CN209188771U - A kind of glassed steel reaction vessels for gas liquid reaction syringe pump method production trim,ethylchlorosilane - Google Patents
A kind of glassed steel reaction vessels for gas liquid reaction syringe pump method production trim,ethylchlorosilane Download PDFInfo
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- CN209188771U CN209188771U CN201821934827.XU CN201821934827U CN209188771U CN 209188771 U CN209188771 U CN 209188771U CN 201821934827 U CN201821934827 U CN 201821934827U CN 209188771 U CN209188771 U CN 209188771U
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- detention
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- kettle body
- reaction kettle
- ethylchlorosilane
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Abstract
The utility model relates to a kind of glassed steel reaction vessels for gas liquid reaction syringe pump method production trim,ethylchlorosilane, including reaction kettle body, the first inlet pipe for being passed through hexamethyldisiloxane is respectively provided with and for the second inlet pipe into hydrogen chloride gas at the top of reaction kettle body, reaction kettle body bottom is equipped with discharge nozzle, driving motor is equipped at reaction kettle body top center, driving motor output end is connected with rotary shaft, rotary shaft one end is through reaction kettle body outer wall and extends to inside reaction kettle body, rotary shaft side wall is equipped with the detention board group part reacted for detention hexamethyldisiloxane cooperation hydrogen chloride gas, detention board group part includes several detention plates on several connection rings and rotary shaft side wall circumferentially and between adjacent connection ring, it is high that the utility model provides a kind of rush reaction efficiency, it is good to produce obtained trim,ethylchlorosilane quality And reaction uniformly produces the glassed steel reaction vessels of trim,ethylchlorosilane for gas liquid reaction syringe pump method.
Description
Technical field
The utility model relates to a kind of reaction kettles, and in particular to one kind produces trim,ethylchlorosilane for gas liquid reaction syringe pump method
Glassed steel reaction vessels.
Background technique
During pumping production trim,ethylchlorosilane by gas liquid reaction, need to hold its raw material hexamethyldisiloxane
Continuous is passed into glassed steel reaction vessels, and hydrogen chloride gas is continually fed at the top of the glassed steel reaction vessels, and with two silicon of hexamethyl
Oxygen alkane reacts to each other, and current glassed steel reaction vessels promote the low efficiency of reaction, gaseous hydrogen chloride cannot adequately with raw material six
Tetramethyldisiloxane reaction, mixing effect is poor, and raw material hexamethyldisiloxane cannot be rapidly and uniformly in glassed steel reaction vessels
It contacts with each other and reacts with hydrogen chloride gas, lower so as to cause the rate of reaction, the trim,ethylchlorosilane quality reacted is not
Thus ideal needs to improve glassed steel reaction vessels.
Utility model content
In view of the deficienciess of the prior art, the purpose of this utility model is to provide a kind of rush reaction efficiency height, production
Obtained trim,ethylchlorosilane quality is good and reaction is uniformly used for the enamel that gas liquid reaction syringe pump method produces trim,ethylchlorosilane
Reaction kettle.
The technical solution of the utility model is achieved in that a kind of for gas liquid reaction syringe pump method production trim,ethylchlorosilane
Glassed steel reaction vessels, including reaction kettle body, it is characterised in that: be separately provided for being passed through pregnancy at the top of the reaction kettle body
First inlet pipe of base disiloxane and for the second inlet pipe into hydrogen chloride gas, the reaction kettle body bottom is provided with discharging
It manages, is provided with driving motor at the reaction kettle body top center, the output end of the driving motor is connected with rotary shaft,
The one end of the rotary shaft far from driving motor is through reaction kettle body outer wall and extends to inside reaction kettle body, the rotation shaft side
The detention board group part reacted for detention hexamethyldisiloxane cooperation hydrogen chloride gas, the detention plate are provided on wall
Component includes several axially equally spaced from each other from circumferentially and being located in the connection ring being spaced apart and rotary shaft side wall along rotary shaft
Several detention plates between adjacent connection ring are mutually permanently connected between adjacent connection ring by several detention plates.
By using above-mentioned technical proposal, raw material hexamethyldisiloxane is from the first inlet pipe being arranged at the top of reaction kettle body
It enters inside reaction kettle body, the reactant hydrogen chloride gas of cooperation enters reaction kettle body internal engagement from the second inlet pipe and carries out
Reaction, and it is provided with driving motor at reaction kettle body top center, under the driving effect of driving motor, output end
The rotary shaft of connection rotates, and drives the detention board group part being arranged on rotary shaft side wall by sufficient group of hexamethyldisiloxane
It stays on detention board group part, detention board group part includes several axially equally spaced from each other from the connection ring and rotation that are spaced apart along rotary shaft
Several detention plates on shaft side wall circumferentially and between adjacent connection ring pass through several resistances between adjacent connection ring
Stay plate to be mutually permanently connected, by above structure, make the uniform detention of raw material hexamethyldisiloxane of liquid in connection ring and
The surface of detention plate, and under the rotation of rotary shaft drive, the hydrogen chloride gas fitted into inside reaction kettle body is filled
The haptoreaction divided, improves reaction efficiency and increases the investment for the raw material hexamethyldisiloxane that can be put into the unit time
Amount ensure that the effect for promoting reaction, and stirring efficiency is high, and simple and reliable for structure, the utility model provides a kind of rush reaction efficiency
The trim,ethylchlorosilane quality that high, production obtains is good and reaction is uniformly for gas liquid reaction syringe pump method production trim,ethylchlorosilane
Glassed steel reaction vessels.
The utility model is further arranged to: being provided between adjacent two pieces of detention plate and is reinforced detention plate.
By using above-mentioned technical proposal, in order to further increase the detention effect to raw material hexamethyldisiloxane, from
And improve and promote reaction efficiency and improve raw material availability, it is provided between adjacent two pieces of detention plate and reinforces detention plate, simultaneously
The structural strength for improving detention board group part entirety, in lasting cooperation rotation process, that improves detention board group part uses the longevity
Life.
The utility model is further arranged to: being transversely provided through reinforcement detention in the middle part of the reinforcement detention plate side wall
Hole.
By using above-mentioned technical proposal, in order to improve the mixing effect to raw material hexamethyldisiloxane, reinforcing hindering
It stays transversely to be provided through in the middle part of plate side wall and reinforces detention hole, thus under the rotation with rotary shaft, using transversely passing through
The reinforcement detention hole reinforced in the middle part of detention plate side wall is worn to be stirred raw material hexamethyldisiloxane and cooperate gaseous chlorination
The reaction of hydrogen Rapid contact, improves reaction efficiency.
The utility model is further arranged to: circumferentially distributed on the connection ring-side wall to have several through-holes.
It is circumferentially distributed on connection ring-side wall to have several through-holes by using above-mentioned technical proposal, it is several by being arranged
Through-hole increases the bond area of raw material hexamethyldisiloxane, and during rotating with rotary shaft, quickly and chlorine
Change hydrogen haptoreaction.
The utility model is further arranged to: circumferentially equally spaced from each other from being arranged at intervals on the reaction kettle body inner sidewall
Several auxiliary detention plates are uniformly provided through several auxiliary detention holes on the auxiliary detention plate side wall.
By using above-mentioned technical proposal, promote to cooperate the detention board group part of rotation to further increase glassed steel reaction vessels
The efficiency and effect of reaction, it is circumferentially equally spaced from each other from being arranged at intervals with several auxiliary detention plates on reaction kettle body inner sidewall,
Several auxiliary detention holes are uniformly provided through on auxiliary detention plate side wall, to make the detention board group part cooperation auxiliary in rotation
Detention plate greatly promotes the hydrogen chloride gas liquid flowability inside reaction kettle body, the contact surface with raw material hexamethyldisiloxane
It is greatly improved with contact velocity.
The utility model is further arranged to: the auxiliary detention hole is in regular hexagon.
By using above-mentioned technical proposal, set auxiliary detention hole on the one hand to improve auxiliary detention in regular hexagon
The integral strength of plate, on the other hand the effect of the structure detention raw material hexamethyldisiloxane is good, cooperates the anti-of hydrogen chloride gas
It answers high-efficient.
Detailed description of the invention
In order to illustrate the embodiment of the utility model or the technical proposal in the existing technology more clearly, below will be to embodiment
Or attached drawing needed to be used in the description of the prior art is briefly described, it should be apparent that, the accompanying drawings in the following description is only
It is some embodiments of the utility model, for those of ordinary skill in the art, before not making the creative labor property
It puts, is also possible to obtain other drawings based on these drawings.
Fig. 1 is specific embodiment of the present invention structural schematic diagram.
Fig. 2 is detention board group part schematic view of the front view in specific embodiment of the present invention.
Fig. 3 is detention board group part overlooking structure diagram in specific embodiment of the present invention.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model
Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole
Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without creative efforts
Every other embodiment obtained, fall within the protection scope of the utility model.
As shown in Figure 1-Figure 3, trim,ethylchlorosilane is produced for gas liquid reaction syringe pump method the utility model discloses a kind of
Glassed steel reaction vessels, including reaction kettle body 1 are respectively set at the top of the reaction kettle body 1 in the utility model specific embodiment
There is the first inlet pipe 2 for being passed through hexamethyldisiloxane and for the second inlet pipe 3 into hydrogen chloride gas, the reaction kettle body
1 bottom is provided with discharge nozzle 13, and driving motor 4, the driving motor 4 are provided at 1 top center of reaction kettle body
Output end be connected with rotary shaft 5, the one end of the rotary shaft 5 far from driving motor 4 is through 1 outer wall of reaction kettle body and extends to
Inside reaction kettle body 1, it is provided on 5 side wall of rotary shaft and is carried out for detention hexamethyldisiloxane cooperation hydrogen chloride gas
The detention board group part of reaction, the detention board group part include several axial equally spaced from each other from the connection being spaced apart along rotary shaft 5
Several detention plates 7 on 5 side wall of ring 6 and rotary shaft circumferentially and between adjacent connection ring 6, adjacent connection ring 6 it
Between be mutually permanently connected by several detention plates 7.
By using above-mentioned technical proposal, raw material hexamethyldisiloxane from be arranged in the first of the top of reaction kettle body 1 into
Pipe 2 enters inside reaction kettle body 1, and the reactant hydrogen chloride gas of cooperation enters inside reaction kettle body 1 from the second inlet pipe 3 matches
Conjunction is reacted, and is provided with driving motor 4 at 1 top center of reaction kettle body, in the driving effect of driving motor 4
Under, the rotary shaft 5 of output end connection rotates, and drives the detention board group part that is arranged on 5 side wall of rotary shaft by hexamethyl two
Sufficient group of siloxanes stays on detention board group part, detention board group part include it is several along rotary shaft 5 it is axial it is equally spaced from each other sow discord every
Several detention plates 7 on 5 side wall of connection ring 6 and rotary shaft of distribution circumferentially and between adjacent connection ring 6 are adjacent
It is mutually permanently connected between connection ring 6 by several detention plates 7, by above structure, makes the two silicon oxygen of raw material hexamethyl of liquid
The uniform detention of alkane fits into reaction kettle on the surface of connection ring 6 and detention plate 7, and under the rotation of rotary shaft 5 drive
Hydrogen chloride gas inside body 1 carries out sufficient haptoreaction, and improving reaction efficiency and increasing in the unit time can put into
Raw material hexamethyldisiloxane input amount, ensure that the effect for promoting reaction, stirring efficiency is high, simple and reliable for structure, this reality
Provide that a kind of rush reaction efficiency is high, production obtains trim,ethylchlorosilane quality is good and reaction is uniformly used for gas-liquid with novel
React the glassed steel reaction vessels of syringe pump method production trim,ethylchlorosilane.
In the utility model specific embodiment, it is provided between adjacent two pieces of detention plate 7 and reinforces detention plate 10.
By using above-mentioned technical proposal, in order to further increase the detention effect to raw material hexamethyldisiloxane, from
And improve and promote reaction efficiency and improve raw material availability, it is provided between adjacent two pieces of detention plate 7 and reinforces detention plate 10, together
When improve the structural strength of detention board group part entirety, in lasting cooperation rotation process, improve the use of detention board group part
Service life.
In the utility model specific embodiment, reinforcement is transversely provided through in the middle part of 10 side wall of reinforcement detention plate
Detention hole 11.
By using above-mentioned technical proposal, in order to improve the mixing effect to raw material hexamethyldisiloxane, reinforcing hindering
It stays transversely to be provided through in the middle part of 10 side wall of plate and reinforces detention hole 11, thus under the rotation with rotary shaft 5, using along cross
Raw material hexamethyldisiloxane is stirred to the reinforcement detention hole 11 in the middle part of reinforcement 10 side wall of detention plate and cooperates gas
The hydrogen chloride gas Rapid contact of state reacts, and improves reaction efficiency.
It is circumferentially distributed on 6 side wall of connection ring to have several through-holes 12 in the utility model specific embodiment.
It is circumferentially distributed on 6 side wall of connection ring to have several through-holes 12 by using above-mentioned technical proposal, if passing through setting
Dry through-hole 12 increases the bond area of raw material hexamethyldisiloxane, and during rotating with rotary shaft 5, quickly
With hydrogen chloride gas haptoreaction.
It is circumferentially equally spaced from each other on 1 inner sidewall of reaction kettle body to sow discord every setting in the utility model specific embodiment
Several auxiliary detention plates 8 are equipped with, are uniformly provided through several auxiliary detention holes 9 on 8 side wall of auxiliary detention plate.
By using above-mentioned technical proposal, promote to cooperate the detention board group part of rotation to further increase glassed steel reaction vessels
The efficiency and effect of reaction, it is circumferentially equally spaced from each other from being arranged at intervals with several auxiliary detention plates on 1 inner sidewall of reaction kettle body
8, it assists uniformly being provided through several auxiliary detention holes 9 on 8 side wall of detention plate, to make the detention board group part cooperation in rotation
Detention plate 8 is assisted, greatly promotes the hydrogen chloride gas liquid flowability inside reaction kettle body 1, with raw material hexamethyldisiloxane
Contact surface and contact velocity greatly improve.
In the utility model specific embodiment, the auxiliary detention hole 9 is in regular hexagon.
By using above-mentioned technical proposal, set auxiliary detention hole 9 on the one hand to improve auxiliary detention in regular hexagon
The integral strength of plate 8, on the other hand the effect of the structure detention raw material hexamethyldisiloxane is good, cooperates the anti-of hydrogen chloride gas
It answers high-efficient.
The above is only the preferred embodiment of the utility model only, is not intended to limit the utility model, all at this
Within the spirit and principle of utility model, any modification, equivalent replacement, improvement and so on should be included in the utility model
Protection scope within.
Claims (6)
1. a kind of glassed steel reaction vessels for gas liquid reaction syringe pump method production trim,ethylchlorosilane, including reaction kettle body (1), special
Sign is: being separately provided for being passed through the first inlet pipe (2) of hexamethyldisiloxane and be used at the top of the reaction kettle body (1)
Into the second inlet pipe (3) of hydrogen chloride gas, reaction kettle body (1) bottom is provided with discharge nozzle (13), the reaction kettle body (1)
It is provided at top center driving motor (4), the output end of the driving motor (4) is connected with rotary shaft (5), the rotation
The one end of shaft (5) far from driving motor (4) is through reaction kettle body (1) outer wall and extends to reaction kettle body (1) inside, the rotation
The detention board group part reacted for detention hexamethyldisiloxane cooperation hydrogen chloride gas is provided on shaft (5) side wall,
The detention board group part includes several axial equally spaced from each other from the connection ring being spaced apart (6) and rotary shaft (5) along rotary shaft (5)
Several detention plates (7) on side wall circumferentially and between adjacent connection ring (6), adjacent connection ring pass through between (6)
Several detention plates (7) are mutually permanently connected.
2. a kind of glassed steel reaction vessels for gas liquid reaction syringe pump method production trim,ethylchlorosilane according to claim 1,
Reinforce detention plate (10) it is characterized by: being provided between adjacent two pieces of detention plate (7).
3. a kind of glassed steel reaction vessels for gas liquid reaction syringe pump method production trim,ethylchlorosilane according to claim 2,
Reinforce detention hole (11) it is characterized by: being transversely provided through in the middle part of reinforcement detention plate (10) side wall.
4. a kind of enamel for gas liquid reaction syringe pump method production trim,ethylchlorosilane according to claim 1 or 2 or 3 is anti-
Answer kettle, it is characterised in that: circumferentially distributed on connection ring (6) side wall there are several through-holes (12).
5. a kind of enamel for gas liquid reaction syringe pump method production trim,ethylchlorosilane according to claim 1 or 2 or 3 is anti-
Answer kettle, it is characterised in that: circumferentially equally spaced from each other from being arranged at intervals with several auxiliary detentions on reaction kettle body (1) inner sidewall
Plate (8) is uniformly provided through several auxiliary detention holes (9) on auxiliary detention plate (8) side wall.
6. a kind of glassed steel reaction vessels for gas liquid reaction syringe pump method production trim,ethylchlorosilane according to claim 5,
It is characterized by: the auxiliary detention hole (9) is in regular hexagon.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821934827.XU CN209188771U (en) | 2018-11-22 | 2018-11-22 | A kind of glassed steel reaction vessels for gas liquid reaction syringe pump method production trim,ethylchlorosilane |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821934827.XU CN209188771U (en) | 2018-11-22 | 2018-11-22 | A kind of glassed steel reaction vessels for gas liquid reaction syringe pump method production trim,ethylchlorosilane |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN209188771U true CN209188771U (en) | 2019-08-02 |
Family
ID=67425485
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201821934827.XU Active CN209188771U (en) | 2018-11-22 | 2018-11-22 | A kind of glassed steel reaction vessels for gas liquid reaction syringe pump method production trim,ethylchlorosilane |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN209188771U (en) |
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2018
- 2018-11-22 CN CN201821934827.XU patent/CN209188771U/en active Active
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