CN208928146U - A kind of chlorination reaction equipment - Google Patents
A kind of chlorination reaction equipment Download PDFInfo
- Publication number
- CN208928146U CN208928146U CN201821138968.0U CN201821138968U CN208928146U CN 208928146 U CN208928146 U CN 208928146U CN 201821138968 U CN201821138968 U CN 201821138968U CN 208928146 U CN208928146 U CN 208928146U
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- CN
- China
- Prior art keywords
- autoclave body
- gas
- chlorination reaction
- pipe
- reaction equipment
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Abstract
The utility model discloses a kind of chlorination reaction equipment, including autoclave body and the kettle cover being tightly connected with the autoclave body, kettle cover is equipped with exhaust structure, the structure can both guarantee the pressure balance in kettle, it is normally carried out the chemical reaction in kettle, also achieve the purpose that prevent from surprisingly occurring, specifically, pass through the downtake pipe being sequentially communicated, gas-liquid separation device carries out gas-liquid separation to the gas of discharge, pass through the gas-liquid separation device being sequentially communicated, drain pipe, fluid reservoir, recycle inlet tube, the liquid separated is delivered in autoclave body, to reduce the waste of solution and the pollution to environment in autoclave body；The utility model, which also passes through the chlorination tube, tee tube and discharge nozzle being sequentially communicated, comes into full contact with chlorine with unclassified stores in chlorine gas transfer to autoclave body, guarantee that chlorination reaction sufficiently carries out, it avoids material from being attached on inside pipe wall, is also convenient for installation and maintenance, facilitate operation.
Description
Technical field
The utility model relates to technical field of chemical production equipment, in particular to a kind of chlorination reaction equipment.
Background technique
Monoxone is important Organic Chemicals, is mainly used in medicine, pesticide, dyestuff, petrochemical industry, daily-use chemical industry
Etc. industries, with the exploitation of its new application field, using very wide with development prospect.Domestic chloroacetic chlorination is anti-at present
Answering inside the autoclave body of equipment has enamel to do back boxing, and surface is harder, is a kind of excellent corrosion resistant apparatus.But this chlorination reaction is set
Standby disadvantage is it is also obvious that required chlorine usually passes through the top that autoclave body is arranged in and the delivery pipe being inserted into liquid phase enters kettle
In vivo, it is reacted with material therein, in the liquid phase due to delivery pipe long period of soaking, material can be attached to the interior of delivery pipe
Wall is not easily cleaned.Existing chlorination reaction equipment, which is equipped with exhaust structure, makes the chemistry in kettle to guarantee the pressure balance in kettle
Reaction is normally carried out, while also achieving the purpose that prevent from surprisingly occurring, but solution is logical in kettle in existing chlorination reaction equipment
It crosses exhaust pipe and is discharged, on the one hand waste reaction solution, on the other hand also result in environmental pollution.
Utility model content
The purpose of this utility model is to provide a kind of chlorination reaction equipment, to solve the above technical problems.
To achieve the goals above, the technical solution of the utility model are as follows:
A kind of chlorination reaction equipment is set at the top of the kettle cover including autoclave body and the kettle cover being tightly connected with the autoclave body
There are feed pipe, downtake pipe and circulation inlet tube, the downtake pipe to be communicated with gas-liquid point far from one end of the kettle cover
From device, the top of the gas-liquid separation device is communicated with second exhaust pipe, the gas far from the side of the downtake pipe
The bottom of liquid separating apparatus is communicated with drain pipe, and the one of the drain pipe one end and fluid reservoir far from the gas-liquid separation device
End connection, the other end of the fluid reservoir are connected to the circulation inlet tube；The top of the kettle cover is equipped with stirring motor, described
The output end of stirring motor is connected with agitating shaft, and the lower end of the agitating shaft extends in the autoclave body；Outside the agitating shaft
Surface is fixedly connected with mixing component；The bottom of the autoclave body is equipped with discharge nozzle, and the lower end of the discharge nozzle is communicated with tee tube,
The lower end of the tee tube is equipped with the first ball valve；The side ports of the tee tube are communicated with chlorination tube, and the chlorination tube is equipped with
Second ball valve and check-valves.
Preferably, the outer wall of the kettle cover is equipped with the first collet, and the side wall bottom end of first collet is equipped with first circulation
Water inlet and first circulation water out.
Preferably, the downtake pipe is equipped with pressure sensor and electromagnetic valve；The circulation inlet tube is equipped with
Third ball valve.
Preferably, the second exhaust pipe is communicated with gas collector far from one end of the gas-liquid separation device.
Preferably, the outer wall of the autoclave body is equipped with the second collet, and the side wall bottom end of second collet is equipped with second circulation
Water inlet and second circulation water out.
Preferably, the mixing component includes the first stirring slurry of at least two, and first agitating paddle is laterally arranged in described
On agitating shaft.
It is further preferred that the blade quantity of first agitating paddle successively increases from top to bottom.
It is further preferred that the mixing component further includes the second stirring slurry, second stirring slurry is located at described first
The lower section of stirring slurry, and second stirring slurry is inclined on the agitating shaft.
Preferably, the autoclave body and the kettle cover are enamel structure.
Compared with prior art, the utility model has the beneficial effects that:
(1) kettle cover of the utility model is equipped with exhaust structure, which can both guarantee the pressure balance in kettle, and make kettle
Interior chemical reaction is normally carried out, and also achievees the purpose that prevent surprisingly to occur, specifically, passing through the first exhaust being sequentially communicated
Pipe, gas-liquid separation device carry out gas-liquid separation to the gas of discharge, pass through the gas-liquid separation device, drain pipe, storage being sequentially communicated
Flow container, circulation inlet tube, the liquid separated are delivered in autoclave body, to reduce in autoclave body the waste of solution and to environment
Pollution.
(2) the utility model passes through the chlorination tube, tee tube and the discharge nozzle that are sequentially communicated, by chlorine gas transfer to autoclave body,
It comes into full contact with chlorine with unclassified stores, guarantees that chlorination reaction sufficiently carries out, avoid material from being attached on inside pipe wall, be also convenient for pacifying
Dress and maintenance, facilitate operation.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of chlorination reaction equipment.
In figure, 1- autoclave body, 2- kettle cover, 3- feed pipe, 4- downtake pipe, 5- circulation inlet tube, 6- gas-liquid separation device,
7- second exhaust pipe, 8- drain pipe, 9- fluid reservoir, 10- stirring motor, 11- agitating shaft, 12- discharge nozzle, 13- tee tube, 14-
Chlorination tube, the first ball valve of 15-, the second ball valve of 16-, 17- check-valves, 18- electromagnetic valve, the first collet of 19-, 20- first circulation
Water inlet, 21- first circulation water out, 22- gas collector, the second collet of 23-, 24- second circulation water inlet, 25-
Two-cycle outlet, the first stirring slurry of 26-, the second stirring slurry of 27-, 28- third ball valve, 29- device for supplying chlorine.
Specific embodiment
Specific embodiment of the present utility model is described further with reference to the accompanying drawing.It should be noted that
The explanation of these embodiments is used to help to understand the utility model, but does not constitute the restriction to the utility model.This
Outside, technical characteristic involved in the various embodiments of the present invention described below is as long as they do not conflict with each other
It can be combined with each other.
As shown in Figure 1, the chlorination reaction equipment of the utility model, the kettle cover 2 including autoclave body 1 and with the sealed connection of autoclave body 1,
The top of kettle cover 2 is equipped with feed pipe 3, downtake pipe 4 and circulation inlet tube 5, and downtake pipe 4 connects far from one end of kettle cover 2
It is connected with gas-liquid separation device 6, the top of gas-liquid separation device 6 is communicated with second exhaust pipe 7 far from the side of downtake pipe 4,
The bottom of gas-liquid separation device 6 is communicated with drain pipe 8, the one end of drain pipe 8 far from gas-liquid separation device 6 and the one of fluid reservoir 9
The other end of end connection, fluid reservoir 9 is connected to circulation inlet tube 5；The top of kettle cover 2 is equipped with stirring motor 10, stirring motor 10
Output end be connected with agitating shaft 11, the lower end of agitating shaft 11 extends in autoclave body 1；The outer surface of agitating shaft 11 is fixedly connected with
Mixing component；The bottom of autoclave body 1 is equipped with discharge nozzle 12, and the lower end of discharge nozzle 12 passes through lap joint flange (not shown) and threeway
The upper port of pipe 13 is connected to, and the lower end of tee tube 13 is equipped with the first ball valve 15；The side ports of tee tube 13 are communicated with chlorination tube 14,
Chlorination tube 14 is equipped with the second ball valve 16 and check-valves 17 far from one end of tee tube 13.
Further, autoclave body 1 and kettle cover 2 are enamel structure.
Further, the outer wall of kettle cover 2 is equipped with the first collet 19, and the side wall bottom end of the first collet 19 is equipped with first circulation water
Import 20 and first circulation water out 21.
Further, second exhaust pipe 7 is communicated with gas collector 22 far from one end of gas-liquid separation device 6.
Further, downtake pipe 4 is equipped with pressure sensor (not shown) and electromagnetic valve 18.
Further, circulation inlet tube is equipped with third ball valve 28.
Further, the outer wall of autoclave body 1 is equipped with the second collet 23, and the side wall bottom end of the second collet 23 is equipped with second circulation water
Import 24 and second circulation water out 25.
Further, mixing component includes the first stirring slurry of at least two 26, and the first agitating paddle 26 is laterally arranged in agitating shaft
On 11, the blade quantity of the first agitating paddle 26 successively increases from top to bottom；Mixing component further includes the second stirring slurry 27, and second
Stirring slurry 27 is located at the lower section of the first stirring slurry 26, and the second stirring slurry 27 is inclined on agitating shaft 11.
The working principle of the chlorinating container of the utility model is as follows:
When work, liquid material enters in autoclave body 1 from feed pipe, opens stirring motor 10, and stirring motor 10 drives stirring
Axis 11 and mixing component rotation, while after chlorination tube 14 is connected to device for supplying chlorine 29, the second ball valve 16 of opening and check-valves
17, close the first ball valve 15, chlorine pass sequentially through chlorination tube 14, tee tube 13, discharge nozzle 12 enter autoclave body 1 in, chlorine and its
Its material comes into full contact with, and guarantees that chlorination reaction sufficiently carries out, chlorination reaction releases a large amount of heat, so that the liquid in autoclave body 1
It is vaporized into vapor, to 23 injection cold water of the first collet 19 and the second interlayer set, achievees the purpose that cooling, is liquefied as vapor
Liquid water provides reaction efficiency；It can detect the intracorporal pressure of kettle by the pressure sensor in the downtake pipe 4 on autoclave body 1,
When pressure is excessive, pressure sensor can transmit a signal to electromagnetic valve 18 simultaneously, and electromagnetic valve 18 is caused to open, in autoclave body 1
Gas and the solution droplets that splash through downtake pipe 4 enter gas-liquid separation device 6, keep the liquid in gas-liquid mixture exhausted
It is most of to be entered in fluid reservoir 9 by drain pipe 8, and gas then passes through second exhaust pipe 7 and is discharged, the liquid inside fluid reservoir 9
When body capacity is exceeded, third ball valve 28 is opened, and the solution in fluid reservoir 9 is returned in autoclave body 1, that is, the waste of solution is avoided to avoid again
The pollution of environment.At the end of work, the second ball valve 16 and check-valves 17 are closed, the first ball valve 15 is opened, passes through discharge nozzle 12
Discharging.
The embodiments of the present invention is explained in detail in conjunction with attached drawing above, but the utility model is not limited to be retouched
The embodiment stated.For a person skilled in the art, right in the case where not departing from the utility model principle and spirit
These embodiments carry out a variety of change, modification, replacement and modification, still fall in the protection scope of the utility model.
Claims (8)
1. a kind of chlorination reaction equipment, it is characterised in that: including autoclave body and the kettle cover being tightly connected with the autoclave body, the kettle cover
Top be equipped with feed pipe, downtake pipe and circulation inlet tube, the downtake pipe far from the kettle cover one end be connected to
There is gas-liquid separation device, the top of the gas-liquid separation device is communicated with second exhaust far from the side of the downtake pipe
Pipe, the bottom of the gas-liquid separation device are communicated with drain pipe, the one end of the drain pipe far from the gas-liquid separation device with
One end of fluid reservoir is connected to, and the other end of the fluid reservoir is connected to the circulation inlet tube；The top of the kettle cover is equipped with and stirs
Motor is mixed, the output end of the stirring motor is connected with agitating shaft, and the lower end of the agitating shaft extends in the autoclave body；It is described
The outer surface of agitating shaft is fixedly connected with mixing component；The bottom of the autoclave body is equipped with discharge nozzle, and the lower end of the discharge nozzle connects
It is connected with tee tube, the lower end of the tee tube is equipped with the first ball valve；The side ports of the tee tube are communicated with chlorination tube, described logical
Chlorine pipe is equipped with the second ball valve and check-valves.
2. chlorination reaction equipment according to claim 1, it is characterised in that: the outer wall of the kettle cover is equipped with the first collet,
The side wall bottom end of first collet is equipped with first circulation water inlet and first circulation water out.
3. chlorination reaction equipment according to claim 1, it is characterised in that: the downtake pipe is equipped with pressure sensing
Device and electromagnetic valve；The circulation inlet tube is equipped with third ball valve.
4. chlorination reaction equipment according to claim 1, it is characterised in that: the second exhaust pipe is far from the gas-liquid point
One end from device is communicated with gas collector.
5. chlorination reaction equipment according to claim 1, it is characterised in that: the outer wall of the autoclave body is equipped with the second collet,
The side wall bottom end of second collet is equipped with second circulation water inlet and second circulation water out.
6. chlorination reaction equipment according to claim 1, it is characterised in that: the mixing component includes at least two first
Stirring slurry, first agitating paddle are laterally arranged on the agitating shaft；The mixing component further includes the second stirring slurry, described
Second agitating paddle is located at the lower section of first stirring slurry, and second stirring slurry is inclined on the agitating shaft.
7. chlorination reaction equipment according to claim 6, it is characterised in that: the blade quantity of first agitating paddle is from upper
Successively increase under.
8. chlorination reaction equipment according to claim 1, it is characterised in that: the autoclave body and the kettle cover are enamel knot
Structure.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821138968.0U CN208928146U (en) | 2018-07-18 | 2018-07-18 | A kind of chlorination reaction equipment |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821138968.0U CN208928146U (en) | 2018-07-18 | 2018-07-18 | A kind of chlorination reaction equipment |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN208928146U true CN208928146U (en) | 2019-06-04 |
Family
ID=66716244
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201821138968.0U Expired - Fee Related CN208928146U (en) | 2018-07-18 | 2018-07-18 | A kind of chlorination reaction equipment |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN208928146U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116969710A (en) * | 2023-07-31 | 2023-10-31 | 湖北工业大学 | Carbon fixing process and equipment suitable for prefabricated part factory |
-
2018
- 2018-07-18 CN CN201821138968.0U patent/CN208928146U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116969710A (en) * | 2023-07-31 | 2023-10-31 | 湖北工业大学 | Carbon fixing process and equipment suitable for prefabricated part factory |
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| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20190604 Termination date: 20200718 |
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| CF01 | Termination of patent right due to non-payment of annual fee |