CN209060573U - A kind of dichloroethanes distillation still on cyhalofop-butyl production line - Google Patents

A kind of dichloroethanes distillation still on cyhalofop-butyl production line Download PDF

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Publication number
CN209060573U
CN209060573U CN201821698970.3U CN201821698970U CN209060573U CN 209060573 U CN209060573 U CN 209060573U CN 201821698970 U CN201821698970 U CN 201821698970U CN 209060573 U CN209060573 U CN 209060573U
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China
Prior art keywords
autoclave body
dichloroethanes
cyhalofop
agitating shaft
production line
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CN201821698970.3U
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Chinese (zh)
Inventor
周娟
周灿亮
孟宪秋
游良奇
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Hubei Zhong Xun Changqing Technology Co Ltd
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Hubei Zhong Xun Changqing Technology Co Ltd
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Abstract

A kind of dichloroethanes distillation still on cyhalofop-butyl production line, it includes autoclave body (1), agitating shaft, sealed water jacket (2), a pair of hollow agitating paddle (3) and heating jacket (5), feed inlet and exhaust outlet are respectively equipped at the top of autoclave body (1), autoclave body (1) bottom is equipped with discharge gate, agitating shaft is made of solid-section (6) and hollow section (7), the outer wall of sealed water jacket (2) is equipped with water inlet pipe (11), sealed water jacket (2) covers on agitating shaft, and it is fixedly mounted at the top of autoclave body (1) by support base, the outer wall upper, annular of hollow section (7) is uniformly provided with one group of A water inlet (10), one group of A water inlet (10) is connected with the inner cavity of sealed water jacket (2) respectively;Advantage is: being capable of Rapid Cleaning after the completion of distillation still use.

Description

A kind of dichloroethanes distillation still on cyhalofop-butyl production line
Technical field
The utility model relates to distillation equipment fields, and in particular to the dichloroethanes distillation on a kind of cyhalofop-butyl production line Kettle.
Background technique
Currently, existing dichloroethanes distillation still can remain many impurity after distillation in distillation still, it is difficult to it cleans, Influence the production efficiency of factory.
Utility model content
The purpose of this utility model provides two chloroethenes on a kind of cyhalofop-butyl production line aiming at above-mentioned deficiency Alkane distillation still.
It includes autoclave body, agitating shaft, sealed water jacket, a pair of hollow agitating paddle and heating jacket to the utility model,
Feed inlet and exhaust outlet are respectively equipped at the top of autoclave body, autoclave body bottom is equipped with discharge gate,
Agitating shaft is made of solid-section and hollow section, and the outer wall of sealed water jacket is equipped with water inlet pipe, and sealed water jacket, which covers, to be stirred It mixes on axis, and is fixedly mounted at the top of autoclave body by support base, the outer wall upper, annular of hollow section is uniformly provided with one group of A water inlet Mouthful, one group of A water inlet is connected with the inner cavity of sealed water jacket respectively,
Agitating shaft is movably arranged in autoclave body by bearing, and drives agitating shaft rotation by motor and speed reducer,
The outer wall of hollow agitating paddle is equipped with multiple groups cleaning brush, is provided with water jet, Yi Duikong between every two cleaning brush Heart agitating paddle is fixedly mounted on agitating shaft in mirror image distribution, and the water inlet of a pair of hollow agitating paddle is connected with hollow section respectively It is logical,
Heating jacket covers on autoclave body outer wall.
Heating jacket is steam heating jacket or oily heating jacket.
Cleaning brush is wire brush.
Shut-off valve is equipped on the discharge gate of water inlet pipe and autoclave body.
Autoclave body includes top cover and tank body, and connecting flange is respectively equipped on top cover and tank body, and top cover covers on tank body, and passes through Metallic gasket and bolt fixed seal connection.
Sealed water jacket is connect with solid-section and hollow section rotatory sealing respectively by sealing ring.
The utility model advantage is: being capable of Rapid Cleaning after the completion of distillation still use.
Detailed description of the invention
Fig. 1 is the utility model structure diagram.
Fig. 2 is the utility model overlooking structure diagram.
Fig. 3 is the A-A schematic cross-sectional view of the utility model Fig. 2.
Fig. 4 is the partial enlargement structural representation of the utility model Fig. 3.
Specific embodiment
As shown in the picture, the utility model it include autoclave body 1, agitating shaft, sealed water jacket 2, a pair of hollow agitating paddle 3 and add Thermal jacket 5,
Feed inlet and exhaust outlet are respectively equipped at the top of autoclave body 1,1 bottom of autoclave body is equipped with discharge gate,
Agitating shaft is made of solid-section 6 and hollow section 7, and the outer wall of sealed water jacket 2 is equipped with water inlet pipe 11, sealed water jacket 2 It covers on agitating shaft, and 1 top of autoclave body is fixedly mounted on by support base, the outer wall upper, annular of hollow section 7 is uniformly provided with one Group A water inlet 10, one group of A water inlet 10 are connected with the inner cavity of sealed water jacket 2 respectively,
Agitating shaft is movably arranged in autoclave body 1 by bearing, and drives agitating shaft rotation by motor and speed reducer,
The outer wall of hollow agitating paddle 3 is equipped with multiple groups cleaning brush 8, is provided with water jet 9 between every two cleaning brush 8, and one Hollow agitating paddle 3 is fixedly mounted on agitating shaft in mirror image distribution, and the water inlet of a pair of hollow agitating paddle 3 respectively with it is hollow Section 7 is connected,
5 sets of heating jacket on 1 outer wall of autoclave body.
Heating jacket 5 is steam heating jacket or oily heating jacket.
Cleaning brush 8 is wire brush.
Shut-off valve is equipped on the discharge gate of water inlet pipe 11 and autoclave body 1.
Autoclave body 1 includes top cover and tank body, is respectively equipped with connecting flange on top cover and tank body, top cover covers on tank body, and leads to Cross metallic gasket and bolt fixed seal connection.
Sealed water jacket 2 is connect with solid-section 6 and 7 rotatory sealing of hollow section respectively by sealing ring.
Working method: successively the liquid containing dichloroethanes, process water, hydrochloric acid and n-butanol being added in autoclave body 1, starting Motor drives agitating shaft rotation, while heating jacket 5 carries out heating distillation to the material in autoclave body 1, and dichloroethanes gas is logical The discharge of 1 exhaust outlet of autoclave body is crossed, remaining product is discharged by the discharge gate of autoclave body 1, when needing to clean autoclave body 1, passes through water inlet Pipe 11 is filled with process water into sealed water jacket 2, and process water is ejected into autoclave body 1 by water jet 9, and starting motor drives stirring Axis rotates, and the wire brush on a pair of hollow agitating paddle 3 constantly scrubs the inner wall of autoclave body 1, and 1 bottom of autoclave body is opened after scrubbing Waste material is discharged in discharge gate.

Claims (6)

1. the dichloroethanes distillation still on a kind of cyhalofop-butyl production line, it is characterised in that it includes autoclave body (1), agitating shaft, close Water shutoff set (2), a pair of hollow agitating paddle (3) and heating jacket (5),
Feed inlet and exhaust outlet are respectively equipped at the top of autoclave body (1), autoclave body (1) bottom is equipped with discharge gate,
Agitating shaft is made of solid-section (6) and hollow section (7), and the outer wall of sealed water jacket (2) is equipped with water inlet pipe (11), sealing water Set (2) covers on agitating shaft, and is fixedly mounted at the top of autoclave body (1) by support base, and the outer wall upper, annular of hollow section (7) is equal Cloth is provided with one group of A water inlet (10), and one group of A water inlet (10) is connected with the inner cavity of sealed water jacket (2) respectively,
Agitating shaft is movably arranged in autoclave body (1) by bearing, and drives agitating shaft rotation by motor and speed reducer,
The outer wall of hollow agitating paddle (3) is equipped with multiple groups cleaning brush (8), and every two cleaning brush is provided with water jet between (8) (9), a pair of hollow agitating paddle (3) is fixedly mounted on agitating shaft in mirror image distribution, and the water inlet of a pair of hollow agitating paddle (3) It is connected respectively with hollow section (7),
Heating jacket (5) covers on autoclave body (1) outer wall.
2. the dichloroethanes distillation still on a kind of cyhalofop-butyl production line according to claim 1, it is characterised in that heating Collet (5) is steam heating jacket or oily heating jacket.
3. the dichloroethanes distillation still on a kind of cyhalofop-butyl production line according to claim 1, it is characterised in that cleaning Brushing (8) is wire brush.
4. the dichloroethanes distillation still on a kind of cyhalofop-butyl production line according to claim 1, it is characterised in that water inlet Shut-off valve is equipped on the discharge gate of pipe (11) and autoclave body (1).
5. the dichloroethanes distillation still on a kind of cyhalofop-butyl production line according to claim 1, it is characterised in that autoclave body (1) include top cover and tank body, connecting flange is respectively equipped on top cover and tank body, top cover covers on tank body, and passes through metal sealing Pad and bolt fixed seal connection.
6. the dichloroethanes distillation still on a kind of cyhalofop-butyl production line according to claim 1, it is characterised in that sealing Water jacket (2) is connect with solid-section (6) and hollow section (7) rotatory sealing respectively by sealing ring.
CN201821698970.3U 2018-10-19 2018-10-19 A kind of dichloroethanes distillation still on cyhalofop-butyl production line Active CN209060573U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201821698970.3U CN209060573U (en) 2018-10-19 2018-10-19 A kind of dichloroethanes distillation still on cyhalofop-butyl production line

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201821698970.3U CN209060573U (en) 2018-10-19 2018-10-19 A kind of dichloroethanes distillation still on cyhalofop-butyl production line

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CN209060573U true CN209060573U (en) 2019-07-05

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111135596A (en) * 2019-10-31 2020-05-12 荆门金贤达生物科技有限公司 Beneficiated burden material preparation production line on etoxazole production line

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111135596A (en) * 2019-10-31 2020-05-12 荆门金贤达生物科技有限公司 Beneficiated burden material preparation production line on etoxazole production line
CN111135596B (en) * 2019-10-31 2024-05-17 荆门金贤达生物科技有限公司 Concentrate preparation production line on etoxazole production line

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