convenient for cleaning of production thiophen acetyl chloride according to claim 1, which is characterized in that described anti-
Answer tank (1) side wall to be equipped with door body and discharge nozzle (15), the door body and the reactor tank (1) hingedly, the discharge nozzle (15)
Inside it is movably equipped with piston.
7. the reactor tank convenient for cleaning of production thiophen acetyl chloride according to claim 1, which is characterized in that the square
Shape framework (11) bottom is fixed with shaft (16), by embedding axis between the shaft (16) and the reactor tank (1) bottom
Hold vertical grafting.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201821712052.1U CN209302740U (en) | 2018-10-22 | 2018-10-22 | A kind of reactor tank convenient for cleaning producing thiophen acetyl chloride |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201821712052.1U CN209302740U (en) | 2018-10-22 | 2018-10-22 | A kind of reactor tank convenient for cleaning producing thiophen acetyl chloride |
Publications (1)
Publication Number | Publication Date |
---|---|
CN209302740U true CN209302740U (en) | 2019-08-27 |
Family
ID=67671379
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201821712052.1U Active CN209302740U (en) | 2018-10-22 | 2018-10-22 | A kind of reactor tank convenient for cleaning producing thiophen acetyl chloride |
Country Status (1)
Country | Link |
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CN (1) | CN209302740U (en) |
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2018
- 2018-10-22 CN CN201821712052.1U patent/CN209302740U/en active Active
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GR01 | Patent grant | ||
GR01 | Patent grant | ||
TR01 | Transfer of patent right |
Effective date of registration: 20210506 Address after: 222523 duigougang Town, Guannan County, Lianyungang City, Jiangsu Province (Chemical Industrial Park) Patentee after: JIANGSU DIPU TECHNOLOGY Co.,Ltd. Address before: 222523 No.17, Weisan Road, chemical industry park, duigougang Town, Guannan County, Lianyungang City, Jiangsu Province Patentee before: LIANYUNGANG HONGYE CHEMICAL Co.,Ltd. |
|
TR01 | Transfer of patent right |