CN209069343U - A kind of enamel reaction still pH online detection instrument - Google Patents

A kind of enamel reaction still pH online detection instrument Download PDF

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Publication number
CN209069343U
CN209069343U CN201822139300.4U CN201822139300U CN209069343U CN 209069343 U CN209069343 U CN 209069343U CN 201822139300 U CN201822139300 U CN 201822139300U CN 209069343 U CN209069343 U CN 209069343U
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CN
China
Prior art keywords
reaction still
enamel reaction
detection instrument
online detection
bypass conduit
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201822139300.4U
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Chinese (zh)
Inventor
敬东海
于永宏
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shanghai Pharma New Asia Pharmaceutical Co Ltd
LIAONING MEDYA PHARMACEUTICAL CO Ltd
Original Assignee
Shanghai Pharma New Asia Pharmaceutical Co Ltd
LIAONING MEDYA PHARMACEUTICAL CO Ltd
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Publication date
Application filed by Shanghai Pharma New Asia Pharmaceutical Co Ltd, LIAONING MEDYA PHARMACEUTICAL CO Ltd filed Critical Shanghai Pharma New Asia Pharmaceutical Co Ltd
Priority to CN201822139300.4U priority Critical patent/CN209069343U/en
Application granted granted Critical
Publication of CN209069343U publication Critical patent/CN209069343U/en
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Abstract

The utility model provides a kind of enamel reaction still pH online detection instrument, it is characterised in that: including enamel reaction still and pH online detection instrument;Wherein, the enamel reaction still is equipped with the bypass conduit being connected to enamel reaction still;The bypass conduit is equipped at least one equipment mounting base;The pH probe of the pH online detection instrument is installed in equipment mounting base.The enamel reaction still is able to achieve real-time detection, highly-safe.

Description

A kind of enamel reaction still pH online detection instrument
Technical field
The utility model relates to chemical reaction equipment field, in particular to a kind of enamel reaction still pH online detection instrument.
Background technique
Existing enamel reaction still cannot install pH meter probe in autoclave body equipment upper opening, if every time because of material reason During reaction, it need to extract reaction solution and be detected outside kettle, testing result can be lagged than actual result, can not achieve real-time detection Effect, influence the problem of the whole control and repeatability of reaction.
And industrialized online pH meter monitoring probe, it is unfavorable for the installation and convenient to use, later period maintenance of enamel still Cumbersome, expense is higher.
And if portable pH meter probe is protruded into detection from reaction kettle hole, it is unfavorable for safety operation, and kettle internal stimulus Smell overflows, and security risk is larger.
Utility model content
The utility model is intended to overcome drawbacks described above, provides one kind and is able to achieve real-time detection, highly-safe enamel reaction Kettle.
The utility model provides a kind of enamel reaction still pH online detection instrument, it is characterised in that: reacts including enamel Kettle and pH online detection instrument;
Wherein, above-mentioned enamel reaction still is equipped with the bypass conduit being connected to enamel reaction still;
Above-mentioned bypass conduit is equipped at least one equipment mounting base;
The pH probe of above-mentioned pH online detection instrument is installed in equipment mounting base.
The bypass conduit is realized in real time to flow into the reaction solution reacted and be somebody's turn to do by way of being connected to enamel reaction still The effect of bypass conduit.And then after various detection devices are installed in the bypass conduit, it can be realized and reaction solution is currently referred to Target real-time monitoring.
Further, a kind of enamel reaction still pH online detection instrument provided by the utility model also has such knot Structure feature: i.e., above equipment mounting base include mounting seat body, elastic mechanism and closing means;
Above-mentioned mounting seat body is fixedly connected with bypass conduit;
Above-mentioned elastic mechanism is set in mounting seat body;The elastic mechanism can be fabricated for colloidal materials, generally With elasticity.
Above-mentioned closing means are installed on the top of elastic mechanism, to closing at the top of mounting seat body.The closing machine Structure is generally bonded with elastic mechanism one side, to realize the effect for being compacted elastic mechanism.
Further, a kind of enamel reaction still pH online detection instrument provided by the utility model also has such knot Structure feature: i.e., be spirally connected connection between above-mentioned mounting seat body and closing means.I.e., in the mounting seat body have internal screw thread or External screw thread has external screw thread or internal screw thread on closing means, to realize closing by way of twisting.
Further, a kind of enamel reaction still pH online detection instrument provided by the utility model also has such knot Structure feature: it i.e., between above-mentioned mounting seat body and closing means is fastened and connected.Such as: the mode of l ock l ock fastening lid.
Further, a kind of enamel reaction still pH online detection instrument provided by the utility model also has such knot Structure feature: i.e., above-mentioned elastic mechanism and closing means, on corresponding position, it is equipped with through-hole.So as to allow pH meter, temperature The probes such as meter pass through.
Further, a kind of enamel reaction still pH online detection instrument provided by the utility model also has such knot Structure feature: i.e., above-mentioned enamel reaction still be equipped with liquid inlet and liquid outlet;
Above-mentioned bypass conduit connection liquid inlet and liquid outlet.
Further, a kind of enamel reaction still pH online detection instrument provided by the utility model also has such knot Structure feature: i.e., above-mentioned bypass conduit be equipped with liquid circulation power device.Generally liquid pump.
Further, a kind of enamel reaction still pH online detection instrument provided by the utility model also has such knot Structure feature: i.e., above-mentioned bypass conduit be equipped with several flow-stop valves.
Further, a kind of enamel reaction still pH online detection instrument provided by the utility model also has such knot Structure feature: i.e., above-mentioned bypass conduit be equipped with shunt tubercle;
The branch pipe being connected to bypass conduit is equipped at above-mentioned shunting tubercle;
Fluid stopping mechanism is equipped on each pipeline being connected to above-mentioned shunting tubercle.
Further, a kind of enamel reaction still pH online detection instrument provided by the utility model also has such knot Structure feature: i.e., further include thermal detector;
The temperature probe of above-mentioned thermal detector is installed in equipment mounting base.
The action and effect of the utility model:
The utility model by drawn on enamel reaction still one can with reaction kettle is intrinsic reacts liquid recycle stream Logical bypass conduit, to realize the reaction solution that will be being reacted by way of being connected to the shunt valve with enamel reaction still Real-time streams are passed through the effect of the bypass conduit.And then after various detection devices are installed in the bypass conduit, it can be realized pair The real-time monitoring of reaction solution current criteria.
Detailed description of the invention
The structural schematic diagram for the enamel reaction still pH online detection instrument that attached drawing 1, embodiment are related to.
Specific embodiment
As shown in Figure 1, present embodiments provide a kind of enamel reaction still pH online detection instrument, by enamel reaction still 100, PH online detection instrument (including pH detection probe 210 and pH meter 220) and thermometer 300 form;
Wherein, which is commercially available reaction kettle using tradition, adopts feed inlet 101 and the discharging of the reaction kettle Mouth 102, or increase feed inlet 101 and discharge port 102 newly on the reaction kettle again;
Fluid circuit 110 is installed between the feed inlet 101 and discharge port 102;
The fluid circuit 110 is equipped with the fluid pump 120 as circulation power;
In the case that the fluid circuit 110 is in access, after starting the fluid pump 120, can be realized will be in reaction kettle Partially liq enter and leave fluid circuit 110 effect, the fluid pump by setting direction circulation liquid open in the present embodiment After dynamic fluid pump, it can be realized and liquid is subjected to the effect that direction as shown by arrows circulates.So as to make to react The current reaction solution of kettle constantly flows through the fluid circuit.
In the present embodiment, there are two equipment mounting seat bodies 120 for installation on the fluid circuit 110;
The equipment mounting seat body 120 welding be arranged close to autoclave body aperture position, be tetrafluoro silk braid pipe material and Structure, the rubber plug 121 of opening is filled in the casing, and the aperture of the rubber plug opening portion is just suitble to pH detection probe 210 or temperature The insertion of meter 300;
After rubber plug is installed, tetrafluoro nut 122 is screwed into the silk braid pipe of mounting seat body 120, rubber plug is pushed down, And close the opening of mounting seat body 120.
On the tetrafluoro nut 122, corresponding to the position of rubber plug opening portion, there is through-hole;
During use, pH detection probe 210 or thermometer 300 are passed sequentially through to the through-hole and rubber plug on the nut On open hole after arrive at the position that flows through of reaction solution, and installation can be realized in tightening nuts.
Every time when cleaning, correction PH meter probe or thermometer, as long as tetrafluoro nut is screwed out, extraction PH meter probe or temperature Meter cleaning correction, facilitates accurately use next time.
On the one hand the setting of this mounting base can effectively prevent reaction solution in cyclic process, overflow by probe hole Out, on the other hand also it is able to achieve the convenient replacement of equipment.Successfully realize the effect of first real-time detection.

Claims (10)

1. a kind of enamel reaction still pH online detection instrument, it is characterised in that: including enamel reaction still and pH online detection instrument;
Wherein, the enamel reaction still is equipped with the bypass conduit being connected to enamel reaction still;
The bypass conduit is equipped at least one equipment mounting base;
The pH probe of the pH online detection instrument is installed in equipment mounting base.
2. a kind of enamel reaction still pH online detection instrument as described in claim 1, it is characterised in that:
The equipment mounting base includes mounting seat body, elastic mechanism and closing means;
The mounting seat body is fixedly connected with bypass conduit;
The elastic mechanism is set in mounting seat body;
The closing means are installed on the top of elastic mechanism, to closing at the top of mounting seat body.
3. a kind of enamel reaction still pH online detection instrument as claimed in claim 2, it is characterised in that:
Be spirally connected connection between the mounting seat body and closing means.
4. a kind of enamel reaction still pH online detection instrument as claimed in claim 2, it is characterised in that:
It is fastened and connected between the mounting seat body and closing means.
5. a kind of enamel reaction still pH online detection instrument as claimed in claim 2, it is characterised in that:
The elastic mechanism and closing means on corresponding position, are equipped with through-hole.
6. a kind of enamel reaction still pH online detection instrument as described in claim 1, it is characterised in that:
The enamel reaction still is equipped with liquid inlet and liquid outlet;
The bypass conduit connection liquid inlet and liquid outlet.
7. a kind of enamel reaction still pH online detection instrument as described in claim 1, it is characterised in that:
The bypass conduit is equipped with liquid circulation power device.
8. a kind of enamel reaction still pH online detection instrument as described in claim 1, it is characterised in that:
The bypass conduit is equipped with several flow-stop valves.
9. a kind of enamel reaction still pH online detection instrument as described in claim 1, it is characterised in that:
The bypass conduit, which is equipped with, shunts tubercle;
It is described to shunt the branch pipe for being equipped at tubercle and being connected to bypass conduit;
Fluid stopping mechanism is equipped on each pipeline being connected to the shunting tubercle.
10. a kind of enamel reaction still pH online detection instrument as described in claim 1-9 is any, it is characterised in that: further include Thermal detector;
The temperature probe of the thermal detector is installed in equipment mounting base.
CN201822139300.4U 2018-12-19 2018-12-19 A kind of enamel reaction still pH online detection instrument Active CN209069343U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201822139300.4U CN209069343U (en) 2018-12-19 2018-12-19 A kind of enamel reaction still pH online detection instrument

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201822139300.4U CN209069343U (en) 2018-12-19 2018-12-19 A kind of enamel reaction still pH online detection instrument

Publications (1)

Publication Number Publication Date
CN209069343U true CN209069343U (en) 2019-07-05

Family

ID=67101755

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201822139300.4U Active CN209069343U (en) 2018-12-19 2018-12-19 A kind of enamel reaction still pH online detection instrument

Country Status (1)

Country Link
CN (1) CN209069343U (en)

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