CN209076672U - A kind of high-efficiency adsorbent preparation facilities of nitrogen-methane - Google Patents

A kind of high-efficiency adsorbent preparation facilities of nitrogen-methane Download PDF

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Publication number
CN209076672U
CN209076672U CN201821497729.4U CN201821497729U CN209076672U CN 209076672 U CN209076672 U CN 209076672U CN 201821497729 U CN201821497729 U CN 201821497729U CN 209076672 U CN209076672 U CN 209076672U
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CN
China
Prior art keywords
autoclave body
nitrogen
methane
discharge port
preparation facilities
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201821497729.4U
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Chinese (zh)
Inventor
田伟
吴运治
勾华杰
原星
刘晨
宋晓琳
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
HENAN HUANYU PETROCHEMICAL EQUIPMENT TECHNOLOGY Co Ltd
Original Assignee
HENAN HUANYU PETROCHEMICAL EQUIPMENT TECHNOLOGY Co Ltd
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Publication date
Application filed by HENAN HUANYU PETROCHEMICAL EQUIPMENT TECHNOLOGY Co Ltd filed Critical HENAN HUANYU PETROCHEMICAL EQUIPMENT TECHNOLOGY Co Ltd
Priority to CN201821497729.4U priority Critical patent/CN209076672U/en
Application granted granted Critical
Publication of CN209076672U publication Critical patent/CN209076672U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model discloses a kind of high-efficiency adsorbent preparation facilities of nitrogen-methane, including autoclave body, agitating device, agitating device includes stirring motor, agitating shaft, stirrer paddle, it is characterized by: the autoclave body side wall is provided with electric heating wire, autoclave body outer wall is provided with thermal insulation layer, stirring motor is arranged above autoclave body, stirring motor is connect with agitating shaft by shaft coupling, autoclave body top is provided with feed opening, thermo detector, manometer, vacuum orifice, autoclave body lower part is provided with discharge port, carbon dioxide mouth, discharge port is connected with high-temperature valve, cooling storehouse is connected with below high-temperature valve, cooling storehouse lower part is provided with cooling bin discharge port external.The beneficial effects of the utility model are for convenience of nitrogen-methane adsorbent industrial volume production, and stringent to monitor batch production technique condition, agitating device increases the efficiency of adsorbent volume production.

Description

A kind of high-efficiency adsorbent preparation facilities of nitrogen-methane
Technical field
The utility model relates to adsorbent Preparation equipment field, prepared by the high-efficiency adsorbent of especially a kind of nitrogen-methane Device.
Background technique
The country primarily directed in coal bed gas (coal mine gas), is reinforced to extraction coal seam by nitrogen-methane Separation Research The comprehensive utilization of gas, for saving using the energy, ensureing that safety of coal mines, tool of preserving the ecological environment have very important significance.Nitrogen- The high-efficiency adsorbent of methane is to the important adsorbent being commonly used in methane PSA technique, and the prior art is to nitrogen-methane height The technical process for imitating adsorbent is to choose suitable molecular sieves, molecular sieve activation, molecular sieve reaming etc., but industrial production is also Lack special preparation facilities.
Summary of the invention
The purpose of this utility model, which is that, overcomes above-mentioned deficiency, provides a kind of high-efficiency adsorbent preparation of nitrogen-methane Device.
In order to achieve the above objectives, the utility model is implemented according to following technical scheme:
A kind of high-efficiency adsorbent preparation facilities of nitrogen-methane, including autoclave body, agitating device, agitating device include stirring Motor, agitating shaft, stirrer paddle, the autoclave body side wall are provided with electric heating wire, and autoclave body outer wall is provided with thermal insulation layer, stirring motor It is arranged above autoclave body, the output shaft of stirring motor is connect with agitating shaft by shaft coupling, and autoclave body top is provided with feed opening, surveys Warm meter, manometer, vacuum orifice, autoclave body lower part are provided with discharge port, carbon dioxide mouth, and discharge port is connected with high-temperature valve, It is connected with cooling storehouse below high-temperature valve, cooling storehouse lower part is provided with cooling bin discharge port external.
Further, the stirring motor and autoclave body junction are provided with thermal insulation layer.
Further, the thermal insulation layer is ceramic thermal barrier layer.Nitrogen-methane adsorbent raw molecule sieve needs high temperature item It is activated under part, reaming, ceramic thermal barrier layer reduces energy consumption, has ensured the continuous production of stirring motor.
Further, the shaft coupling is diaphragm-type shaft coupling.Diaphragm-type shaft coupling can adapt to the working environment of high temperature.
The beneficial effects of the utility model are stringent to monitor volume production work for convenience of nitrogen-methane adsorbent industrial volume production Skill condition, agitating device increase the efficiency of adsorbent volume production.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the utility model.
Appended drawing reference: 1, autoclave body, 2, electric heating wire, 3, ceramic thermal barrier layer, 4, feed opening, 5, thermo detector, 6, diaphragm-type connection Axis device, 7, stirring motor, 8, manometer, 9, vacuum orifice, 10, stirring, 11, stirrer paddle, 12, carbon dioxide mouth, 13, Cooling storehouse, 14, cooling bin discharge port external, 15, high-temperature valve.
Specific embodiment
The utility model will be further described below with reference to the accompanying drawings and specific embodiments, in the signal of this utility model Property embodiment and explanation be used to explain the utility model, but be not intended to limit the scope of the present invention.
A kind of high-efficiency adsorbent preparation facilities of nitrogen-methane as shown in Figure 1, including autoclave body 1, agitating device, stirring Device includes stirring motor 7, agitating shaft 10, stirrer paddle 11, and 1 side wall of autoclave body is provided with electric heating wire 2,1 outer wall of autoclave body It is provided with ceramic thermal barrier layer 3, stirring motor 7 is arranged above autoclave body, and the output shaft and agitating shaft 10 of stirring motor 7 pass through diaphragm Type shaft coupling 6 connects, and 1 top of autoclave body is provided with feed opening 4, thermo detector 5, manometer 8, vacuum orifice 9, the setting of 1 lower part of autoclave body There are discharge port, carbon dioxide mouth 12, discharge port is connected with high-temperature valve 15, and cooling storehouse 13 is connected with below high-temperature valve 15, cold But 13 lower part of storehouse is provided with cooling bin discharge port external 14.The stirring motor 7 is provided with ceramic thermal barrier layer 3 with 1 junction of autoclave body.
When the utility model is used, active carbon molecular sieve is inserted from feed opening 4, turns off feed opening 4, from vacuum orifice It will be vacuumized in autoclave body at 9, manometer 8 measures the stopping of suitable vacuum degree;Electric heating wire 2 is then turned on to be heated, Thermo detector 5 monitors heating temperature, is heated to suitable temperature and is kept for a period of time activated;Then pass through carbon dioxide mouth 12, which are passed through carbon dioxide active carbon molecular sieve intracorporal to kettle, carries out reaming, and electric heating wire 2 continues to be heated to suitable reaming temperature Degree is kept for a period of time;Then high-temperature valve 15 is opened, the intracorporal active carbon molecular sieve of kettle, which enters in cooling storehouse 13, to be cooled down, High-temperature valve 15 turns off, and then the feed inlet 4 of autoclave body repeats above-mentioned technique, completes duration amount to the high adsorbent of nitrogen-methane It produces.
The limitation that the technical solution of the utility model is not limited to the above specific embodiments, all skills according to the present utility model The technology deformation that art scheme is made, each falls within the protection scope of the utility model.

Claims (4)

1. a kind of high-efficiency adsorbent preparation facilities of nitrogen-methane, including autoclave body, agitating device, agitating device includes stirring electricity Machine, agitating shaft, stirrer paddle, it is characterised in that: the autoclave body side wall is provided with electric heating wire, and autoclave body outer wall is provided with heat-insulated Layer, stirring motor are arranged above autoclave body, and the output shaft of stirring motor is connect with agitating shaft by shaft coupling, the setting of autoclave body top There are feed opening, thermo detector, manometer, vacuum orifice, autoclave body lower part is provided with discharge port, carbon dioxide mouth, and discharge port connects It is connected to high-temperature valve, is connected with cooling storehouse below high-temperature valve, cooling storehouse lower part is provided with cooling bin discharge port external.
2. a kind of high-efficiency adsorbent preparation facilities of nitrogen-methane according to claim 1, it is characterised in that: described to stir It mixes motor and autoclave body junction is provided with thermal insulation layer.
3. a kind of high-efficiency adsorbent preparation facilities of nitrogen-methane according to claim 2, it is characterised in that: it is described every Thermosphere is ceramic thermal barrier layer.
4. a kind of high-efficiency adsorbent preparation facilities of nitrogen-methane according to claim 1, it is characterised in that: described Axis device is diaphragm-type shaft coupling.
CN201821497729.4U 2018-09-13 2018-09-13 A kind of high-efficiency adsorbent preparation facilities of nitrogen-methane Expired - Fee Related CN209076672U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201821497729.4U CN209076672U (en) 2018-09-13 2018-09-13 A kind of high-efficiency adsorbent preparation facilities of nitrogen-methane

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201821497729.4U CN209076672U (en) 2018-09-13 2018-09-13 A kind of high-efficiency adsorbent preparation facilities of nitrogen-methane

Publications (1)

Publication Number Publication Date
CN209076672U true CN209076672U (en) 2019-07-09

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201821497729.4U Expired - Fee Related CN209076672U (en) 2018-09-13 2018-09-13 A kind of high-efficiency adsorbent preparation facilities of nitrogen-methane

Country Status (1)

Country Link
CN (1) CN209076672U (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110357775A (en) * 2019-08-23 2019-10-22 四川武胜春瑞医药化工有限公司 A kind of preparation method and preparation facilities of phthalic acid
CN114797682A (en) * 2022-04-27 2022-07-29 上海化工院检测有限公司 Rapid cooling safe melting kettle

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110357775A (en) * 2019-08-23 2019-10-22 四川武胜春瑞医药化工有限公司 A kind of preparation method and preparation facilities of phthalic acid
CN114797682A (en) * 2022-04-27 2022-07-29 上海化工院检测有限公司 Rapid cooling safe melting kettle
CN114797682B (en) * 2022-04-27 2024-01-23 上海化工院检测有限公司 Quick cooling safety melting kettle

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CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20190709

Termination date: 20210913