CN209188300U - A kind of molecular sieve cation replacement system - Google Patents
A kind of molecular sieve cation replacement system Download PDFInfo
- Publication number
- CN209188300U CN209188300U CN201821668379.3U CN201821668379U CN209188300U CN 209188300 U CN209188300 U CN 209188300U CN 201821668379 U CN201821668379 U CN 201821668379U CN 209188300 U CN209188300 U CN 209188300U
- Authority
- CN
- China
- Prior art keywords
- cylinder
- suoshu
- fixed
- screwed
- molecular sieve
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000002808 molecular sieve Substances 0.000 title claims abstract description 33
- -1 molecular sieve cation Chemical class 0.000 title claims abstract description 21
- 241000883990 Flabellum Species 0.000 claims description 18
- 230000005540 biological transmission Effects 0.000 claims description 13
- 238000007789 sealing Methods 0.000 claims description 10
- 238000003756 stirring Methods 0.000 claims description 8
- 238000005192 partition Methods 0.000 claims description 4
- 238000000034 method Methods 0.000 abstract description 13
- 239000000047 product Substances 0.000 abstract 2
- 239000013067 intermediate product Substances 0.000 abstract 1
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 description 12
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 10
- 239000000463 material Substances 0.000 description 7
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 6
- 239000001110 calcium chloride Substances 0.000 description 5
- 229910001628 calcium chloride Inorganic materials 0.000 description 5
- 235000011148 calcium chloride Nutrition 0.000 description 5
- ORTQZVOHEJQUHG-UHFFFAOYSA-L copper(II) chloride Chemical compound Cl[Cu]Cl ORTQZVOHEJQUHG-UHFFFAOYSA-L 0.000 description 5
- 239000001103 potassium chloride Substances 0.000 description 5
- 235000011164 potassium chloride Nutrition 0.000 description 5
- 229910021592 Copper(II) chloride Inorganic materials 0.000 description 4
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 4
- 238000010586 diagram Methods 0.000 description 4
- 229910001220 stainless steel Inorganic materials 0.000 description 4
- 239000010935 stainless steel Substances 0.000 description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 2
- 241000209094 Oryza Species 0.000 description 2
- 235000007164 Oryza sativa Nutrition 0.000 description 2
- 150000001768 cations Chemical class 0.000 description 2
- 238000005260 corrosion Methods 0.000 description 2
- 230000007797 corrosion Effects 0.000 description 2
- ZZUFCTLCJUWOSV-UHFFFAOYSA-N furosemide Chemical compound C1=C(Cl)C(S(=O)(=O)N)=CC(C(O)=O)=C1NCC1=CC=CO1 ZZUFCTLCJUWOSV-UHFFFAOYSA-N 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 235000009566 rice Nutrition 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 239000004411 aluminium Substances 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 229910021645 metal ion Inorganic materials 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Combined Means For Separation Of Solids (AREA)
Abstract
The utility model discloses a kind of molecular sieve cations to replace system, including filter press, multistage pump, beater, interchanger and circulating pump；The output port of beater is communicated to the input port of multistage pump, and the output port of multistage pump is communicated to filter press input port；The output port of interchanger is communicated to the input port of circulating pump, and the output port of circulating pump is communicated to the input port of filter press；It during the entire process of molecular sieve cation replacement, is mutually communicated between the process equipment of each step, intermediate products do not need to contact with external environment, to reduce the contaminated possibility of product, improve product quality；And each procedure of processing consistent operation, improve processing efficiency.
Description
Technical field
The utility model relates to molecular sieve processing technique fields, and in particular to a kind of molecular sieve cation replacement system.
Background technique
Molecular sieve connects the four connecting framework structure of three-dimensional formed by oxygen bridge by silicon, aluminium, there is many holes in the structure
The uniform duct marshalling of diameter and the very big hole of internal surface area are a kind of porous solids with specific crystal structure；
Additionally water lower containing electricity price and ionic radius biggish metal ion and compound state.
Na molecular sieve is also 4A molecular sieve, and preparation process is to be reacted with potassium chloride, calcium chloride solution with NaA type, K+ or
The part or all of location swap of Na+ in Ca2+ and NaA type generates KA type molecular sieve or CaA type molecular sieve.NaX type molecule
Sieve calcium chloride, copper chloride solution are reacted with NaX type, generate CaX type and CuX type molecular sieve.
But molecular sieve is processed respectively using multiple steps during existing molecular sieve cation replacement, respectively
Continuity is poor between a step, molecular sieve cation replacement low efficiency, and mutually isolated between each step, conveys in product
Influence to product quality is be easy to cause with during replacement process equipment.
It, can will be in molecular sieve cation replacement process accordingly, it is desirable to provide a kind of molecular sieve cation replaces system
Each step it is highly integrated, improve molecular sieve cation replacement efficiency, it is ensured that product quality.
Utility model content
The purpose of this utility model is to provide a kind of molecular sieve cations to replace system, to solve existing molecular sieve sun
Cation replacement low efficiency of the ion more exchange device to molecular sieve, the problem of product stability difference.
To achieve the above object, the technical solution of the utility model are as follows:
A kind of molecular sieve cation replacement system, including filter press, multistage pump, beater, interchanger and circulating pump；It is described
The output port of beater is communicated to the input port of the multistage pump, and the output port of the multistage pump is communicated to the filters pressing
Machine input port；The output port of the interchanger is communicated to the input port of the circulating pump, the output end of the circulating pump
Mouth is communicated to the input port of filter press.
Preferably, the beater includes first cylinder, and the bottom of the first cylinder of Yu Suoshu is provided with rotating seat, in
It is provided with multiple first fixed blocks on the inner wall of the rotating seat, the scraper plate of rectangle is fixed on the first fixed block of Yu Suoshu；In
The top of first cylinder is provided with the first sealing cover；First is fixed with bolt in the upper surface of first sealing cover
There is the first reversing piece in the upper end of support, the first support frame of Yu Suoshu with being screwed, the input terminal rotation of the first reversing piece of Yu Suoshu
It is connected to first motor；Be equipped with the first drive shaft in the inner along the axial direction of first cylinder, first drive shaft it is upper
End and lower end are rotatably connected in respectively on first reversing piece and the rotating seat；In being provided with multiple stir in first drive shaft
Mix paddle；In being fixed with discharge nozzle on first fixed block, the upper end of the discharge nozzle extends to the upper of first sealing cover
Side.
Preferably, the agitating paddle includes discoid agitator disk, and the upside of Yu Suoshu agitator disk is screwed with circle with screw thread
The first of tubular is screwed on cylinder, and the first flabellum of multiple arc-shapeds is provided on the outer wall of Yu Suoshu agitator disk；In the agitator disk
The center point of downside be provided with second and be screwed on cylinder, Yu Suoshu second is screwed on the outer wall of cylinder and is provided with multiple third flabellums；Edge
The agitator disk radial to its downside be provided with multiple second flabellums.
Preferably, the interchanger includes the second cylinder, and the edge of the lower end of the second cylinder of Yu Suoshu is provided at least 3
A supporting leg；In being fixed with multiple second fixed blocks on the inner wall of second cylinder, in a column along vertical direction described the
Partition is fixed on two fixed blocks；Fixing seat is fixed in the bottom of the inner cavity of second cylinder；In second cylinder
Top is provided with cover board, and the upside of Yu Suoshu cover board is fixed with the second support frame, the upper end of the second support frame of Yu Suoshu with bolt
It is fixed with the second reversing piece with bolt, Yu Suoshu the second reversing piece input port is screwed with the second motor；In second cylinder
Inside it is equipped with transmission shaft；The top and bottom of the transmission shaft are rotatably connected in respectively in second reversing piece and the fixing seat；
In being provided with multiple stirring flabellums on the transmission shaft.
The utility model has the advantages that
Beater is buried in below ground, selects 304 anticorrosion materials；Multistage pump pipeline is communicated to the bottom of beater
Portion, and have sinking for 0.35 rice diameter around duct bottom, convenient for the material of hollander tub all on on filter press；Choosing
With multistage pump, the purpose is to molecular sieve is transported on filter press；Interchanger its select 304 anticorrosion materials, with reduce KCl or
Chloride ion corrosion common iron in CaCl2 or CuCl2 solution, the blade and agitating shaft of stirring select stainless steel entirely；Circulating pump
It is common stainless steel pump, is used for a KCl or CaCl2 or CuCl2 solution is transported to filter press；Molecule is realized in filter press
Sieve the exchange of cation；
It during the entire process of molecular sieve cation replacement, is mutually communicated between the process equipment of each step, is produced from centre
Product do not need to contact with external environment, to reduce the contaminated possibility of product, improve product quality；And each procedure of processing
Consistent operation improves processing efficiency.
Detailed description of the invention
Fig. 1 is the system block diagram of the molecular sieve cation replacement system of utility model.
Fig. 2 is the structural schematic diagram of beater in utility model.
Fig. 3 is the structural schematic diagram of interchanger in utility model.
Fig. 4 is the structural schematic diagram of agitating paddle in utility model.
In figure: 1- filter press；2- multistage pump；3- beater；31- first motor；The first reversing piece of 32-；33- first is supported
Frame；34- discharge nozzle；The first sealing cover of 35-；36- scraper plate；The first fixed block of 37-；38- agitating paddle；381- first is screwed on cylinder；
382- agitator disk；The first flabellum of 383-；The second flabellum of 384-；385- third flabellum；386- second is screwed on cylinder；39- rotating seat；
The first cylinder of 310-；The first drive shaft of 311-；4- interchanger；The second cylinder of 41-；42- partition；The second fixed block of 43-；44- is solid
Reservation；45- supporting leg；46- stirs flabellum；47- transmission shaft；48- cover board；The second support frame of 49-；The second reversing piece of 410-；411-
Second motor；5- circulating pump.
Specific embodiment
The following examples illustrate the utility model, but is not intended to limit the scope of the present invention.
Embodiment
The molecular sieve cation of the present embodiment replaces system, including filter press 1, multistage pump 2, beater 3,4 and of interchanger
Circulating pump 5；The output port of the beater 3 is communicated to the input port of the multistage pump 2 with the screw thread mode of being screwed on, described more
The output port of grade pump 2 is communicated to 1 input port of filter press with the screw thread mode of being screwed on；The output port of the interchanger 4
It is communicated to the input port of the circulating pump 5 with the screw thread mode of being screwed on, the output port of the circulating pump 5 is screwed on mode with screw thread
It is communicated to the input port of filter press 1.
Beater is buried in below ground, selects 304 anticorrosion materials；Multistage pump pipeline is communicated to the bottom of beater
Portion, and have sinking for 0.35 rice diameter around duct bottom, convenient for the material of hollander tub all on on filter press；Choosing
With multistage pump, the purpose is to molecular sieve is transported on filter press；Interchanger its select 304 anticorrosion materials, with reduce KCl or
Chloride ion corrosion common iron in CaCl2 or CuCl2 solution, the blade and agitating shaft of stirring select stainless steel entirely；
Circulating pump is common stainless steel pump, is used for a KCl or CaCl2 or CuCl2 solution is transported to filter press；It is pressing
The exchange of molecular sieve cation is realized in filter；
It during the entire process of molecular sieve cation replacement, is mutually communicated between the process equipment of each step, is produced from centre
Product do not need to contact with external environment, to reduce the contaminated possibility of product, improve product quality；And each procedure of processing
Consistent operation improves processing efficiency.
The beater 3 includes first cylinder 310, and the bottom of the first cylinder of Yu Suoshu 310 is fixed with rotation with bolt
Swivel base 39 is fixed with multiple first fixed blocks 37, the first fixed block of Yu Suoshu 37 with bolt on the inner wall of Yu Suoshu rotating seat 39
Upper snap fit is fixed with the scraper plate 36 of rectangle；The first sealing cover 35 is fixed with bolt in the top of first cylinder 310；
It is fixed with the first support frame 33 with bolt in the upper surface of first sealing cover 35, the upper end of the first support frame of Yu Suoshu 33 is used
Being screwed has the first reversing piece 32, and the input terminal of the first reversing piece of Yu Suoshu 32 is screwed with first motor 31；Along described
What the axial direction of one cylinder 310 rotated in the inner is equipped with the first drive shaft 311, the top and bottom of first drive shaft 311
What is rotated respectively is rotatably connected on first reversing piece 32 and the rotating seat 39；In using screw thread in first drive shaft 311
It is screwed with multiple agitating paddles 38；In being fixed with discharge nozzle 34, the upper end of the discharge nozzle 34 on first fixed block 37
Extend to the upside of first sealing cover 35.
First reversing piece 32 realizes transmission using bevel gear set, and 32 output end of the first reversing piece is screwed with first
Bevel gear, the input terminal of the first drive shaft of Yu Suoshu 311 are screwed with second bevel gear, the first bevel gear and second cone
Power transmitting is realized in gear intermeshing, and realizes horizontal direction being converted to the rotation on vertical direction, realizes commutation.
The agitating paddle 38 includes discoid agitator disk 382, and the upside of Yu Suoshu agitator disk 382 is screwed with circle with screw thread
The first of tubular is screwed on cylinder 381, and the first flabellum 383 of multiple arc-shapeds is connected on the outer wall of Yu Suoshu agitator disk 382；In institute
The center point for stating the downside of agitator disk 382 is connected with second and is screwed on cylinder 386, and Yu Suoshu second is screwed on the outer wall of cylinder 386 and is clamped
There are multiple third flabellums 385；Multiple second flabellums 384 are connected with radial to its downside along the agitator disk 382.
First flabellum, second flabellum and the third flabellum are realized in different location to machined material respectively
Stirring, make raw material be uniformly mixed, improve reaction rate.
The interchanger 4 includes the second cylinder 41, and the edge of the lower end of the second cylinder of Yu Suoshu 41 is screwed with screw thread
At least three supporting leg 45；In being fixed with multiple second fixed blocks 43 on the inner wall of second cylinder 41, along vertical side
To column second fixed block 43 on be fixed with partition 42；Bottom bolt in the inner cavity of second cylinder 41
It is fixed with fixing seat 44；It is fixed with cover board 48 with bolt in the top of second cylinder 41, the upside of Yu Suoshu cover board 48 is used
Bolt is fixed with the second support frame 49, and the upper end of the second support frame of Yu Suoshu 49 is fixed with the second reversing piece 410 with bolt, in institute
It states 410 input port of the second reversing piece and is screwed with the second motor 411；In being equipped with transmission shaft 47 in second cylinder 41；Institute
The top and bottom for stating transmission shaft 47 are rotatably connected in respectively in second reversing piece 410 and the fixing seat 44；In the transmission
Multiple stirring flabellums 46 are screwed with screw thread on axis 47.
Second reversing piece 410 realizes transmission using bevel gear set, and 410 output end of the second reversing piece is screwed with
Third hand tap gear, the input terminal of Yu Suoshu transmission shaft 47 are screwed with the 4th bevel gear, the third hand tap gear and the 4th cone
Power transmitting is realized in gear intermeshing, and realizes horizontal direction being converted to the rotation on vertical direction, realizes commutation.
Although above having made detailed description to the utility model with generality explanation and specific embodiment,
On the basis of the utility model, it can be made some modifications or improvements, this is apparent to those skilled in the art
's.Therefore, these modifications or improvements on the basis of without departing from the spirit of the present invention, belong to the utility model and want
Seek the range of protection.
Claims (4)
1. a kind of molecular sieve cation replaces system, which is characterized in that including filter press (1), multistage pump (2), beater (3),
Interchanger (4) and circulating pump (5)；The output port of the beater (3) is communicated to the input port of the multistage pump (2), institute
The output port for stating multistage pump (2) is communicated to the filter press (1) input port；The output port of the interchanger (4) is connected to
Output port to the input port of the circulating pump (5), the circulating pump (5) is communicated to the input port of filter press (1).
2. molecular sieve cation replaces system according to claim 1, which is characterized in that the beater (3) includes first
Cylinder (310), the bottom of the first cylinder of Yu Suoshu (310) are provided with rotating seat (39), on the inner wall of Yu Suoshu rotating seat (39)
Multiple first fixed blocks (37) are provided with, the scraper plate (36) of rectangle is fixed on the first fixed block of Yu Suoshu (37)；In described
The top of one cylinder (310) is provided with the first sealing cover (35)；It is fixed in the upper surface of first sealing cover (35) with bolt
Have the first support frame (33), there are the first reversing piece (32), Yu Suoshu in the upper end of the first support frame of Yu Suoshu (33) with being screwed
The input terminal of first reversing piece (32) is screwed with first motor (31)；It is worn in the inner along the axial direction of first cylinder (310)
Equipped with the first drive shaft (311), the top and bottom of first drive shaft (311) are rotatably connected in first reversing piece respectively
(32) and on the rotating seat (39)；In being provided with multiple agitating paddles (38) on first drive shaft (311)；In described first
It is fixed on fixed block (37) discharge nozzle (34), the upper end of the discharge nozzle (34) extends to the upper of first sealing cover (35)
Side.
3. molecular sieve cation replaces system according to claim 2, which is characterized in that the agitating paddle (38) includes disk
The agitator disk (382) of shape, the upside of Yu Suoshu agitator disk (382) are screwed with cylindric first with screw thread and are screwed on cylinder (381), in
The first flabellum (383) of multiple arc-shapeds is provided on the outer wall of the agitator disk (382)；Under the agitator disk (382)
The center point of side is provided with second and is screwed on cylinder (386), and Yu Suoshu second, which is screwed on the outer wall of cylinder (386), is provided with multiple thirds fans
Leaf (385)；Its downside is provided with multiple second flabellums (384) along the agitator disk (382).
4. molecular sieve cation replaces system according to claim 1, which is characterized in that the interchanger (4) includes second
Cylinder (41), the edge of the lower end of the second cylinder of Yu Suoshu (41) are provided at least three supporting leg (45)；In second cylinder
(41) multiple second fixed blocks (43) are fixed on inner wall, on column second fixed block (43) along vertical direction
It is fixed with partition (42)；Fixing seat (44) are fixed in the bottom of the inner cavity of second cylinder (41)；
It is provided with cover board (48) in the top of second cylinder (41), the upside of Yu Suoshu cover board (48) is fixed with bolt
The upper end of two support frames (49), the second support frame of Yu Suoshu (49) is fixed with the second reversing piece (410), Yu Suoshu second with bolt
Reversing piece (410) input port is screwed with the second motor (411)；Transmission shaft (47) are equipped in second cylinder (41)；
The top and bottom of the transmission shaft (47) are rotatably connected in respectively on second reversing piece (410) and the fixing seat (44)；In
Multiple stirring flabellums (46) are provided on the transmission shaft (47).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821668379.3U CN209188300U (en) | 2018-10-15 | 2018-10-15 | A kind of molecular sieve cation replacement system |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821668379.3U CN209188300U (en) | 2018-10-15 | 2018-10-15 | A kind of molecular sieve cation replacement system |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN209188300U true CN209188300U (en) | 2019-08-02 |
Family
ID=67407953
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201821668379.3U Expired - Fee Related CN209188300U (en) | 2018-10-15 | 2018-10-15 | A kind of molecular sieve cation replacement system |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN209188300U (en) |
-
2018
- 2018-10-15 CN CN201821668379.3U patent/CN209188300U/en not_active Expired - Fee Related
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| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20190802 |