CN208975789U - A kind of efficient precipitated calcium carbonate prepares reaction kettle - Google Patents

A kind of efficient precipitated calcium carbonate prepares reaction kettle Download PDF

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Publication number
CN208975789U
CN208975789U CN201821174784.XU CN201821174784U CN208975789U CN 208975789 U CN208975789 U CN 208975789U CN 201821174784 U CN201821174784 U CN 201821174784U CN 208975789 U CN208975789 U CN 208975789U
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China
Prior art keywords
stirring rod
heating
heating tube
reaction kettle
puddle support
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Expired - Fee Related
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CN201821174784.XU
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Chinese (zh)
Inventor
黄栋
刘志宏
陈冬梅
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Gao'an Shengyuan Calcium Carbonate Development Co Ltd
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Gao'an Shengyuan Calcium Carbonate Development Co Ltd
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Abstract

A kind of efficient precipitated calcium carbonate prepares reaction kettle, including reaction kettle shell, heating mechanism and rabbling mechanism, using special heating mechanism, unique heating mechanism shell can be bonded common response kettle housing bottom arcuate structure, internal multiple heating tubes can be good at playing uniformly heated left and right, and radiating fin is set at the top of heating tube, effectively the heat of heating tube can be come out, heating effect is good;It is special to increase mounting plate for heating mechanism housing bottom arcwall face structure, it can be good at for heating tube being fixed on heating cavities bottom.Reaction kettle internal mix material peripheral portion is sufficiently stirred with the second puddle support using the first puddle support, service efficiency is high, center is sufficiently stirred using the realization of third stirring rod, and special E font structure can greatly increase the stirring contact area with material.Using effect is good.The utility model uses the structure of a variety of puddle supports, and agitating mode is reasonable, and mixing effect is good.

Description

A kind of efficient precipitated calcium carbonate prepares reaction kettle
Technical field
The utility model prepares reaction kettle more particularly to a kind of efficient precipitated calcium carbonate.
Background technique
Precipitated calcium carbonate is made from chemical processes.Since its settling volume (2.4-2.8mL/g) ratio uses machine The powdered whiting settling volume (1.1-1.9mL/g) of tool method production greatly, therefore referred to as precipitated calcium carbonate.Its chemical formula For CaCO3, it reacts with all strong acid, generation and corresponding calcium salt (such as calcium chloride CaCl2), while releasing titanium dioxide Carbon.Under room temperature (25 DEG C), the concentration product of precipitated calcium carbonate in water is 8.7/1029, solubility 0.0014;Lightweight carbonic acid The pH value of calcium aqueous solution is 9.5~10.2;The pH value of saturation of the air precipitated calcium carbonate aqueous solution is 8.0~8.6;Precipitated calcium carbonate It is nontoxic, odorless, nonirritant, it is usually white.
Precipitated calcium carbonate is a kind of inorganic chemical product with extensive use, for rubber, plastics, sealant, ink, The industries such as papermaking are modified precipitated calcium carbonate surface, can improve it in the using effect in each field.
Precipitated calcium carbonate method of modifying has two kinds, dry and wet.Conventional wet modified technique is that precipitated calcium carbonate is suspended Liquid, solid content is 10~15%, and temperature is at 20~50 DEG C.After being heated to 70~90 DEG C, modifying agent is added, after being sufficiently stirred, Dehydration, is crushed to obtain product drying.Since the suspended fluid solid content of precipitated calcium carbonate that carburizing reagent generates is not high, generally 10~ 15%, one ton of product of every production need to heat 6~9 tons of liquid, and the consumption energy is larger, high production cost.
Chinese patent literature CN2541436Y is disclosed " a kind of nanometer calcium carbonate synthesis reactor ", and reactor top is circle Column-shaped barrel, lower part are cone, and discharge gate is housed in cone bottom end, and reactor shell is provided with blender, agitating shaft upper end with Motor axis connection, agitating shaft lower end are equipped with agitator arm, annular inflatable pipeline are housed on conical shell inner wall, in annular inflatable Interval is equipped with microvesicle generators on pipeline.Since the reactor only has inside to stir, structure is simple, and stirring efficiency is also not Enough height.And the reaction unit does not have heating mechanism, cannot accomplish to heat precipitated calcium carbonate suspension well, heating effect is not It is good.
Utility model content
The utility model proposes a kind of efficient precipitated calcium carbonate regarding to the issue above and prepares reaction kettle.
Specific technical solution is as follows:
A kind of efficient precipitated calcium carbonate prepares reaction kettle, which is characterized in that including reaction kettle shell, heating mechanism and Rabbling mechanism, the reaction kettle case top be it is columnar structured, bottom is hollow hemisphere structure, is set on the reaction kettle It is equipped with feed inlet, discharge port and support leg, the feed inlet quantity is two, is set to two sides at the top of the reaction kettle;Institute Stating discharge port quantity is 1, is located at reaction kettle housing bottom center;The support leg quantity is 4, is square column Body structure is evenly distributed on the reactor bottom surrounding in being vertically arranged;
The heating mechanism includes heating mechanism shell, and the heating mechanism shell is stainless steel integral structure, described At circular ring type at the top of heating mechanism, bottom is in hollow hemisphere structure, the heating mechanism housing bottom and the reaction kettle Enclosure interior bottom shape, size, position are corresponding, and the heating mechanism shell is fixedly installed on the reaction kettle interior bottom portion Surrounding;The heating mechanism enclosure interior is provided with heating cavities, and the heating cavities bottom centre position is provided with outflux, The outflux is located at the discharge port top position;The heating cavities are internally provided with the first heating tube, the second heating Pipe, third heating tube and the 4th heating tube, first heating tube, the second heating tube, third heating tube and the 4th heating Pipe is cirque structure, and first heating tube, the second heating tube and third heating tube quantity are one, is added described Hot cavity bottom is uniformly distributed from inside to outside;The 4th heating tube quantity is two, at the top of the heating cavities from upper and Under be uniformly distributed;
First heating tube, the second heating tube, third heating tube and the 4th heating tube bottom pass through welding and connect It is connected to mounting plate, top is fixedly installed radiating fin, and the radiating fin quantity at the top of each heating tube is 6;The peace Loading board inside bolt and nut and the heating cavities by being fixedly connected;
Rabbling mechanism include stirring motor, stirring motor axis, cross stirring rod, the first stirring rod, the second stirring rod and Center stirring rod, the stirring motor axis are cylindrical structure, and top is fixedly connected with the stirring motor, and stirring motor axis is logical It crosses motor and drives and realize rotation, the cross stirring rod top center is fixed in stirring motor axis bottom, and described ten Word stirring rod is in cross-shaped structure, is horizontally disposed;The first stirring rod quantity is two, in being vertically arranged, is symmetrically fixed Cross stirring rod two sides of the bottom are connected to, the first puddle support, first puddle support are provided on first stirring rod In frame type structure, quantity of first puddle support on the first stirring rod is six, is distributed in first stirring in two vertical setting of types Bar two sides, every the first puddle support of vertical setting of types are evenly distributed side from top to bottom on first stirring rod;Second stirring Bar quantity is two, in being vertically arranged, is symmetrically fixedly connected on cross stirring rod bottom both ends, on second stirring rod It is provided with the second puddle support, second puddle support is in semicircle ring structure, and quantity of second puddle support on the second stirring rod is Six, second stirring rod both ends, every the second puddle support of vertical setting of types one end on second stirring rod are distributed in two vertical setting of types It is evenly distributed from top to bottom;The center stirring rod is in cylindrical structure, and in being vertically arranged, top is fixedly connected on described ten Word stirring rod bottom centre position, third puddle support is provided on the center stirring rod, and the third puddle support is in E type knot Structure, the third puddle support quantity are 8, wherein four third stirring rods are evenly distributed at the top of the center stirring rod circumferentially Surrounding, four additional third stirring rod are evenly distributed on center stirring rod lower part week position around.
Further, valve is provided on the feed inlet and discharge port.
Further, first heating tube, the second heating tube, the annular radius of third heating tube are sequentially increased.
Further, at triangle bulge-structure at the top of the radiating fin.
Further, first puddle support is fixedly connected with first stirring rod.
Further, second puddle support is fixedly connected with second stirring rod.
Further, the third puddle support is fixedly connected with the center stirring rod.
The utility model has the following beneficial effects:
Using special heating mechanism, unique heating mechanism shell can be bonded common response kettle housing bottom arc knot Structure, internal multiple heating tubes can be good at playing uniformly heated left and right, and radiating fin is arranged at the top of heating tube, can Effectively the heat of heating tube is come out, heating effect is good;For heating mechanism housing bottom arcwall face structure, special increasing Mounting plate is added, can be good at for heating tube being fixed on heating cavities bottom.
Reaction kettle internal mix material peripheral portion is sufficiently stirred with the second puddle support using the first puddle support, is used High-efficient, center is sufficiently stirred using the realization of third stirring rod, and special E font structure can greatly increase and object The stirring contact area of material.Using effect is good.The utility model uses the structure of a variety of puddle supports, and agitating mode is reasonable, Mixing effect is good.
Detailed description of the invention
Fig. 1 is partial sectional view inside the utility model.
Fig. 2 is rabbling mechanism main view.
Fig. 3 is rabbling mechanism left view.
Description of symbols:
Reaction kettle shell 10, feed inlet 11, discharge port 12, support leg 13;
Heating mechanism 14, heating mechanism shell 15, outflux 16, the first heating tube 17, the second heating tube 18, third heating Pipe 19, the 4th heating tube 20, mounting plate 21, radiating fin 22, heating cavities 23;
Rabbling mechanism 24, stirring motor 1, stirring motor axis 2, cross stirring rod 3, the first stirring rod 4, the second stirring rod 5, Center stirring rod 6, the first puddle support 7, second stir 14 framves 8, third puddle support 9;
Temperature sensor 25, single-chip microcontroller 26.
Specific embodiment
It is clear to be more clear the technical solution of the utility model, the utility model is described further below, The technical characteristic of any pair of technical solutions of the utility model carries out the scheme that equivalencing is obtained with conventional reasoning and each falls within this reality With novel protected range.Being fixedly connected mentioned in the utility model, fixed setting are the general connection in machinery field Mode, welding, gluing, bolt and nut connection and screw connection.
A kind of efficient precipitated calcium carbonate prepares reaction kettle, which is characterized in that including reaction kettle shell, heating mechanism and Rabbling mechanism, the reaction kettle case top be it is columnar structured, bottom is hollow hemisphere structure, is set on the reaction kettle It is equipped with feed inlet, discharge port and support leg, the feed inlet quantity is two, is set to two sides at the top of the reaction kettle;Institute Stating discharge port quantity is 1, is located at reaction kettle housing bottom center;The support leg quantity is 4, is square column Body structure is evenly distributed on the reactor bottom surrounding in being vertically arranged;
The heating mechanism includes heating mechanism shell, and the heating mechanism shell is stainless steel integral structure, described At circular ring type at the top of heating mechanism, bottom is in hollow hemisphere structure, the heating mechanism housing bottom and the reaction kettle Enclosure interior bottom shape, size, position are corresponding, and the heating mechanism shell is fixedly installed on the reaction kettle interior bottom portion Surrounding;The heating mechanism enclosure interior is provided with heating cavities, and the heating cavities bottom centre position is provided with outflux, The outflux is located at the discharge port top position;The heating cavities are internally provided with the first heating tube, the second heating Pipe, third heating tube and the 4th heating tube, first heating tube, the second heating tube, third heating tube and the 4th heating Pipe is cirque structure, and first heating tube, the second heating tube and third heating tube quantity are one, is added described Hot cavity bottom is uniformly distributed from inside to outside;The 4th heating tube quantity is two, at the top of the heating cavities from upper and Under be uniformly distributed;
First heating tube, the second heating tube, third heating tube and the 4th heating tube bottom pass through welding and connect It is connected to mounting plate, top is fixedly installed radiating fin, and the radiating fin quantity at the top of each heating tube is 6;The peace Loading board inside bolt and nut and the heating cavities by being fixedly connected;
Rabbling mechanism include stirring motor, stirring motor axis, cross stirring rod, the first stirring rod, the second stirring rod and Center stirring rod, the stirring motor are fixed on the reaction kettle top center, and the stirring motor axis is cylindrical body knot Structure, top are fixedly connected with the stirring motor, and stirring motor axis is driven by motor and realizes rotation, stirring motor axis bottom Reaction kettle shell is run through in portion, stretches to reaction kettle enclosure interior, and be fixed on the cross stirring rod top center, described Cross stirring rod is in cross-shaped structure, is horizontally disposed;The first stirring rod quantity is two, in being vertically arranged, symmetrically admittedly Surely cross stirring rod two sides of the bottom are connected to, the first puddle support, first stirring are provided on first stirring rod Frame is in frame type structure, and quantity of first puddle support on the first stirring rod is six, is distributed in described first in two vertical setting of types and stirs Bar two sides are mixed, every the first puddle support of vertical setting of types is evenly distributed side from top to bottom on first stirring rod;Described second stirs Mixing bar quantity is two, in being vertically arranged, is symmetrically fixedly connected on cross stirring rod bottom both ends, second stirring rod On be provided with the second puddle support, second puddle support is in semicircle ring structure, quantity of second puddle support on the second stirring rod It is six, is distributed in second stirring rod both ends in two vertical setting of types, every the second puddle support of vertical setting of types is one on second stirring rod End is evenly distributed from top to bottom;The center stirring rod is in cylindrical structure, and in being vertically arranged, top is fixedly connected on described Cross stirring rod bottom centre position, third puddle support is provided on the center stirring rod, and the third puddle support is in E type knot Structure, the third puddle support quantity are 8, wherein four third stirring rods are evenly distributed at the top of the center stirring rod circumferentially Surrounding, four additional third stirring rod are evenly distributed on center stirring rod lower part week position around.
Further, reaction kettle hull outside is fixedly installed single-chip microcontroller, and inside is fixedly installed temperature sensor, temperature Sensor, first heating tube, the second heating tube, third heating tube and the 4th heating tube pass through electric wire and the monolithic Machine connection, temperature sensor are DS18B20 digital temperature sensor, and single-chip microcontroller is STC51 single-chip microcontroller, and temperature sensor is by temperature Data transmission determines the switch of each heating tube by temperature data to single-chip microcontroller, single-chip microcontroller, is more than that set temperature is closed, is lower than Set temperature is opened, and it may be value range that set temperature, which can be fixed value, herein, by being set to mcu programming, Single-chip microcontroller is set as well-known technique in the art, this will not be repeated here.
Further, valve is provided on the feed inlet and discharge port.
Further, first heating tube, the second heating tube, the annular radius of third heating tube are sequentially increased.
Further, at triangle bulge-structure at the top of the radiating fin.
Further, first puddle support is fixedly connected with first stirring rod.
Further, second puddle support is fixedly connected with second stirring rod.
Further, the third puddle support is fixedly connected with the center stirring rod.
The utility model has the following beneficial effects:
Using special heating mechanism, unique heating mechanism shell can be bonded common response kettle housing bottom arc knot Structure, internal multiple heating tubes can be good at playing uniformly heated left and right, and radiating fin is arranged at the top of heating tube, can Effectively the heat of heating tube is come out, heating effect is good;For heating mechanism housing bottom arcwall face structure, special increasing Mounting plate is added, can be good at for heating tube being fixed on heating cavities bottom.
Reaction kettle internal mix material peripheral portion is sufficiently stirred with the second puddle support using the first puddle support, is used High-efficient, center is sufficiently stirred using the realization of third stirring rod, and special E font structure can greatly increase and object The stirring contact area of material.Using effect is good.The utility model uses the structure of a variety of puddle supports, and agitating mode is reasonable, Mixing effect is good.

Claims (7)

1. a kind of efficient precipitated calcium carbonate prepares reaction kettle, which is characterized in that including reaction kettle shell, heating mechanism and stir Mix mechanism, the reaction kettle case top be it is columnar structured, bottom is hollow hemisphere structure, is arranged on the reaction kettle There are feed inlet, discharge port and support leg, the feed inlet quantity is two, is set to two sides at the top of the reaction kettle;It is described Discharge port quantity is 1, is located at reaction kettle housing bottom center;The support leg quantity is 4, is square cylinder Structure is evenly distributed on the reactor bottom surrounding in being vertically arranged;
The heating mechanism includes heating mechanism shell, and the heating mechanism shell is stainless steel integral structure, the heating At circular ring type at the top of mechanism, bottom is in hollow hemisphere structure, the heating mechanism housing bottom and the reaction kettle shell Interior bottom portion shape, size, position are corresponding, and the heating mechanism shell is fixedly installed on the reaction kettle interior bottom portion four Week;The heating mechanism enclosure interior is provided with heating cavities, and the heating cavities bottom centre position is provided with outflux, institute It states outflux and is located at the discharge port top position;The heating cavities be internally provided with the first heating tube, the second heating tube, Third heating tube and the 4th heating tube, first heating tube, the second heating tube, third heating tube and the 4th heating tube are equal For cirque structure, first heating tube, the second heating tube and third heating tube quantity are one, empty in the heating Bottom of chamber portion is uniformly distributed from inside to outside;The 4th heating tube quantity is two, at the top of the heating cavities from top to bottom Even distribution;
First heating tube, the second heating tube, third heating tube and the 4th heating tube bottom pass through and be welded and connected with Mounting plate, top are fixedly installed radiating fin, and the radiating fin quantity at the top of each heating tube is 6;The mounting plate By being fixedly connected inside bolt and nut and the heating cavities;
Rabbling mechanism includes stirring motor, stirring motor axis, cross stirring rod, the first stirring rod, the second stirring rod and center Stirring rod, the stirring motor axis are cylindrical structure, and top is fixedly connected with the stirring motor, and stirring motor axis passes through electricity Machine, which drives, realizes rotation, and the cross stirring rod top center is fixed in stirring motor axis bottom, and the cross stirs Bar is mixed in cross-shaped structure, is horizontally disposed;The first stirring rod quantity is two, in being vertically arranged, is symmetrically fixedly connected In being provided with the first puddle support on cross stirring rod two sides of the bottom, first stirring rod, first puddle support is in side Frame-type structure, quantity of first puddle support on the first stirring rod are six, are distributed in first stirring rod two in two vertical setting of types Side, every the first puddle support of vertical setting of types are evenly distributed side from top to bottom on first stirring rod;The second stirring rod number Amount is two, in being vertically arranged, is symmetrically fixedly connected on cross stirring rod bottom both ends, is arranged on second stirring rod There is the second puddle support, second puddle support is in semicircle ring structure, and quantity of second puddle support on the second stirring rod is six, Be distributed in second stirring rod both ends in two vertical setting of types, every the second puddle support of vertical setting of types on second stirring rod one end from upper and Under be evenly distributed;The center stirring rod is in cylindrical structure, and in being vertically arranged, top is fixedly connected on the cross stirring Bar bottom centre position is provided with third puddle support on the center stirring rod, and the third puddle support is in E type structure, described Third puddle support quantity is 8, wherein four third stirring rods are evenly distributed on center stirring rod top week around, separately Outer four third stirring rods are evenly distributed on center stirring rod lower part week position around.
2. a kind of efficient precipitated calcium carbonate as described in claim 1 prepares reaction kettle, it is characterized in that, the feed inlet with go out Valve is provided in material mouth.
3. a kind of efficient precipitated calcium carbonate as described in claim 1 prepares reaction kettle, it is characterized in that, first heating Pipe, the second heating tube, the annular radius of third heating tube are sequentially increased.
4. a kind of efficient precipitated calcium carbonate as described in claim 1 prepares reaction kettle, it is characterized in that, the radiating fin top Portion is at triangle bulge-structure.
5. a kind of efficient precipitated calcium carbonate as described in claim 1 prepares reaction kettle, it is characterized in that, first puddle support It is fixedly connected with first stirring rod.
6. a kind of efficient precipitated calcium carbonate as described in claim 1 prepares reaction kettle, it is characterized in that, second puddle support It is fixedly connected with second stirring rod.
7. a kind of efficient precipitated calcium carbonate as described in claim 1 prepares reaction kettle, it is characterized in that, the third puddle support It is fixedly connected with the center stirring rod.
CN201821174784.XU 2018-07-24 2018-07-24 A kind of efficient precipitated calcium carbonate prepares reaction kettle Expired - Fee Related CN208975789U (en)

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CN201821174784.XU CN208975789U (en) 2018-07-24 2018-07-24 A kind of efficient precipitated calcium carbonate prepares reaction kettle

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201821174784.XU CN208975789U (en) 2018-07-24 2018-07-24 A kind of efficient precipitated calcium carbonate prepares reaction kettle

Publications (1)

Publication Number Publication Date
CN208975789U true CN208975789U (en) 2019-06-14

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Application Number Title Priority Date Filing Date
CN201821174784.XU Expired - Fee Related CN208975789U (en) 2018-07-24 2018-07-24 A kind of efficient precipitated calcium carbonate prepares reaction kettle

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Granted publication date: 20190614