CN209085974U - A kind of sampling of isotope assay sample trace and embedding utensil - Google Patents

A kind of sampling of isotope assay sample trace and embedding utensil Download PDF

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Publication number
CN209085974U
CN209085974U CN201821583586.9U CN201821583586U CN209085974U CN 209085974 U CN209085974 U CN 209085974U CN 201821583586 U CN201821583586 U CN 201821583586U CN 209085974 U CN209085974 U CN 209085974U
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internal pressure
embedding
trace
embedded box
wedge
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CN201821583586.9U
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林东明
陈新军
宣思鹏
韩飞
韦记朋
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Shanghai Maritime University
Shanghai Ocean University
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Shanghai Maritime University
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Abstract

The utility model relates to a kind of sampling of isotope assay sample trace and embedding utensils, spoon and encapsulation embedding two utensils of device are extracted including trace samplings, it is spoon portion that trace samplings, which extract spoon, the integral structure of embedded box groove portion, encapsulation embedding device includes pressing plate, left inside pressure shelves, right internal pressure shelves, high internal pressure wedge and low internal pressure wedge structure, the present invention realizes the convenient of stable isotope determination sample trace samplings, accurately extract and encapsulate embedding, it solves existing experimental tool and is difficult to simplicity, fast and accurately extract trace samplings, cause to be repeated several times and extract, weigh the weighing deviation generated during trace samplings, the problems such as sample is contaminated;Solve the problem of existing experimental tool extracts because trace is repeated several times, weighs sample, and encapsulation embedding tool shortage, experimental cost and its time cost is caused to be increased.

Description

A kind of sampling of isotope assay sample trace and embedding utensil
Technical field
The invention belongs to field of biotechnology more particularly to existing isotope mass spectrometer to be applied to siphonopods, fish isogonism When the carbon of the soft tissues such as the sclerous tissues such as matter jaw, inner casing and muscle, sexual gland, nitrogen stable isotope determination trace samplings sampling and Embed utensil.
Background technique
When carrying out the bioecologys such as siphonopods, fish, breeding ecology research, the survey of the stable isotopes such as carbon, nitrogen Setting analysis is an important research contents.It was distributed in marine food web nutrition relationship, the breeding Energy input of these types Cheng Zhong, ingest source, surplus Energy input method of salary distribution etc. of ingesting of food organisms decide growth, development, and final numerous Spread out activity and tactful selection adaptation of laying eggs.With the development of current engineering technology, Measurement for Biochemistry, stable isotope skill Art has become one kind maturely and is widely used in the research of marine organisms Feeding Ecology, marine organisms breeding ecology, It can be with the consumer organism source of tracer marine organisms, the accumulation of individual surplus energy of ingesting and its distribution etc..The stabilization used is same The plain instrument in position has the advantages that simple, easy, safely and fast isotopic masses such as measurement carbon, nitrogen.
In general, needing to carry out 1.0mg~1.5mg to dry tissue samples before carrying out tissue stabilization isotope assay The extraction and encapsulation embedding of trace pulverized specimen.However, it is limited to the tool limitation that current trace samplings extract and encapsulation embeds, it is difficult Tissue pulverized specimen is extracted with disposably trace, and extracts with needing multiplicating property-weighs, increase extraction-weighing, even It is that trace subtracts and takes-weigh.In this way, the muptiple-use step that repeats is easy to cause the trace samplings that finally weigh there are deviation, to survey Determine result and subsequent analysis and research generate very big otherness;Meanwhile this repetition extraction-weighing step, definitely increasing Add sample is contaminated to happen, has increased the uncertainty and its error of measurement result.It is mentioned in addition, trace is repeated several times After taking-weighing, existing experimental tool can not easily encapsulate embedded samples, increase experimental cost and its time at This.
Therefore, in the stable isotope determination analysis of tissue samples, as far as possible easy, quick, accurately trace is needed Tissue pulverized specimen is extracted, and is quickly and conveniently packaged embedding to it, to minimize the weighing error of trace samplings, drop Low experimental cost and its time cost, and reduced to the maximum extent by repeating to measure the issuable dirt of institute in extraction process Dye happens.
Summary of the invention
Technical problem solved by the invention be to provide a kind of isotope assay sample trace sampling and embedding utensil with Solve the disadvantage in above-mentioned background technique.
Technical problem solved by the invention is realized using following technical scheme:
A kind of sampling of isotope assay sample trace and embedding utensil, including trace samplings extract spoon and encapsulation embedding device two A utensil, trace samplings extract spoon be spoon portion, embedded box groove portion integral structure, encapsulation embedding device include pressing plate, left inside pressure shelves, Right internal pressure shelves, high internal pressure wedge and low internal pressure wedge structure;Left inside pressure shelves, right internal pressure shelves, high internal pressure are fixed in the pressing plate one side Wedge and low internal pressure wedge, for encapsulating embedded box, another side is to design for whole plane, for being compacted embedded box;
Further, the spoon portion is thin rod shape extended pattern, is about 50.0mm, diameter 1.5mm;The end in the spoon portion For circular shallow grooves, diameter 1.5mm, maximum groove depth 0.3mm;
Further, the embedded box groove portion is flat extended pattern, is about 60.0mm, wide about 11.0mm, thick about 3.0mm;It is open rectangular recess in the middle part of the end of the embedded box, for being placed in and holding in the palm steady embedded box, groove is about 15.0mm, groove width about 5.0mm, groove depth about 1.8mm;
Further, the pressing plate is about 20.0mm, wide about 10.5mm, thickness about 0.6mm;
Further, narrow frame of the left and right internal pressure shelves for internal pressure embedded box, the high about 3.0mm of shelves, base portion are wide about 3.5mm, thickness about 0.5mm, inside are 1/4 arc structure, radius 3.0mm;
Further, the high and low internal pressure wedge is used for the Wide frame of internal pressure embedded box, the high about 2.5mm of high internal pressure wedge, base The wide about 3.0mm in portion, about 45 ° of wedge oblique angle;The high about 1.8mm of low internal pressure wedge, the wide about 3.0mm of base portion, about 30 ° of wedge oblique angle;
The present invention realizes convenient, accurately extraction and the encapsulation embedding of stable isotope determination sample trace samplings, has Beneficial effect is: solving existing experimental tool and is difficult to easy, quick and accurately extracts trace samplings, multiplicating is caused to mention It takes, weigh the problems such as weighing deviation generated during trace samplings, sample are contaminated;Existing experimental tool is solved because repeatedly heavy Multiple trace extracts, weighs sample, and encapsulation embedding tool lacks, and causes what experimental cost and its time cost be increased to ask Topic.
Detailed description of the invention
Fig. 1 is that trace samplings of the invention extract spoon structural schematic diagram one;
Fig. 2 is that trace samplings of the invention extract spoon structural schematic diagram two;
Fig. 3 is that encapsulation of the invention embeds device structural schematic diagram one;
Fig. 4 is that encapsulation of the invention embeds device structural schematic diagram two;
Fig. 5 is that encapsulation of the invention embeds device structural schematic diagram three;
Specific embodiment
In order to be easy to understand the technical means, the creative features, the aims and the efficiencies achieved by the present invention, tie below Conjunction is specifically illustrating, and the present invention is further explained.
As shown in Figs. 1-5: trace extracts sample and encapsulates embedding utensil when a kind of stable isotope determination, mainly by trace Two utensil compositions such as sample extraction spoon and encapsulation embedding device.
As shown in Figs. 1-2: trace samplings extract the integral structure that spoon is spoon portion 1, embedded box groove portion 2.Spoon portion 1 is thin rod shape Extended pattern is about 50.0mm, diameter 1.5mm for convenient, the accurate extraction of trace samplings;End is circular shallow grooves, directly Diameter 1.5mm, maximum groove depth 0.3mm.Embedded box groove portion 2 is flat extended pattern, is about 60.0mm, wide about 11.0mm, thick about 3.0mm;It is open rectangular recess in the middle part of end, for being placed in and holding in the palm steady embedded box, groove is about 15.0mm, and groove width is about 5.0mm, groove depth about 1.8mm.
As in Figure 3-5: encapsulation embedding device is pressing plate 3, left inside pressure shelves 4, right internal pressure shelves 5, high internal pressure wedge 6 and low internal pressure The structure compositions such as wedge 7.Pressing plate 3 is about 20.0mm, wide about 10.5mm, thickness about 0.6mm;Left inside pressure shelves are fixed in 3 one side of pressing plate 4, right internal pressure shelves 5, high internal pressure wedge 6 and low internal pressure wedge 7, for quickly and conveniently encapsulating embedded box, another side is that whole plane is set Meter, for being compacted embedded box.Narrow frame of the left and right internal pressure shelves for internal pressure embedded box, the high about 3.0mm of shelves, base portion are wide about 3.5mm, thickness about 0.5mm, inside are 1/4 arc structure, radius 3.0mm.High and low internal pressure wedge is used for the broadside of internal pressure embedded box Frame, the high about 2.5mm of high internal pressure wedge, the wide about 3.0mm of base portion, about 45 ° of wedge oblique angle;The high about 1.8mm of low internal pressure wedge, base portion are wide about 3.0mm, about 30 ° of wedge oblique angle.High and low internal pressure wedge can be designed so that the Wide frame of embedded box is successively pressed into, and avoid both sides The occurrence of being expanded outwardly caused by when frame is because of encapsulation embedding.
The above shows and describes the basic principles and main features of the present invention and the advantages of the present invention.The technology of the industry Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this The principle of invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these changes Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its Equivalent thereof.

Claims (6)

1. a kind of isotope assay sample trace sampling and embedding utensil, including trace samplings extract spoon and encapsulation embedding device two Utensil, the trace samplings extract the integral structure that spoon is spoon portion, embedded box groove portion, and the encapsulation embedding device includes pressing plate, a left side Internal pressure shelves, right internal pressure shelves, high internal pressure wedge and low internal pressure wedge structure, be fixed in the pressing plate one side left inside pressure shelves, right internal pressure shelves, High internal pressure wedge and low internal pressure wedge, for encapsulating embedded box, another side designs for whole plane, for being compacted embedded box.
2. a kind of isotope assay sample trace sampling according to claim 1 and embedding utensil, which is characterized in that described Spoon portion be thin rod shape extended pattern, be about 50.0mm, diameter 1.5mm;The end in the spoon portion is circular shallow grooves, diameter 1.5mm, maximum groove depth 0.3mm.
3. a kind of isotope assay sample trace sampling according to claim 1 and embedding utensil, which is characterized in that described Embedded box groove portion be flat extended pattern, be about 60.0mm, wide about 11.0mm, thickness about 3.0mm;In the middle part of the end of the embedded box For open rectangular recess, for being placed in and holding in the palm steady embedded box, groove is about 15.0mm, and groove width about 5.0mm, groove depth is about 1.8mm。
4. a kind of isotope assay sample trace sampling according to claim 1 to 3 and embedding utensil, feature exist In the pressing plate is about 20.0mm, wide about 10.5mm, thickness about 0.6mm.
5. a kind of isotope assay sample trace sampling according to claim 4 and embedding utensil, which is characterized in that described Left and right internal pressure shelves be used for internal pressure embedded box narrow frame, the high about 3.0mm of shelves, the wide about 3.5mm of base portion, thickness about 0.5mm, inside For 1/4 arc structure, radius 3.0mm.
6. a kind of isotope assay sample trace sampling according to claim 5 and embedding utensil, which is characterized in that described High and low internal pressure wedge be used for internal pressure embedded box Wide frame, the high about 2.5mm of high internal pressure wedge, the wide about 3.0mm of base portion, wedge oblique angle is about 45°;The high about 1.8mm of low internal pressure wedge, the wide about 3.0mm of base portion, about 30 ° of wedge oblique angle.
CN201821583586.9U 2018-09-27 2018-09-27 A kind of sampling of isotope assay sample trace and embedding utensil Active CN209085974U (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109141963A (en) * 2018-09-27 2019-01-04 上海海洋大学 A kind of sampling of isotope assay sample trace and embedding utensil

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109141963A (en) * 2018-09-27 2019-01-04 上海海洋大学 A kind of sampling of isotope assay sample trace and embedding utensil

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