CN209155887U - A kind of ammonia nitrogen low temperature distillation bottle and ammonia nitrogen cryogenic alembic - Google Patents
A kind of ammonia nitrogen low temperature distillation bottle and ammonia nitrogen cryogenic alembic Download PDFInfo
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- CN209155887U CN209155887U CN201821682191.4U CN201821682191U CN209155887U CN 209155887 U CN209155887 U CN 209155887U CN 201821682191 U CN201821682191 U CN 201821682191U CN 209155887 U CN209155887 U CN 209155887U
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- distillation
- ammonia nitrogen
- nitrogen
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- ball bubble
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Abstract
The utility model discloses a kind of ammonia nitrogen low temperature distillation bottles, including distilling bottle body, integrally formed with distillation ball bubble at the top of the distillation bottle body, ball bubble top is distilled to steep integrally formed with imitative nitrogen ball, the distillation bottle body bottom is integrally formed with evacuated tube, it distills ball bubble side and is equipped with air inlet pipe, imitative nitrogen ball bubble side is equipped with distillation cascade, and a kind of ammonia nitrogen cryogenic alembic including this cucurbit, including cooling system, drainage system, Distallation systm and aerating system, the utility model is by the way that cucurbit to be connected to aerating system, air pump provides gas source for distillation, power is provided for the absorption of ammonia nitrogen, be conducive to the extraction and measured value analysis of ammonia nitrogen, reduce error.By designing imitative nitrogen ball bubble, and air inlet pipe one end is protruded into inside cucurbit body, is gathered in ammonia nitrogen steam up in imitative nitrogen ball bubble, entered in absorption bottle by ammonia nitrogen steam outleting pipe in communication again, cooperate rubber stopper beyond the Great Wall simultaneously, ammonia and nitrogen components can be prevented to be lost, keep test sample more accurate.
Description
Technical field
The utility model relates to ammonia nitrogen distillation detection technique field more particularly to a kind of ammonia nitrogen low temperature distillation bottles and ammonia nitrogen
Cryogenic alembic.
Background technique
Water pollution problems more causes the concern of people as an environmental protection problem outstanding, in order to ensure water quality mark
It is quasi- qualified, it needs to detect the water quality in production, life, the ammonia-nitrogen content in water is characterization organic matter in water quality monitoring
Project is often surveyed, and has become an important water quality monitoring index.Laboratory chemical method measurement ammonia nitrogen index needs to carry out early period
Pretreatment, traditional ammonia nitrogen pretreatment unit distilling effect is poor, and distillation is not easy to control, and ammonia and nitrogen components are not easy to steam, greatly
Affect measured value analysis.
Summary of the invention
The purpose of this utility model is that: it is poor for traditional ammonia nitrogen pretreatment unit distilling effect, it distills not easily-controllable
The problem of system, ammonia and nitrogen components are not easy to steam, and influence measured value analysis, the utility model provide a kind of ammonia nitrogen low temperature distillation bottle and ammonia
Nitrogen cryogenic alembic.
The technical solution adopted in the utility model is as follows:
A kind of ammonia nitrogen low temperature distillation bottle, including distillation bottle body, the distillation bottle body top are steamed integrally formed with distillation ball bubble
It evaporates ball bubble top to steep integrally formed with imitative nitrogen ball, the distillation bottle body bottom distills ball bubble side and set integrally formed with evacuated tube
There is air inlet pipe, imitates nitrogen ball bubble side and be equipped with distillation cascade, the imitative nitrogen ball bubble top is equipped with adding mouth, and gas is entered from air inlet pipe
Inside cucurbit body, distillation ingredient is discharged from distillation cascade, and the evacuated tube of bottom the water after separation can be discharged.
Further, it is internal to extend into imitative nitrogen ball bubble for described distillation cascade one end, and the other end is vacantly on the outside of imitative nitrogen ball steeps, just
It is connect in distillation cascade with other pipelines.
Further, described air inlet pipe one end is extend into inside cucurbit body, and extends to the bottom of distillation bottle body, another
Vacantly on the outside of distillation ball bubble, the bottom that air inlet pipe extends to distillation bottle body can make the gas entered from distillation bottle body bottom at end
Toward rising, farthest separate ammonia and nitrogen components.
A kind of ammonia nitrogen cryogenic alembic, including casing, cooling system, drainage system, Distallation systm and aerating system, it is described
There are four Distallation systm is set；
The Distallation systm includes the cucurbit for being fixed on casing top, the heating device of cucurbit lower part, absorption bottle and
Ammonia nitrogen steam outleting pipe, the bottleneck of the cucurbit are plugged with rubber stopper, and ammonia nitrogen steam outleting pipe one end is connected to absorption bottle,
The other end is connected to the distillation cascade of cucurbit；
The aerating system includes air pump, aeration tube and the check valve being arranged on aeration tube, and the aeration tube one end connects
Air pump is connect, the other end is connected to the air inlet pipe of cucurbit；
The cooling system includes water tank, water pump and cooler, and the water pump is placed in inside water tank, water pump and cooler
Between be communicated with water inlet pipe and outlet pipe；
The drainage system includes the drainpipe being connected to cucurbit bottom, and the drainpipe is equipped with solenoid valve, described
Solenoid valve is fixed on the 4th partition, and the drainpipe is connected with draining gathering tube, is offered on the casing and is converged with draining
The corresponding drainpipe outlet of general pipeline.
The working principle of the utility model are as follows:
After cucurbit is added in experimental liquid and water sample, rubber stopper, heating device steam the ammonia and nitrogen components in water sample beyond the Great Wall, with
Water sample separates, and air pump provides gas source for distillation in aerating system, provides power for the absorption of ammonia nitrogen, makes ammonia nitrogen steam by gas
Impact to upstream, and be largely gathered in imitative nitrogen ball bubble, to be easier to enter cooler, cooling system to ammonia nitrogen steam into
Row condensation, the water that condensate liquid flow in absorption bottle and is absorbed, while separating are flowed out from cucurbit bottom through drainpipe.
Further, the heating device is arranged between first partition and second partition, and the cucurbit bottom is fixed
Inside heating device, heating device is separated with first partition and second partition, other glass apparatus is avoided direct contact with and makes
At damage, while playing fixed function.
Further, the cooler is serpentine condenser, and the absorption bottle is set on the casing immediately below cooler, institute
The casing internal that water tank is placed below absorption bottle is stated, film-cooled heat can be increased using serpentine condenser, is conducive to accelerate ammonia
The condensation of nitrogen.
Further, the aerating system further includes the gas flowmeter being arranged between air pump and check valve, the gas
The tolerance of flowmeter body is adjusted to 0.25L/min, and gas flowmeter can be adjusted gas flow, to reach best ammonia
Nitrogen steams effect.
Further, the absorption bottle is provided with boric acid, and boric acid absorbs the ammonia and nitrogen components steamed.
In conclusion by adopting the above-described technical solution, the beneficial effects of the utility model are:
It is the suction of ammonia nitrogen 1. the utility model, by the way that cucurbit to be connected to aerating system, air pump provides gas source for distillation
It receives and power is provided, in cucurbit, impact meeting Xiang Shangliu of the ammonia nitrogen steam by gas is more conducive to the extraction of ammonia nitrogen, has
Conducive to measured value analysis, error is reduced.
2. the utility model by above the distillation ball of cucurbit bubble integrally formed imitative nitrogen ball steep, and by air inlet pipe
Distillation bottle body bottom is protruded into one end, ramps up gas from distillation bottle body bottom, and ammonia nitrogen steam is up gathered in imitative nitrogen ball bubble,
Entered in absorption bottle by ammonia nitrogen steam outleting pipe in communication again, while cooperating rubber stopper beyond the Great Wall, can prevent ammonia nitrogen at
It shunts and loses, separate ammonia and nitrogen components utmostly, test sample is more accurate.
3. the utility model sets four Distallation systms altogether, four groups of water samples can be detected simultaneously, improve work effect
Rate has saved the time.
Detailed description of the invention
The utility model will illustrate by example and with reference to the appended drawing, in which:
Fig. 1 is the structural schematic diagram of the utility model；
Fig. 2 is the cross-sectional view of the utility model；
Fig. 3 is the cucurbit structure chart of the utility model；
Fig. 4 is the utility model internal structure chart.
In the figure, it is marked as 1- casing, 2- Distallation systm, 21- cucurbit, 211- imitate nitrogen ball bubble, 212- distills ball bubble, 213-
Distill bottle body, 214- evacuated tube, 215- distillation cascade, 216- air inlet pipe, 217- adding mouth, 22- rubber stopper, 23- absorption bottle, 24-
Heating device, 25- ammonia nitrogen steam outleting pipe, 3- aerating system, 31- air pump, 32- check valve, 33- aeration tube, 34- gas flow
Meter, 4- cooling system, 41- water tank, 42- water pump, 43- water inlet pipe, 44- outlet pipe, 45- cooler, 47- water tank door, 5- draining
System, 51- solenoid valve, 52- drainpipe, 53- drain gathering tube, 54- drainpipe outlet, 6- liquid crystal touch screen, the main partition of 7-, 8-
First partition, 9- second partition, 10- third partition, 11- electric cabinet, the 4th partition of 12-.
Specific embodiment
All features disclosed in this specification can be with any other than mutually exclusive feature and/or step
Mode combines.
It elaborates with reference to the accompanying drawing to the utility model.
Embodiment 1
A kind of ammonia nitrogen low temperature distillation bottle, including distillation bottle body 213,213 top of distillation bottle body is integrally formed with distillation
Ball bubble 212,212 top of distillation ball bubble is integrally formed with imitative nitrogen ball bubble 211, and the 21 body bottom of cucurbit is integrally formed with emptying
Pipe 214, distillation ball steep 212 sides and are equipped with air inlet pipe 216, imitate 211 sides of nitrogen ball bubble and are equipped with distillation cascade 215, the imitative nitrogen ball bubble
211 tops are equipped with adding mouth 217, and gas enters inside distillation bottle body 213 from air inlet pipe 216, distill ingredient from distillation cascade 215
Discharge, the evacuated tube 214 of bottom the water after separation can be discharged.
Embodiment 2
On the basis of embodiment 1, described 215 one end of distillation cascade is extend into inside imitative nitrogen ball bubble 211, and the other end vacantly exists
Imitative 211 outside of nitrogen ball bubble, connect convenient for distillation cascade 215 with other pipelines.
Embodiment 3
On the basis of embodiment 1, described 216 one end of air inlet pipe is extend into inside distillation bottle body 213, and extends to distillation
The bottom of bottle body 213, for the other end vacantly in 212 outside of distillation ball bubble, the bottom that air inlet pipe 216 extends to distillation bottle body 213 can
So that the gas entered farthest separates ammonia and nitrogen components from distillation 213 bottom of bottle body toward rising.
Embodiment 4
A kind of ammonia nitrogen cryogenic alembic, including casing 1, cooling system 4, drainage system 5, Distallation systm 2 and aerating system
3, there are four the Distallation systm 2 is set；
Cucurbit 21 of the Distallation systm 2 including being fixed on 1 top of casing, the heating device 24 of 21 lower part of cucurbit,
Absorption bottle 23 and ammonia nitrogen steam outleting pipe 25, the bottleneck of the cucurbit 21 are plugged with rubber stopper 22, the ammonia nitrogen steam outleting pipe
25 one end are connected to absorption bottle 23, and the other end is connected to the distillation cascade 215 of cucurbit 21；
The aerating system 3 includes air pump 31, aeration tube 33 and the check valve 32 being arranged on aeration tube 33, the aeration
33 one end of pipe connects air pump 31, and the other end is connected to the air inlet pipe 216 of cucurbit 21；
The cooling system 4 includes water tank 41, water pump 42 and cooler 45, and the water pump 42 is placed in 41 the inside of water tank,
Water inlet pipe 43 and outlet pipe 44 are communicated between water pump 42 and cooler 45；
The drainage system 5 includes the drainpipe 52 being connected to 21 bottom of cucurbit, and the drainpipe 52 is equipped with electromagnetism
Valve 51, the solenoid valve 51 are fixed on the 4th partition 12, and the drainpipe 52 is connected with draining gathering tube 53, the casing
Drainpipe 52 corresponding with draining gathering tube 53 is offered on 1 to export.
After cucurbit 21 is added in experimental liquid and water sample, rubber stopper 22, heating device 24 make the ammonia and nitrogen components in water sample beyond the Great Wall
It steams, is separated with water sample, air pump 31 provides gas source for distillation in aerating system 3, provides power for the absorption of ammonia nitrogen, steams ammonia nitrogen
Vapour by gas impact to upstream, and be largely gathered in imitative nitrogen ball bubble 211, it is cooling to be easier to enter cooler 45
System 4 condenses ammonia nitrogen steam, and condensate liquid flow in absorption bottle 23 and is absorbed, while the water separated is from cucurbit 21
It is flowed out through drainpipe 52 bottom.
Embodiment 5
On the basis of embodiment 4, the heating device 24 is arranged between first partition 8 and second partition 9, the steaming
It evaporates 21 bottom of bottle and is fixed on 24 the inside of heating device, heating device 24 is separated with first partition 8 and second partition 9, is avoided straight
It contacts other glass apparatus to cause to damage, while playing fixed function.
Embodiment 6
On the basis of embodiment 4, the cooler 45 is serpentine condenser, and the absorption bottle 23 is being set to cooler 45 just
On the casing 1 of lower section, the water tank 41 is placed on inside the casing 1 of 23 lower section of absorption bottle, can be increased using serpentine condenser
Film-cooled heat is conducive to the condensation for accelerating ammonia nitrogen.
Embodiment 7
On the basis of embodiment 4, the aerating system 3 further includes the gas being arranged between air pump 31 and check valve 32
Flowmeter 34, the tolerance of the gas flowmeter 34 are adjusted to 0.25L/min, and gas flowmeter 34 can carry out gas flow
It adjusts, effect is steamed with the ammonia nitrogen for reaching best.
Embodiment 8
On the basis of embodiment 4, the absorption bottle 23 is provided with boric acid, and boric acid inhales the ammonia and nitrogen components steamed
It receives.
Claims (8)
1. a kind of ammonia nitrogen low temperature distillation bottle, including distillation bottle body (213), which is characterized in that one at the top of the distillation bottle body (213)
Body formed to have distillation ball bubble (212), (211) are steeped integrally formed with imitative nitrogen ball in distillation ball bubble (212) top, the distillation bottle body
(213) bottom distills ball bubble (212) side and is equipped with air inlet pipe (216), imitate nitrogen ball bubble (211) integrally formed with evacuated tube (214)
Side is equipped with distillation cascade (215), is equipped with adding mouth (217) at the top of the imitative nitrogen ball bubble (211).
2. a kind of ammonia nitrogen low temperature distillation bottle according to claim 1, described distillation cascade (215) one end extend into imitative nitrogen ball bubble
(211) internal, the other end is vacantly on the outside of imitative nitrogen ball bubble (211).
3. a kind of ammonia nitrogen low temperature distillation bottle according to claim 1, described air inlet pipe (216) one end extend into distillation bottle body
(213) internal, and the bottom of distillation bottle body (213) is extended to, the other end is vacantly on the outside of distillation ball bubble (212).
4. a kind of ammonia nitrogen cryogenic alembic, including casing (1), cooling system (4) and drainage system (5), which is characterized in that also wrap
Distallation systm (2) and aerating system (3) are included, there are four the Distallation systm (2) sets；
The Distallation systm (2) includes the cucurbit (21) for being fixed on casing (1) top, the heating device of cucurbit (21) lower part
(24), the bottleneck of absorption bottle (23) and ammonia nitrogen steam outleting pipe (25), the cucurbit (21) is plugged with rubber stopper (22), the ammonia
Nitrogen vapor escape pipe (25) one end is connected to absorption bottle (23), and the other end is connected to the distillation cascade (215) of cucurbit (21)；
The aerating system (3) includes air pump (31), aeration tube (33) and the check valve (32) being arranged on aeration tube (33), institute
Aeration tube (33) one end connection air pump (31) is stated, the other end is connected to the air inlet pipe (216) of cucurbit (21)；
The cooling system (4) includes water tank (41), water pump (42) and cooler (45), and the water pump (42) is placed in water tank
(41) the inside, is communicated with water inlet pipe (43) and outlet pipe (44) between water pump (42) and cooler (45)；
The drainage system (5) includes the drainpipe (52) being connected to cucurbit (21) bottom, and the drainpipe (52) is equipped with
Solenoid valve (51), the solenoid valve (51) are fixed on the 4th partition (12), the drainpipe (52) with draining gathering tube
(53) it is connected, drainpipe (52) corresponding with draining gathering tube (53) is offered on the casing (1) and is exported.
5. a kind of ammonia nitrogen cryogenic alembic according to claim 4, the heating device (24) is arranged in first partition (8)
Between second partition (9), cucurbit (21) bottom is fixed on inside heating device (24).
6. a kind of ammonia nitrogen cryogenic alembic according to claim 4, the cooler (45) is serpentine condenser, the suction
It receives bottle (23) to be set on the casing (1) immediately below cooler (45), the water tank (41) is placed on the machine below absorption bottle (23)
Shell (1) is internal.
7. a kind of ammonia nitrogen cryogenic alembic according to claim 4, the aerating system (3) further includes being arranged in air pump
(31) tolerance of the gas flowmeter (34) between check valve (32), the gas flowmeter (34) is adjusted to 0.25L/min.
8. a kind of ammonia nitrogen cryogenic alembic according to claim 4, the absorption bottle (23) is provided with boric acid.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821682191.4U CN209155887U (en) | 2018-10-17 | 2018-10-17 | A kind of ammonia nitrogen low temperature distillation bottle and ammonia nitrogen cryogenic alembic |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821682191.4U CN209155887U (en) | 2018-10-17 | 2018-10-17 | A kind of ammonia nitrogen low temperature distillation bottle and ammonia nitrogen cryogenic alembic |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN209155887U true CN209155887U (en) | 2019-07-26 |
Family
ID=67334003
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201821682191.4U Active CN209155887U (en) | 2018-10-17 | 2018-10-17 | A kind of ammonia nitrogen low temperature distillation bottle and ammonia nitrogen cryogenic alembic |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN209155887U (en) |
-
2018
- 2018-10-17 CN CN201821682191.4U patent/CN209155887U/en active Active
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| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20200804 Address after: Area B, third floor, Zhongxing smart Yinchuan big data center, Suyin Industrial Park, Yinchuan City, Ningxia Hui Autonomous Region, 750000 Patentee after: Yinchuan Lianhua Technology Development Co., Ltd Address before: 730060 4th Floor, Building A, 256 Xigudong Road, Xigu District, Lanzhou City, Gansu Province Patentee before: LANZHOU LIANHUA ENVIRONMENTAL PROTECTION TECHNOLOGY Co.,Ltd. |