CN209039527U - Rapid quenching minitype high voltage kettle - Google Patents
Rapid quenching minitype high voltage kettle Download PDFInfo
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- CN209039527U CN209039527U CN201821903876.7U CN201821903876U CN209039527U CN 209039527 U CN209039527 U CN 209039527U CN 201821903876 U CN201821903876 U CN 201821903876U CN 209039527 U CN209039527 U CN 209039527U
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- China
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- autoclave
- cold end
- seal head
- cold
- cone seal
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Abstract
The utility model relates to quench autoclave technology field, specially rapid quenching minitype high voltage kettle, the reaction kettle is connected by the connector of Be-Cu alloy bipyramid with cold end autoclave, junction is fixed by attaching nut, attaching nut is upper, and there are two water nozzles, water nozzle is connect with water cooling system, for connector water cooling；The other end of cold end autoclave is sealed using cone seal head, and cone seal head is fixed on cold end autoclave end by clamping nut；Cone seal head center is equipped with capillary, and capillary is connected to cold end autoclave and pressure system；Sample holder lower end is magnetic bottom end, and magnetic bottom end is located in cold end autoclave；Magnetic bottom end upper end is connected with the thin stick of non-magnetic stainless steel, and the thin stick of non-magnetic stainless steel penetrates into reaction kettle cylinder type sample bin；It is placed with magnet outside cold end autoclave, controls the position of sample holder.Rapid quenching minitype high voltage kettle provided by the utility model, quenching mode is rapidly and efficiently safe, autoclave body long service life.
Description
Technical field
The utility model relates to quench autoclave technology field, specially rapid quenching minitype high voltage kettle.
Background technique
It is existing can rapid quenching minitype high voltage kettle, by reaction kettle and quenching kettle two parts form, with 40Cr type stainless steel
Nut connection.Compared with Tuttle type autoclave, which increases quenching kettle.Reaction kettle is by nickel-base material (GH141, GH169
Type) it is made and (is equivalent to Rene41, Inconel718), the long 30cm of autoclave body, inner and outer diameter is respectively Ф 0.8cm and Ф 3cm, is quenched
The material of fiery kettle is 1Cr18Ni9Ti type stainless steel, and the design of entire material can guarantee that autoclave can be for a long time 700~800
DEG C, continuous work under conditions of 100~150MPa.Cooler is installed, when experiment carries out, cooling water is continuous on quenching kettle outer wall
Be circulated in cooler, make to quench kettle and be maintained at nearly room temperature state, while can be used to quench.The sealing of autoclave uses spherical surface
Pad, is connected by seal head and capillary with pressure system.In use process, for autoclave in being horizontally arranged, reaction kettle is located at pipe
In formula electric furnace, when quenching, autoclave body is extracted out, and autoclave is rotated by 90 ° from electric furnace, change it by horizontal position perpendicular
Position, the sample cell in reaction kettle can be fallen in quenching kettle due to gravity, and quenching is realized within several seconds.
Above-mentioned autoclave in use, appoint there are this some problems:
First: safety.When operator extracts reaction kettle body out from high-temperature electric resistance furnace, rotate and the process that is fixed
In, it is careless slightly, easily scald, meanwhile, in order to guarantee that sample cell can smoothly be fallen into quenching kettle from reaction kettle, usually to tap
Reaction kettle, to autoclave, there is certain damages, and under 1000 to 2000 atmospheric pressures, there is great safety is hidden
Suffer from；
Second: quenching efficiency.During reaction kettle is from be horizontally arranged to being disposed vertically, sample cell is easy to be stuck in reaction kettle
In, it can not achieve quenching.
Third: material loss.Firstly, reaction kettle is faced with the mutation of hot environment to room temperature environment, right in quenching process
It has certain damage, influences its service life.Secondly, ball ring used by autoclave seals is loss product, one at a time,
It consumes larger.
Utility model content
The purpose of the utility model is to provide a kind of novel minitype high voltage kettles, change quenching and sealing means, can be real
Now fast and safely efficient quenching.
The specific technical proposal is:
Rapid quenching minitype high voltage kettle, including reaction kettle further include cone seal head, clamping nut, cold end autoclave, connect
Connect device, attaching nut, sample holder；
The reaction kettle is connected by the connector of Be-Cu alloy bipyramid with cold end autoclave, and junction is by connection spiral shell
Mother is fixed, and attaching nut is upper there are two water nozzle, and water nozzle is connect with water cooling system, for connector water cooling；
The other end of cold end autoclave is sealed using cone seal head, and cone seal head is fixed on cold end by clamping nut
Autoclave end；Cone seal head center is equipped with capillary, and capillary is connected to cold end autoclave and pressure system；
Sample holder lower end is magnetic bottom end, and magnetic bottom end is located in cold end autoclave；Magnetic bottom end upper end is connected with non-
The thin stick of magnetic stainless steel, the thin stick of non-magnetic stainless steel penetrate into reaction kettle cylinder type sample bin；It is placed outside cold end autoclave
There is magnet, controls the position of sample holder.
Rapid quenching minitype high voltage kettle provided by the utility model, advantage be, first, quenching mode is rapidly and efficiently pacified
Entirely, pass through the sample holder inside external magnet control, i.e., the quenching of controllable sample cell.Second, sealed taper can be anti-for a long time
Multiple to use, third, reaction kettle does not have to face extreme temperature change, is conducive to the long-time service of autoclave body.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the utility model.
Specific embodiment
Hereinafter, the specific implementation to the utility model is described in detail referring to attached drawing.
As shown in Figure 1, rapid quenching minitype high voltage kettle, including cone seal head 7, clamping nut 6, cold end autoclave 5, company
Connect device 4, attaching nut 3, sample holder 2 and reaction kettle 1.
Reaction kettle 1 is connected by the connector 4 of Be-Cu alloy bipyramid with cold end autoclave 5, and junction is by attaching nut 3
Fixed, there are two water nozzle on attaching nut 3, water nozzle is connect with water cooling system, for 4 water cooling of connector；
The other end of cold end autoclave 5 is sealed using cone seal head 7, and cone seal head 7 is fixed on by clamping nut 6
5 end of cold end autoclave；7 center of cone seal head is equipped with capillary, and capillary is connected to cold end autoclave 5 and pressure system；
2 lower end of sample holder is magnetic bottom end, and magnetic bottom end is located in cold end autoclave 5；Magnetic bottom end upper end is connected with
The thin stick of non-magnetic stainless steel, the thin stick of non-magnetic stainless steel penetrate into 1 cylinder type sample bin of reaction kettle；5 outside of cold end autoclave
It is placed with magnet, controls the position of sample holder 2.
In use process, rapid quenching minitype high voltage kettle is disposed vertically, and sample cell is placed in 1 sample bin of reaction kettle, quenching
When, sample holder 2 is driven using the magnet of 5 outside of cold end autoclave, allows sample cell to move to quenching position from hot end, to realize
Rapid quenching.
Claims (1)
1. rapid quenching minitype high voltage kettle, including reaction kettle (1), which is characterized in that further include cone seal head (7), compress spiral shell
Cap (6), cold end autoclave (5), connector (4), attaching nut (3), sample holder (2)；
The reaction kettle (1) is connected by the connector (4) of Be-Cu alloy bipyramid with cold end autoclave (5), and junction is by even
Connected nut (3) is fixed, and there are two water nozzle on attaching nut (3), water nozzle is connect with water cooling system, for connector (4) water
It is cold；
The other end of cold end autoclave (5) is sealed using cone seal head (7), and cone seal head (7) is solid by clamping nut (6)
It is scheduled on cold end autoclave (5) end；Cone seal head (7) center is equipped with capillary, and capillary is connected to cold end autoclave (5) and presses
Force system；
Sample holder (2) lower end is magnetic bottom end, and magnetic bottom end is located in cold end autoclave (5)；Magnetic bottom end upper end is connected with
The thin stick of non-magnetic stainless steel, the thin stick of non-magnetic stainless steel penetrate into reaction kettle (1) cylinder type sample bin；Cold end autoclave (5)
Outside is placed with magnet, controls the position of sample holder (2).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821903876.7U CN209039527U (en) | 2018-11-19 | 2018-11-19 | Rapid quenching minitype high voltage kettle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821903876.7U CN209039527U (en) | 2018-11-19 | 2018-11-19 | Rapid quenching minitype high voltage kettle |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN209039527U true CN209039527U (en) | 2019-06-28 |
Family
ID=67042668
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201821903876.7U Expired - Fee Related CN209039527U (en) | 2018-11-19 | 2018-11-19 | Rapid quenching minitype high voltage kettle |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN209039527U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109266822A (en) * | 2018-11-19 | 2019-01-25 | 中国科学院地球化学研究所 | Rapid quenching minitype high voltage kettle |
-
2018
- 2018-11-19 CN CN201821903876.7U patent/CN209039527U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109266822A (en) * | 2018-11-19 | 2019-01-25 | 中国科学院地球化学研究所 | Rapid quenching minitype high voltage kettle |
| CN109266822B (en) * | 2018-11-19 | 2023-11-24 | 中国科学院地球化学研究所 | Small-sized autoclave for rapid quenching |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20190628 Termination date: 20201119 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |