CN209123904U - A kind of Chemical Manufacture reaction kettle - Google Patents
A kind of Chemical Manufacture reaction kettle Download PDFInfo
- Publication number
- CN209123904U CN209123904U CN201821592745.1U CN201821592745U CN209123904U CN 209123904 U CN209123904 U CN 209123904U CN 201821592745 U CN201821592745 U CN 201821592745U CN 209123904 U CN209123904 U CN 209123904U
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- CN
- China
- Prior art keywords
- autoclave body
- storehouse
- mixing chamber
- middle position
- motor
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Abstract
The utility model discloses a kind of Chemical Manufacture reaction kettles, including autoclave body, the two sides of the autoclave body bottom are symmetrically installed with outlet valve, the bottom of the autoclave body two sides is equipped with the first support plate, the side of the autoclave body inner bottom is equipped with the second refrigerator, second support plate is installed, and the middle position of the second support plate is provided with through-hole, is equipped with annular groove at the top of second support plate above the second refrigerator on the inside of the autoclave body.Utility model device passes through the mutual cooperation of first motor, first gear, tooth form casing, second gear, rotation axis, annular groove, movable pulley, centrifugation rotation operation is carried out to mixing chamber, and pass through the mutual cooperation of the second motor and agitating paddle, mixed solution inside mixing chamber is stirred, so that mixed effect is more preferable, improve mixed speed, reduce the time of reaction, and the solution position inside mixing chamber is incuded by water level sensor, it avoids solution from splashing, flows out the inside of mixing chamber.
Description
Technical field
The utility model relates to Chemical Manufacture equipment technical field, specially a kind of Chemical Manufacture reaction kettle.
Background technique
(R)-(+) -2- (4- hydroxyphenoxy) methyl propionate, referred to as: MAQ is (R)-(+) -2- (4- hydroxyphenoxy)
The derived product of propionic acid is the important intermediate for synthesizing the Chiral pesticides such as high lid, clodinafop-propargyl, cover grass energy, quizalofopethyl, height lid, alkynes
Careless ester, cover grass energy, quizalofopethyl etc. are efficient, highly selective, low-residual aryloxyphenoxypropionate class herbicides, can be to prevent
Except 1 year or perennial gramineae weed, it is very suitable for using in fields such as soybean, cotton, rape and vegetables, methyl propionate
Production stage is more various, needs to use reaction kettle, and existing reaction kettle structure is more inflexible, function is more single, mostly
The production procedure of methyl propionate can not independently be met, and the mixed effect in existing reaction kettle is poor, the product quality produced
It is uneven.
Utility model content
The purpose of this utility model is to provide a kind of Chemical Manufacture reaction kettles, to solve to propose in above-mentioned background technique
The problem of.
To achieve the above object, the utility model provides the following technical solutions: a kind of Chemical Manufacture reaction kettle, including kettle
Body, the two sides of the autoclave body bottom are symmetrically installed with outlet valve, and the bottom of the autoclave body two sides is equipped with the first support plate, described
The side of autoclave body inner bottom is equipped with the second refrigerator, is equipped with second above the second refrigerator on the inside of the autoclave body
Fagging, and the middle position of the second support plate is provided with through-hole, is equipped with annular groove at the top of second support plate, institute
That states annular groove is internally provided with multiple groups movable pulley, and the top of movable pulley described in multiple groups is equipped with mixing chamber jointly, described to stir
The middle position for mixing orlop portion is equipped with solenoid valve, is provided with water level sensor at the top of side on the inside of the mixing chamber, institute
It states the middle position on the outside of mixing chamber and tooth form casing is installed, the middle position of the autoclave body side is provided with the first rotation
Storehouse, it is described first rotation storehouse inside bottom end first motor is installed, be equipped on the outside of the output end of the first motor with
The intermeshing first gear of tooth form casing, the autoclave body are equipped with second turn far from the middle position of the first rotation storehouse side
Storehouse is moved, rotation axis is installed between the middle position of the top and bottom inside second rotation storehouse, the rotation axis
Be equipped on side wall with the intermeshing second gear of tooth form casing, be arranged with kettle cover, the kettle cover at the top of the mixing chamber
The two sides at top are all provided with feed inlet, and feed inlet extends to the inside of mixing chamber, the middle position at the top of the kettle cover
It is provided with the second motor, the output end of second motor is equipped with agitating paddle, and agitating paddle is located at the inside of mixing chamber, described
Bottom end inside mixing chamber is provided with electric heating wire storehouse, and electric heating wire storehouse is internally provided with multiple groups electric heating wire, the kettle
Body is rotated far from first is equipped with air pump at the top of the one end of storehouse side, and the input terminal of air pump is provided with air inlet pipe, and air pump is logical
The inside for crossing air inlet pipe and autoclave body is interconnected, and the autoclave body is equipped with collection far from the bottom of first rotation storehouse side one end
Storehouse, and refrigeration storehouse is installed at the top of collecting bin, the refrigeration storehouse is equipped with the first refrigerator, the system far from the side of autoclave body
Cold storehouse is internally provided with condenser pipe, and the first refrigerator and condenser pipe are interconnected, and the output end of the air pump is equipped with row
Tracheae, and condenser pipe of the exhaust pipe inside refrigeration storehouse extends to the inside of collecting bin, the output end of the air pump passes through row
Tracheae and collecting bin are interconnected, and the middle position of described autoclave body one end side is equipped with control panel.
Preferably, sealing cover is provided at the top of the feed inlet.
Preferably, teflon coatings are provided on the outside of the agitating paddle.
Preferably, the middle position of autoclave body front bottom is provided with observation window.
Preferably, the bottom of first support plate is provided with multiple groups anti-skid bulge.
Preferably, it is provided with motor bin on the outside of second motor, and motor bin is internally provided with damping and silencing cotton.
Compared with prior art, the utility model has the beneficial effects that the Chemical Manufacture with reaction kettle by first motor,
The mutual cooperation of first gear, tooth form casing, second gear, rotation axis, annular groove, movable pulley, is centrifuged mixing chamber
Rotation operation, and pass through the mutual cooperation of the second motor and agitating paddle, the mixed solution inside mixing chamber is stirred, so that
Mixed effect is more preferable, improves the speed of mixing, reduces the time of reaction, and by water level sensor to the solution inside mixing chamber
Position is incuded, and solution is avoided to splash, and flows out the inside of mixing chamber, mixing while can be by electric heating wire storehouse inside
Electric heating wire carries out heating mixing, while can also carry out distillation procedure to device internal solution, improve device accuracy and
Functionality, after device distills device by the mutual cooperation of air inlet pipe, air pump, exhaust pipe, the first refrigerator and condenser pipe
Gas is condensed, and is individually collected, and the reaction effect of device is improved, and reduces production cost, environmentally protective.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the utility model；
Fig. 2 is the main view of the utility model；
Fig. 3 is structure enlargement diagram at the A of the utility model.
In figure: 1, autoclave body；2, outlet valve；3, the first support plate；4, solenoid valve；5, the second support plate；6, annular groove；7,
Movable pulley；8, electric heating wire storehouse；9, first motor；10, the first rotation storehouse；11, first gear；12, tooth form casing；13, it stirs
Storehouse；14, water level sensor；15, kettle cover；16, feed inlet；17, the second motor；18, agitating paddle；19, air inlet pipe；20, air pump；
21, the first refrigerator；22, condenser pipe；23, collecting bin；24, control panel；25, exhaust pipe；26, the second rotation storehouse；27, freeze
Storehouse；28, second gear；29, rotation axis；30, the second refrigerator.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model
Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole
Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work
Every other embodiment obtained, fall within the protection scope of the utility model.
Fig. 1-3 is please referred to, a kind of embodiment provided by the utility model: a kind of Chemical Manufacture reaction kettle, including autoclave body
1, the two sides of 1 bottom of autoclave body are symmetrically installed with outlet valve 2, the use model 4V210-08 of the solenoid valve, the bottom of 1 two sides of autoclave body
Portion is equipped with the first support plate 3, and the side of 1 inner bottom of autoclave body is equipped with the second refrigerator 30, the model of the refrigerator
The top of CBE-330WNO, the second refrigerator 30 of 1 inside of autoclave body are equipped with the second support plate 5, and the centre of the second support plate 5
Through-hole is provided at position, the top of the second support plate 5 is equipped with annular groove 6, and the multiple groups that are internally provided with of annular groove 6 are slided
Driving wheel 7, the top of multiple groups movable pulley 7 are equipped with mixing chamber 13 jointly, and the middle position of 13 bottom of mixing chamber is equipped with electromagnetism
Valve 4, the use model 4V210-08 of the solenoid valve, mixing chamber are provided with water level sensor at the top of 13 inside side, the water
The middle position of the use model 14WMB-FS of level sensor, 13 outside of mixing chamber are equipped with tooth form casing 12, autoclave body 1 one
The middle position of side is provided with the first rotation storehouse 10, and the bottom end inside the first rotation storehouse 10 is equipped with first motor 9, the motor
Use model Y90S-2, be equipped with and intermeshing first tooth of tooth form casing 12 on the outside of the output end of first motor 9
Wheel 11, autoclave body 1 are equipped with the second rotation storehouse 26 far from the middle position of the first rotation 10 side of storehouse, and second rotates inside storehouse 26
Top and bottom middle position between rotation axis 29 is installed, be equipped on the side wall of rotation axis 29 and tooth form casing 12
Intermeshing second gear 28, the top of mixing chamber 13 are arranged with kettle cover 15, and the two sides at 15 top of kettle cover are all provided with charging
Mouth 16, and feed inlet 16 extends to the inside of mixing chamber 13, the middle position at 15 top of kettle cover is provided with the second motor 17, should
The use model Y90S-2 of motor, the output end of the second motor 17 is equipped with agitating paddle 18, and agitating paddle 18 is located at mixing chamber
13 inside, the bottom end inside mixing chamber 13 be provided with electric heating wire storehouse 8, and electric heating wire storehouse 8 is internally provided with multiple groups electricity
Heater strip, the use model 0Cr21Al6Nb of the electric heating wire, top peace of the autoclave body 1 far from first rotation 10 side one end of storehouse
Equipped with air pump 20, the use model MOA-P101-CD of the air pump, and the input terminal of air pump 20 is provided with air inlet pipe 19, and gas
Pump 20 is interconnected by the inside of air inlet pipe 19 and autoclave body 1, bottom installation of the autoclave body 1 far from first rotation 10 side one end of storehouse
There is collecting bin 23, and the top of collecting bin 23 is equipped with refrigeration storehouse 27, storehouse 27 of freezing is equipped with the first system far from the side of autoclave body 1
Cooler 21, the model CBE-330WNO of the refrigerator, refrigeration storehouse 27 are internally provided with condenser pipe 22, and the first refrigerator 21
It is interconnected with condenser pipe 22, the output end of air pump 20 is equipped with exhaust pipe 25, and exhaust pipe 25 is inside refrigeration storehouse 27
Condenser pipe 22 extends to the inside of collecting bin 23, and the output end of air pump 20 is interconnected by exhaust pipe 25 and collecting bin 23, kettle
The middle position of 1 one end side of body is equipped with control panel 24, the use model JG-128C of the control panel, control plane
Plate 24 by conducting wire respectively with electric heating wire, first motor 9, the second motor 17, air pump 20, the first refrigerator, control panel 24
With the second refrigerator 30 be electrically connected, control panel 24 by electric signal respectively with outlet valve 2, solenoid valve 4 and water level sensor 14
It is electrically connected, outlet valve 2, solenoid valve 4, electric heating wire, first motor 9, water level sensor 14, the second motor 17 in device,
Air pump 20, the first refrigerator, control panel 24 and the second refrigerator 30 are the prior art, composed structure and connection type and show
There is device identical.
In this embodiment, the top of feed inlet 16 is provided with sealing cover, and the outside of obturation effect, agitating paddle 18 is provided with spy
The middle position of fluorine dragon coating, anticorrosion, the positive bottom of autoclave body 1 is provided with observation window, observes inner case, the first support plate
3 bottom is provided with multiple groups anti-skid bulge, anti-skidding, and the outside of the second motor 17 is provided with motor bin, and the inside of motor bin is set
It is equipped with damping and silencing cotton, the second motor 17 is protected, while also guaranteeing the airtightness of device.
Working principle: the device electrical component is all powered by external power supply, is powered on, and opens control panel 24,
Before use, injecting solution and solute to the inside of agitating paddle 18 by feed inlet 16, control is gone to stir by water level sensor 14
13 water level inside situation of storehouse incudes when water level is excessively high by the input terminal of water level sensor 14, then water level sensor 14
Output end transmits electric signal to control panel 24, is reminded by control panel 24 to operator, in use, passing through control
Panel 24 opens the second motor 17 and is stirred operation to the inside of mixing chamber 13, and when rotating, can be by by electric heating wire
Electric heating wire inside storehouse 8 is powered, and temperature adjusting can be carried out by control panel 24, thus molten to the mixing inside mixing chamber 13
Liquid is heated, and first gear 11 can be driven to be rotated, first gear 11 drives tooth form casing by opening first motor 9
12 and second gear 28 rotated, and slided by movable pulley 7 in the inside of annular groove 6, and then to mixing chamber
13 carry out rotation operation, can be by control panel 24 to electric heating wire when device needs to carry out distillation procedure to internal solution
Heating temperature be adjusted, by open air pump 20, low-boiling solvent vapo(u)r is extracted out, and be directed at exhaust through air inlet pipe 19
The first refrigerator 21 is opened while air pump 20 operates, by condenser pipe 22 to the steaming inside exhaust pipe 25 in the inside of pipe 25
Vapour carries out condensation operation, and the condensed inside for falling into collecting bin 23 is collected, can be by beating after device distillation
Mixed solution after distillation is fallen into the bottom of autoclave body 1 by open electromagnetic valve 4, and it is cold to mixed solution progress to open the second refrigerator 30
But, it crystallizes, crystallization finishes, and when device is centrifuged and is dried, the inside that can put into mixing chamber 13 again is carried out
Operation.
It is obvious to a person skilled in the art that the present invention is not limited to the details of the above exemplary embodiments, and
And without departing substantially from the spirit or essential attributes of the utility model, it can realize that this is practical new in other specific forms
Type.Therefore, in all respects, the present embodiments are to be considered as illustrative and not restrictive, this is practical new
The range of type is indicated by the appended claims rather than the foregoing description, it is intended that containing for the equivalent requirements of the claims will be fallen in
All changes in justice and range are embraced therein.It should not treat any reference in the claims as limiting
Related claim.
Claims (6)
1. a kind of Chemical Manufacture reaction kettle, including autoclave body (1), it is characterised in that: symmetrically pacify the two sides of autoclave body (1) bottom
Equipped with outlet valve (2), the bottom of autoclave body (1) two sides is equipped with the first support plate (3), autoclave body (1) inner bottom
Side is equipped with the second refrigerator (30), is equipped with the second support above the second refrigerator (30) on the inside of the autoclave body (1)
Plate (5), and the middle position of the second support plate (5) is provided with through-hole, is equipped with annular at the top of second support plate (5)
Sliding slot (6), the annular groove (6) are internally provided with multiple groups movable pulley (7), and the top of movable pulley (7) described in multiple groups is common
It is equipped with mixing chamber (13), the middle position of mixing chamber (13) bottom is equipped with solenoid valve (4), the mixing chamber (13)
It is provided at the top of the side of inside water level sensor (14), the middle position on the outside of the mixing chamber (13) is equipped with tooth profile sleeve
It manages (12), the middle position of autoclave body (1) side is provided with the first rotation storehouse (10), and first rotation storehouse (10) is internal
Bottom end be equipped with first motor (9), be equipped on the outside of the output end of the first motor (9) mutual with tooth form casing (12)
The first gear (11) of engagement, the autoclave body (1) are equipped with second turn far from the middle position of first rotation storehouse (10) side
It moves storehouse (26), rotation axis (29) is installed between the middle position of the internal top and bottom of second rotation storehouse (26),
It is equipped on the side wall of the rotation axis (29) and tooth form casing (12) intermeshing second gear (28), the mixing chamber
(13) it is arranged at the top of kettle cover (15), the two sides at the top of the kettle cover (15) are all provided with feed inlet (16), and feed inlet
(16) inside of mixing chamber (13) is extended to, the middle position at the top of the kettle cover (15) is provided with the second motor (17), institute
The output end for stating the second motor (17) is equipped with agitating paddle (18), and agitating paddle (18) is located at the inside of mixing chamber (13), described
The internal bottom end of mixing chamber (13) is provided with electric heating wire storehouse (8), and electric heating wire storehouse (8) are internally provided with multiple groups electric heating
Silk, the autoclave body (1) rotates far from first and is equipped with air pump (20) at the top of storehouse (10) side one end, and the input of air pump (20)
End is provided with air inlet pipe (19), and air pump (20) is interconnected by the inside of air inlet pipe (19) and autoclave body (1), the autoclave body
(1) bottom far from first rotation storehouse (10) side one end is equipped with collecting bin (23), and is equipped at the top of collecting bin (23)
Freeze storehouse (27), refrigeration storehouse (27) is equipped with the first refrigerator (21) far from the side of autoclave body (1), the refrigeration storehouse (27)
Be internally provided with condenser pipe (22), and the first refrigerator (21) and condenser pipe (22) are interconnected, the air pump (20) it is defeated
Outlet is equipped with exhaust pipe (25), and exhaust pipe (25) extends to collecting bin through the internal condenser pipe (22) of refrigeration storehouse (27)
(23) output end of inside, the air pump (20) is interconnected by exhaust pipe (25) and collecting bin (23), the autoclave body (1)
The middle position of one end side is equipped with control panel (24).
2. a kind of Chemical Manufacture reaction kettle according to claim 1, it is characterised in that: the top of the feed inlet (16)
It is provided with sealing cover.
3. a kind of Chemical Manufacture reaction kettle according to claim 1, it is characterised in that: the outside of the agitating paddle (18)
It is provided with teflon coatings.
4. a kind of Chemical Manufacture reaction kettle according to claim 1, it is characterised in that: the positive bottom of the autoclave body (1)
Middle position be provided with observation window.
5. a kind of Chemical Manufacture reaction kettle according to claim 1, it is characterised in that: first support plate (3)
Bottom is provided with multiple groups anti-skid bulge.
6. a kind of Chemical Manufacture reaction kettle according to claim 1, it is characterised in that: outside second motor (17)
Side is provided with motor bin, and motor bin is internally provided with damping and silencing cotton.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821592745.1U CN209123904U (en) | 2018-09-28 | 2018-09-28 | A kind of Chemical Manufacture reaction kettle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821592745.1U CN209123904U (en) | 2018-09-28 | 2018-09-28 | A kind of Chemical Manufacture reaction kettle |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN209123904U true CN209123904U (en) | 2019-07-19 |
Family
ID=67230643
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201821592745.1U Expired - Fee Related CN209123904U (en) | 2018-09-28 | 2018-09-28 | A kind of Chemical Manufacture reaction kettle |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN209123904U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115753769A (en) * | 2022-11-17 | 2023-03-07 | 宿迁嘉禾塑料金属制品有限公司 | PVA collodion production process and catalytic process monitoring equipment of PVA collodion production process |
-
2018
- 2018-09-28 CN CN201821592745.1U patent/CN209123904U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115753769A (en) * | 2022-11-17 | 2023-03-07 | 宿迁嘉禾塑料金属制品有限公司 | PVA collodion production process and catalytic process monitoring equipment of PVA collodion production process |
| CN115753769B (en) * | 2022-11-17 | 2024-02-23 | 宿迁嘉禾塑料金属制品有限公司 | PVA collodion production process and catalysis process monitoring equipment of PVA collodion production process |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20190719 Termination date: 20210928 |