CN209237400U - A kind of gas thermal crystalline kettle with function of measuring of Meropenem side chain production - Google Patents
A kind of gas thermal crystalline kettle with function of measuring of Meropenem side chain production Download PDFInfo
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- CN209237400U CN209237400U CN201821746173.8U CN201821746173U CN209237400U CN 209237400 U CN209237400 U CN 209237400U CN 201821746173 U CN201821746173 U CN 201821746173U CN 209237400 U CN209237400 U CN 209237400U
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- autoclave body
- crystallization
- measuring
- crystallization autoclave
- measuring tank
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Abstract
The utility model is a kind of gas thermal crystalline kettle with function of measuring of Meropenem side chain production, including crystallization autoclave body, air pump and measuring tank, it crystallizes autoclave body bottom end and is equipped with shock reducing support leg, discharge port and pH electrode, heater, air pump and pH transmitter are equipped with outside crystallization kettle body, it crystallizes autoclave body top and is equipped with motor and measuring tank, the output end of motor is equipped with agitating shaft, and agitating shaft is equipped with agitating paddle and scrapes wall blade.The utility model is by by the combination of feeding device and measuring tank, demand of the multiple equipment to place can be reduced, reduce haulage time, the direct contact of heat gas and solution simultaneously can accelerate the efficiency of heating, and the use of shock-absorbing leg can be avoided the vibration that motor operating generates and be transmitted on ground.The utility model is structurally reasonable, has very strong practicability.
Description
Technical field
The utility model relates to crystallization kettle technical fields more particularly to a kind of having for Meropenem side chain production to measure
The gas thermal crystalline kettle of function.
Background technique
Crystallization kettle is to set the hybrid reaction of material mixing, heating, cooling, stirring etc. in the industries such as chemical industry, pharmacy, food
Standby, currently used for the crystallization kettle of Meropenem side chain preparation, internal heating conductive structure, most of is using in kettle wall
Cavity is opened up, opens up conduction oil in the two sides of cavity, this heating structure heating efficiency is low, and needs individual measuring tank meter
Quantity of fluid, the transportation problem of the material between equipment have seriously affected the efficiency of medical preparation processing.
Summary of the invention
The utility model aims to solve the problem that the deficiencies in the prior art, and provide a kind of Meropenem side chain production has meter
Measure the gas thermal crystalline kettle of function.
In order to achieve the above object, the utility model adopts the following technical solutions:
A kind of gas thermal crystalline kettle with function of measuring of Meropenem side chain production, including crystallization autoclave body, the knot
Brilliant autoclave body bottom end is equipped with shock reducing support leg, and the center bottom of the crystallization autoclave body is equipped with discharge port, the crystallization autoclave body bottom end discharging
Mouth side is equipped with pH electrode, and the pH electrode is through crystallization autoclave body bottom end, if the crystallization autoclave body upper end and middle and lower part are equipped with
Dry gas hole is equipped with check valve in the stomata of middle and lower part, and side is equipped with heater outside the crystallization kettle body, the heater it is defeated
The connection of the stomata of outlet and middle and lower part, the heater top are equipped with air pump, the input of the output end and heater of the air pump
End connection, the input terminal of the air pump and the stomata of upper end connect, and the crystallization autoclave body side is additionally provided with pH transmitter, the pH
Transmitter is connect with pH electrode cable, and the crystallization autoclave body top is equipped with motor, and the output end of the motor is equipped with agitating shaft, institute
It states agitating shaft to protrude into crystallization autoclave body, is equipped with the first agitating paddle and the second agitating paddle on the agitating shaft from top to bottom, it is described to stir
It mixes to be additionally provided on axis and scrapes wall blade, the wall blade of scraping is contacted with crystallization inner wall of kettle, the lower connecting rod position for scraping wall blade
In the centre of the first agitating paddle and the second agitating paddle, the upper connecting rod for scraping wall blade is located at the top of the second agitating paddle, institute
It states crystallization autoclave body top and is additionally provided with measuring tank, the measuring tank bottom end is equipped with feed opening, and the feed opening is through crystallization autoclave body top
End, the measuring tank are equipped with liquidometer far from motor side, and the metering upper end is equipped with feed inlet.
Particularly, the shock reducing support leg includes damping base, and spring is equipped in the damping base, and the spring upper end is set
There is supporting leg, the supporting leg upper end is fixedly connected with crystallization autoclave body bottom end.
Particularly, first agitating paddle and the second agitating paddle are equipped with flow-disturbing block.
The beneficial effects of the utility model are: the utility model is by that can subtract the combination of feeding device and measuring tank
Few demand of the multiple equipment to place reduces haulage time, while the direct contact of heat gas and solution can be accelerated to heat
Efficiency, and the use of shock-absorbing leg can be avoided motor operating generate vibration be transmitted on ground.The utility model knot
Structure is reasonable, has very strong practicability.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the utility model;
Fig. 2 is shock-absorbing leg structural schematic diagram;
In figure: 1- crystallizes autoclave body;2- shock reducing support leg;3- discharge port;4-pH electrode;5- heater;6- air pump;7-pH pick-up
Device;8- motor;9- agitating shaft;The first agitating paddle of 10-;The second agitating paddle of 11-;12- scrapes wall blade;13- measuring tank;14- liquid level
Meter;15- feed inlet;16- damping base;17- spring;18- supporting leg;
Specific embodiment
The utility model is described in further detail with reference to the accompanying drawings and examples:
As shown in Figure 1, 2, the gas thermal crystalline kettle with function of measuring of a kind of Meropenem side chain production, including crystallization
Autoclave body 1,1 bottom end of crystallization autoclave body are equipped with shock reducing support leg 2, and the center bottom of the crystallization autoclave body 1 is equipped with discharge port 3, described
It crystallizes 1 bottom end discharge port of autoclave body, 3 side and is equipped with pH electrode 4, the pH electrode 4 is through crystallization 1 bottom end of autoclave body, the crystallization autoclave body
1 upper end and middle and lower part are equipped with several stomatas, are equipped with check valve in the stomata of middle and lower part, the 1 outside side of crystallization autoclave body is set
Having heaters 5, the output end of the heater 5 and the stomata of middle and lower part connect, and air pump 6 is equipped with above the heater 5, described
The output end of air pump 6 is connect with the input terminal of heater 5, and the input terminal of the air pump 6 and the stomata of upper end connect, the crystallization
1 side of autoclave body is additionally provided with pH transmitter 7, and the pH transmitter 7 is connect with 4 conducting wire of pH electrode, and 1 top of crystallization autoclave body is equipped with
Motor 8, the output end of the motor 8 are equipped with agitating shaft 9, and the agitating shaft 9 protrudes into crystallization autoclave body 1, on the agitating shaft 9 from
Under to the first agitating paddle 10 and the second agitating paddle 11 is equipped with, be additionally provided on the agitating shaft 9 and scrape wall blade 12, it is described to scrape wall paddle
Leaf 12 is contacted with crystallization 1 inner wall of autoclave body, and the lower connecting rod for scraping wall blade 12 is located at the first agitating paddle 10 and the second agitating paddle
11 centre, the upper connecting rod for scraping wall blade 12 are located at the top of the second agitating paddle 11, and 1 top of crystallization autoclave body is also set
There is measuring tank 13,13 bottom end of measuring tank is equipped with feed opening, and the feed opening is through crystallization 1 top of autoclave body, the measuring tank
13 are equipped with liquidometer 14 far from 8 side of motor, and 13 top of measuring tank is equipped with feed inlet 15.
Particularly, the shock reducing support leg 2 includes damping base 16, is equipped with spring 17, the bullet in the damping base 16
17 upper end of spring is equipped with supporting leg 18, and 18 upper end of supporting leg is fixedly connected with crystallization 1 bottom end of autoclave body.
Particularly, first agitating paddle 10 and the second agitating paddle 11 are equipped with flow-disturbing block.
Using first pouring into solution in crystallization autoclave body 1 from the feed inlet of measuring tank 13 before the utility model, in measuring tank
Quantitative acid solution is poured into 13, is opened feed opening and is poured into acid solution in crystallization autoclave body 1, is shown according to pH transmitter 7
Numerical value after added from feed inlet 15 it is suitable acid or alkali adjustment crystallization autoclave body 1 in solution pH value, power on equipment
It starts running, the gas of heating is sent into solution by air pump 6 from the stomata of middle and lower part, and solution temperature under the action of heat transmitting is sent out
Changing, solute start to be precipitated, and the crystallization adhered on inner wall is fallen under the action of scraping wall blade 12, crystallize after the completion of being precipitated logical
Cross the discharge of discharge port 3.
The utility model is exemplarily described above in conjunction with attached drawing, it is clear that the utility model specific implementation not by
The limitation of aforesaid way, if the method concept of the utility model and the various improvement of technical solution progress are used, or without
Improvement directly applies to other occasions, both is within the protection scope of the present invention.
Claims (3)
1. a kind of gas thermal crystalline kettle with function of measuring of Meropenem side chain production, which is characterized in that including crystallization kettle
Body (1), the crystallization autoclave body (1) bottom end are equipped with shock reducing support leg (2), and the center bottom of crystallization autoclave body (1) is equipped with discharge port
(3), crystallization autoclave body (1) bottom end discharge port (3) side is equipped with pH electrode (4), and the pH electrode (4) is through crystallization autoclave body
(1) bottom end, the crystallization autoclave body (1) upper end and middle and lower part are equipped with several stomatas, are equipped with check valve, institute in the stomata of middle and lower part
It states the external side of crystallization autoclave body (1) and is equipped with heater (5), the output end of the heater (5) and the stomata of middle and lower part connect, institute
It states and is equipped with air pump (6) above heater (5), the output end of the air pump (6) is connect with the input terminal of heater (5), the gas
The stomata of the input terminal and upper end that pump (6) connects, and crystallization autoclave body (1) side is additionally provided with pH transmitter (7), the pH pick-up
Device (7) is connect with pH electrode (4) conducting wire, and the crystallization autoclave body (1) top is equipped with motor (8), and the output end of the motor (8) is set
Have agitating shaft (9), the agitating shaft (9) is protruded into crystallization autoclave body (1), is equipped with first on the agitating shaft (9) from top to bottom and stirs
Mix paddle (10) and the second agitating paddle (11), be additionally provided with and scrape wall blade (12) on the agitating shaft (9), it is described scrape wall blade (12) with
The contact of autoclave body (1) inner wall is crystallized, the lower connecting rod for scraping wall blade (12) is located at the first agitating paddle (10) and the second agitating paddle
(11) centre, the upper connecting rod for scraping wall blade (12) are located at the top of the second agitating paddle (11), the crystallization autoclave body (1)
Top is additionally provided with measuring tank (13), and measuring tank (13) bottom end is equipped with feed opening, and the feed opening is through crystallization autoclave body (1) top
End, the measuring tank (13) are equipped with liquidometer (14) far from motor (8) side, and measuring tank (13) top is equipped with feed inlet
(15)。
2. a kind of gas thermal crystalline kettle with function of measuring of Meropenem side chain production according to claim 1,
It is characterized in that, the shock reducing support leg (2) includes damping base (16), is equipped with spring (17) in the damping base (16), described
Spring (17) upper end is equipped with supporting leg (18), and supporting leg (18) upper end is fixedly connected with crystallization autoclave body (1) bottom end.
3. a kind of gas thermal crystalline kettle with function of measuring of Meropenem side chain production according to claim 1,
It is characterized in that, first agitating paddle (10) and the second agitating paddle (11) are equipped with flow-disturbing block.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201821746173.8U CN209237400U (en) | 2018-10-26 | 2018-10-26 | A kind of gas thermal crystalline kettle with function of measuring of Meropenem side chain production |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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CN201821746173.8U CN209237400U (en) | 2018-10-26 | 2018-10-26 | A kind of gas thermal crystalline kettle with function of measuring of Meropenem side chain production |
Publications (1)
Publication Number | Publication Date |
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CN209237400U true CN209237400U (en) | 2019-08-13 |
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ID=67526047
Family Applications (1)
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CN201821746173.8U Active CN209237400U (en) | 2018-10-26 | 2018-10-26 | A kind of gas thermal crystalline kettle with function of measuring of Meropenem side chain production |
Country Status (1)
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CN (1) | CN209237400U (en) |
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2018
- 2018-10-26 CN CN201821746173.8U patent/CN209237400U/en active Active
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
GR01 | Patent grant | ||
GR01 | Patent grant | ||
EE01 | Entry into force of recordation of patent licensing contract |
Assignee: Gold Value (China) Financial Leasing Co.,Ltd. Assignor: TIANJIN JINGYE FINE CHEMICALS Co.,Ltd. Contract record no.: X2022980015639 Denomination of utility model: A gas-thermal crystallization kettle with metering function for the production of meropenem side chain Granted publication date: 20190813 License type: Exclusive License Record date: 20220920 |
|
EE01 | Entry into force of recordation of patent licensing contract |