CN209076664U - Reaction kettle with condensing unit - Google Patents

Reaction kettle with condensing unit Download PDF

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Publication number
CN209076664U
CN209076664U CN201821711130.6U CN201821711130U CN209076664U CN 209076664 U CN209076664 U CN 209076664U CN 201821711130 U CN201821711130 U CN 201821711130U CN 209076664 U CN209076664 U CN 209076664U
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CN
China
Prior art keywords
reaction kettle
condensing unit
pipe
condensation chamber
condenser pipe
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201821711130.6U
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Chinese (zh)
Inventor
葛国华
吴卫红
涂军华
李蒋健
张成龙
孙小冬
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jiangxi Sanyuan Pharmaceutical Co Ltd
Original Assignee
Jiangxi Sanyuan Pharmaceutical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
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Priority to CN201821711130.6U priority Critical patent/CN209076664U/en
Application granted granted Critical
Publication of CN209076664U publication Critical patent/CN209076664U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

The utility model discloses a kind of reaction kettles with condensing unit, including reaction kettle ontology, reaction kettle bodies top is provided with return pipe, return pipe upper end is provided with condenser pipe, condenser pipe is set to inside condensation chamber, condensation chamber is provided with inlet tube and outlet tube, outlet tube protrudes into the reaction kettle body interior, the utility model structure is simple, it is easy to operate, liquid charging stock can be used, cooling condensation is carried out to condenser pipe, the liquid charging stock that reaction kettle is added is preheated in advance simultaneously, it both can be energy saving, it can accelerate reaction rate again, condensation effect is good, liquid is added more uniform, it avoids reaction excessively fierceness or hot-spot in reaction kettle and generates danger.

Description

Reaction kettle with condensing unit
Technical field
The utility model relates to field of chemical equipment, specially a kind of reaction kettle with condensing unit.
Background technique
During chemical reaction, some reactants or product are readily volatilized to come out due to low boiling point, pollute the environment or The progress for influencing reaction, needs to be sealed reaction kettle, but it is excessive to will lead to reaction kettle internal pressure after sealing, and generates safety Problem.So needing a kind of reaction kettle with condensation reflux unit, traditional condensing unit is spherical condensation tube, condensation effect Bad, and need to injecting condensed water in condenser pipe, energy consumption is excessive and waste water resource.
Liquid charging stock in prior art in reaction process is directly added by pipeline, it is easy to be caused mixing uneven or be put Local reaction temperature is excessively high and explosion danger occurs in thermal response.And lacks one kind in prior art to be able to carry out photocatalysis anti- The reaction kettle answered.
The utility model is to solve the problems, such as above-mentioned technical proposal, provides a kind of simple, reliable novel belt There is the reaction kettle of condensing unit, solves the problems, such as chemical production process.
Utility model content
The utility model provides a kind of reaction kettle with condensing unit, is asked with solve to occur in above-mentioned background technique Topic.
To achieve the above object, the utility model provides the following technical solutions: a kind of reaction kettle with condensing unit, packet Reaction kettle ontology and condensation chamber are included, the reaction kettle bodies top is provided with return pipe, and the return pipe upper end is provided with condensation Pipe, the condenser pipe are set to inside the condensation chamber, and inlet tube and outlet tube, the outlet tube are provided on the condensation chamber Connect with the reaction kettle ontology and the reaction kettle body interior protruded into connecting pin, can be used liquid charging stock to condenser pipe into Row cooling condensation, while the liquid charging stock that reaction kettle is added is preheated in advance, it not only can be energy saving, but also reaction speed can be accelerated Rate.
Further, the condenser pipe is the 1-30 ring pipes interconnected, and the condenser pipe top is connected with through cold The blow-down pipe of solidifying room, the blow-down pipe, which is located on one end outside the condensation chamber, is provided with valve, can generate preferably cold Solidifying effect.
Further, what the outlet tube lower end was located at the reaction kettle ontology is internally provided with liqiud outlet head, so that liquid adds Enter more uniform.
Further, the liqiud outlet head is the cylinder of upside down funnel shape or bottom end closure, has fluid hole on the liqiud outlet head, So that liquid addition is more uniform.
Further, it is provided with insulating layer outside the condensation chamber, so that condensation effect is more preferable.
Further, it is provided with feeding port on the reaction kettle ontology, convenient for feeding intake.
Further, there is sealing cover on the feeding port, convenient for being sealed to reaction kettle.
Further, the condenser pipe is made of glass or steel, and anti-locking apparatus is corroded.
Further, there is erosion shield on the condensation chamber interior walls and the condenser pipe, anti-locking apparatus is corroded.
Further, the reaction kettle body interior is provided with visible light source, is convenient for light-catalyzed reaction.
Compared with prior art, the utility model has the beneficial effects that (1) structure is simple, it is easy to operate;(2) can make Cooling condensation is carried out to condenser pipe with liquid charging stock, while the liquid charging stock that reaction kettle is added is preheated in advance, can both be saved The energy, and reaction rate can be accelerated;(3) setting of the ring pipe interconnected is so that condensation effect is more preferable;(4) liqiud outlet head Setting so that liquid be added it is more uniform, avoid local reaction excessively acutely and cause danger;(5) setting of visible light source makes Light-catalyzed reaction can be carried out by obtaining reaction kettle.
Detailed description of the invention
Fig. 1 is the utility model topology view;
Fig. 2 is the utility model embodiment schematic views;
In figure: 1- reaction kettle ontology, 2- return pipe, 3- condenser pipe, 4- condensation chamber, 5- inlet tube, 6- outlet tube, 7- go out liquid Head, 8- fluid hole, 9- feeding port, 31- blow-down pipe, 32- valve.
Specific embodiment
In order to illustrate more clearly of the technical solution of the utility model, implement below in conjunction with the part of the utility model Example, is clearly and completely described the technical solution of the utility model.
Embodiment 1
The present embodiment combination Fig. 1, a kind of reaction kettle with condensing unit, including reaction kettle ontology 1, reaction kettle ontology 1 Reaction kettle is commonly used for industry, is provided with feeding port 9 on reaction kettle ontology 1, there is sealing cover, 1 top of reaction kettle ontology on feeding port 9 It is welded with steel return pipe 2, reaction kettle ontology 1 is connected to return pipe 2, and the welding of 2 upper end of return pipe is provided with steel condenser pipe 3, Condenser pipe 3 is 5 steel annular pipes interconnected, and 3 top of condenser pipe is welded with blow-down pipe 31, condenser pipe 3 and blow-down pipe 31 It is connected to, is provided with valve 32 on blow-down pipe 31, condenser pipe 3 is set to inside condensation chamber 4, and condensation chamber 4 is one outside condenser pipe 3 A cavity that can inject liquid, there is anticorrosive PTFE erosion resisting coating on 4 inner wall of condensation chamber and condenser pipe 3, outside condensation chamber 4 It is provided with insulating layer, condensation chamber 4, which is provided with, is welded with steel inlet tube 5 and steel outlet tube 6, and 6 other end of outlet tube protrudes into instead The inside of kettle ontology 1 is answered, one end that 6 lower end of outlet tube is located inside reaction kettle ontology 1 is welded with liqiud outlet head 7, and liqiud outlet head 7 is to fall Infundibulate is set, there is fluid hole 8 on liqiud outlet head 7, showerhead shape is presented.
Reaction kettle start to work when, liquid reaction raw material by inlet tube 5 enter condensation chamber 4, full of after condensation chamber 4 by going out liquid Pipe 6 enters in reaction kettle ontology 1, is uniformly spilled into reaction kettle by the fluid hole 8 on liqiud outlet head 7, the low boiling point liquid in reaction kettle Body enters condenser pipe 3 by return pipe 2, passes back into reaction kettle after condensation.
The present embodiment structure is simple, easy to operate, and liquid charging stock can be used and carry out cooling condensation to condenser pipe, while is right The liquid charging stock that reaction kettle is added preheats in advance, not only can be energy saving, but also can accelerate reaction rate, and condensation effect is good, liquid Body is added more uniform avoid and reacts excessively fierce or hot-spot in reaction kettle and generate danger.
Embodiment 2
The present embodiment combination Fig. 2, a kind of reaction kettle with condensing unit, including reaction kettle ontology 1, reaction kettle ontology 1 Reaction kettle is commonly used for industry, is provided with feeding port 9 on reaction kettle ontology 1, there is sealing cover, 1 top of reaction kettle ontology on feeding port 9 It is welded with steel return pipe 2, reaction kettle ontology 1 is connected to return pipe 2, and the welding of 2 upper end of return pipe is provided with steel condenser pipe 3, Condenser pipe 3 is 5 steel annular pipes interconnected, and 3 top of condenser pipe is welded with blow-down pipe 31, condenser pipe 3 and blow-down pipe 31 It is connected to, is provided with valve 32 on blow-down pipe 31, condenser pipe 3 is set to inside condensation chamber 4, and condensation chamber 4 is one outside condenser pipe 3 A cavity that can inject liquid, there is anticorrosive PTFE erosion resisting coating on 4 inner wall of condensation chamber and condenser pipe 3, outside condensation chamber 4 It is provided with insulating layer, condensation chamber 4, which is provided with, is welded with steel inlet tube 5 and steel outlet tube 6, and 6 other end of outlet tube protrudes into instead The inside of kettle ontology 1 is answered, one end that 6 lower end of outlet tube is located inside reaction kettle ontology 1 is welded with liqiud outlet head 7, and liqiud outlet head 7 is bottom Closed cylinder is held, there is fluid hole 8 on liqiud outlet head 7, it can be to beneath and surrounding hydrojet.
Reaction kettle start to work when, liquid reaction raw material by inlet tube 5 enter condensation chamber 4, full of after condensation chamber 4 by going out liquid Pipe 6 enters in reaction kettle ontology 1, is uniformly spilled into reaction kettle by the fluid hole 8 on liqiud outlet head 7, the low boiling point liquid in reaction kettle Body enters condenser pipe 3 by return pipe 2, passes back into reaction kettle after condensation.
The present embodiment structure is simple, easy to operate, and liquid charging stock can be used and carry out cooling condensation to condenser pipe, while is right The liquid charging stock that reaction kettle is added preheats in advance, not only can be energy saving, but also can accelerate reaction rate, and condensation effect is good, liquid Body is added more uniform avoid and reacts excessively fierce or hot-spot in reaction kettle and generate danger, while the circle of bottom end closure It is more uniform that liquid is added in cylindricality liqiud outlet head 7.
Embodiment 3
The present embodiment combination Fig. 1, a kind of reaction kettle with condensing unit, including reaction kettle ontology 1, reaction kettle ontology 1 For the common reaction kettle of industry, reaction kettle ontology 1 is internally provided with radiation of visible light lamp, is provided with feeding port on reaction kettle ontology 1 9, there is sealing cover on feeding port 9,1 top of reaction kettle ontology is connected with glass system return pipe 2, reaction kettle ontology 1 with rubber seal It is connected to return pipe 2,2 upper end of return pipe has glass system to be integrally formed condenser pipe 3, and condenser pipe 3 is 5 glass rings interconnected There is blow-down pipe 31 on shape pipe, 3 top of condenser pipe, and condenser pipe 3 is connected to blow-down pipe 31, and valve 32 is provided on blow-down pipe 31, condensation Pipe 3 is set to inside condensation chamber 4, and condensation chamber 4 is the cavity that one outside condenser pipe 3 can inject liquid, and condensation chamber 4 is double Layer glass system, intermediate evacuated state reach heat insulation effect, and condensation chamber 4 has inlet tube 5 and steel outlet tube 6, and outlet tube 6 is logical It crosses and covers effective rubber seal and be connected to condensation chamber 4,6 other end of outlet tube protrudes into the inside of reaction kettle ontology 1,6 lower end of outlet tube One end inside reaction kettle ontology 1 is welded with liqiud outlet head 7, and liqiud outlet head 7 is upside down funnel shape, has fluid hole on liqiud outlet head 7 8, showerhead shape is presented.
Reaction kettle start to work when, liquid reaction raw material by inlet tube 5 enter condensation chamber 4, full of after condensation chamber 4 by going out liquid Pipe 6 enters in reaction kettle ontology 1, is uniformly spilled into reaction kettle by the fluid hole 8 on liqiud outlet head 7, the low boiling point liquid in reaction kettle Body enters condenser pipe 3 by return pipe 2, passes back into reaction kettle after condensation.
The present embodiment structure is simple, easy to operate, and liquid charging stock can be used and carry out cooling condensation to condenser pipe, while is right The liquid charging stock that reaction kettle is added preheats in advance, not only can be energy saving, but also can accelerate reaction rate, and condensation effect is good, liquid Body is added more uniform avoid and reacts excessively fierce or hot-spot in reaction kettle and generate danger, on the basis of embodiment 1 On changed steel condenser system into glass system, greatly avoid corrosion of equipment, condensation situations can also be observed, be more conducive to Reaction carries out, and also increases light emitting source in reaction kettle inner top, the fluorescent lamp that light emitting source is one 1000 watts can carry out photocatalysis Reaction.
The utility model is not limited to above-mentioned specific embodiment, and those skilled in the art can also make a variety of changes accordingly Change, but any variation equivalent or similar with the utility model should all be covered in the range of the utility model claims.

Claims (10)

1. a kind of reaction kettle with condensing unit, including reaction kettle ontology (1) and condensation chamber (4), it is characterised in that: described anti- It answers and is provided with return pipe (2) at the top of kettle ontology (1), return pipe (2) upper end is provided with condenser pipe (3), the condenser pipe (3) It is internal to be set to the condensation chamber (4), is provided with inlet tube (5) and outlet tube (6), the outlet tube on the condensation chamber (4) (6) it is connect with the reaction kettle ontology (1) and reaction kettle ontology (1) inside is protruded into connecting pin.
2. the reaction kettle according to claim 1 with condensing unit, it is characterised in that: the condenser pipe (3) is 1-30 A ring pipe interconnected, condenser pipe (3) top are connected with the blow-down pipe (31) through condensation chamber (4), the emptying Pipe (31), which is located on the external one end of the condensation chamber (4), is provided with valve (32).
3. the reaction kettle according to claim 1 with condensing unit, it is characterised in that: outlet tube (6) the lower end position Liqiud outlet head (7) are internally provided in the reaction kettle ontology (1).
4. the reaction kettle according to claim 3 with condensing unit, it is characterised in that: the liqiud outlet head (7) is to be inverted The cylinder of infundibulate or bottom end closure has fluid hole (8) on the liqiud outlet head (7).
5. the reaction kettle according to claim 1 with condensing unit, it is characterised in that: set outside the condensation chamber (4) It is equipped with insulating layer.
6. the reaction kettle according to claim 1 with condensing unit, it is characterised in that: on the reaction kettle ontology (1) It is provided with feeding port (9).
7. the reaction kettle according to claim 6 with condensing unit, it is characterised in that: have on the feeding port (9) close Capping.
8. the reaction kettle according to claim 1 with condensing unit, it is characterised in that: the condenser pipe (3) is glass Or steel is made.
9. the reaction kettle according to claim 8 with condensing unit, it is characterised in that: condensation chamber (4) inner wall and There is erosion shield on the condenser pipe (3).
10. the reaction kettle according to claim 1 with condensing unit, it is characterised in that: in the reaction kettle ontology (1) Portion is provided with visible light source.
CN201821711130.6U 2018-10-22 2018-10-22 Reaction kettle with condensing unit Expired - Fee Related CN209076664U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201821711130.6U CN209076664U (en) 2018-10-22 2018-10-22 Reaction kettle with condensing unit

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201821711130.6U CN209076664U (en) 2018-10-22 2018-10-22 Reaction kettle with condensing unit

Publications (1)

Publication Number Publication Date
CN209076664U true CN209076664U (en) 2019-07-09

Family

ID=67120173

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201821711130.6U Expired - Fee Related CN209076664U (en) 2018-10-22 2018-10-22 Reaction kettle with condensing unit

Country Status (1)

Country Link
CN (1) CN209076664U (en)

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CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20190709

Termination date: 20211022