CN208883506U - A kind of continuous atomizing carbonators - Google Patents

A kind of continuous atomizing carbonators Download PDF

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Publication number
CN208883506U
CN208883506U CN201821532837.0U CN201821532837U CN208883506U CN 208883506 U CN208883506 U CN 208883506U CN 201821532837 U CN201821532837 U CN 201821532837U CN 208883506 U CN208883506 U CN 208883506U
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China
Prior art keywords
pipe
tower
slurry
carbonators
inlet pipe
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Expired - Fee Related
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CN201821532837.0U
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Chinese (zh)
Inventor
王爱兵
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Nanjing Ai Feng Technology Co Ltd
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Nanjing Ai Feng Technology Co Ltd
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Priority to CN201821532837.0U priority Critical patent/CN208883506U/en
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Abstract

The utility model discloses a kind of continuous atomizing carbonators, including vertical carbonizing tower, carbon-dioxide generator, inlet pipe, grout outlet, loop exit, slurry recycling system;Loop exit connects inlet pipe by slurry recycling system, and slurry recycling system includes circulation pipe, circulating pump, heater, is also connected with slurry tank at the top of inlet pipe;The bottom of inlet pipe connects slurry dispenser, slurry dispenser includes several distributor pipes, high-pressure nozzle, the bottom of inlet pipe connects distributor pipe, the radial uniform distribution of distributor pipe, the tower wall of vertical carbonizing tower is equipped with carbon dioxide pipe, several air inlet spray heads are uniformly equipped on carbon dioxide pipe, carbon dioxide pipe connects carbon-dioxide generator.Carbon dioxide, calcium hydroxide effectively spray, so that the contact area of carbon dioxide and calcium hydroxide is big, time of contact is long, and carburizing reagent speed is fast, and carbonization efficiency improves, while being carbonized completely, save raw material, rationally effective control carburizing temperature.

Description

A kind of continuous atomizing carbonators
Technical field
The present invention relates to carbonizing plant field, specially a kind of continuous atomizing carbonators.
Background technique
Calcium carbonate is a kind of inorganic compound, is commonly called as lime stone, lime stone, mountain flour, marble, calcite, is a kind of chemical combination Object, chemical formula are CaCO3, it is in neutrality, is substantially insoluble in, is dissolved in acid.Calcium carbonate is important construction material, industrial to use Way is very wide, and calcium carbonate is mainly used for the multiple fields such as plastics, rubber in the prior art.Nanometer calcium carbonate is also known as ultra tiny carbonic acid Calcium, the most mature industry of nanometer calcium carbonate application is that plastics industry is mainly used in high-grade plastic products.China is carbon in the world The big producer of sour calcium resource, currently, domestic production nanometer calcium carbonate carbonizing plant mainly has normal agitation carbonators, continuous Multistage spray carbonation tower and hypergravity synthesizer etc..
Carbonizing plant in the prior art has the following problems when producing nanometer grade calcium carbonate: 1, due to calcium hydroxide Be injection, the uniformity of injection, between influence calcium hydroxide and carbon dioxide contact area and time of contact, influence to be carbonized Speed;2, the efficiency being carbonized, existing continuous spray chamber's carbonators spray calcium hydroxide solution, and processing speed is slow, carbon It is slow to change speed;3, most preferably 60-80 degrees Celsius of the temperature of carburizing reagent, the temperature of solution is difficult to effectively keep in reaction process Optimum temperature.
Summary of the invention
To solve the above problems, carbon dioxide is evenly distributed, hydrogen-oxygen the invention discloses a kind of continuous atomizing carbonators Change calcium effectively to spray, so that the contact area of carbon dioxide and calcium hydroxide is big, time of contact is long, and carburizing reagent speed is fast, The efficiency that is carbonized improves, while being carbonized completely, saves raw material, rationally effective control carburizing temperature.
In order to reach the goals above, the invention provides the following technical scheme:
A kind of continuous atomizing carbonators, including vertical carbonizing tower, carbon-dioxide generator, inlet pipe, grout outlet, circulation Outlet, slurry recycling system;The top of the vertical carbonizing tower is equipped with inlet pipe, and the bottom of the vertical carbonizing tower is equipped with pulp The lower part side of pipe, the vertical carbonizing tower is equipped with loop exit, and the loop exit is connected by slurry recycling system into slurry Pipe, the slurry recycling system include circulation pipe, circulating pump, heater, are equipped with heater, the circulation on the circulation pipe Pipe connects inlet pipe by circulating pump, is also connected with slurry tank at the top of the inlet pipe;The bottom of the inlet pipe connects slurry Distributor, the slurry dispenser include several distributor pipes, high-pressure nozzle, and the distributor pipe is equipped with high-pressure nozzle;It is described into The bottom for starching pipe connects distributor pipe, and the tower wall of the radial uniform distribution of distributor pipe, the vertical carbonizing tower is equipped with dioxy Change carbon air inlet pipe, the rounded circular tower wall of carbon dioxide pipe, if being uniformly equipped on the carbon dioxide pipe Dry air inlet spray head, the carbon dioxide pipe connect carbon-dioxide generator.
Further, the tower body of the vertical carbonizing tower is equipped with transparent windows.
Further, the heater is electric heater.Electric heater is easy to use, the convenient control to temperature.
Further, PH detector is equipped in the vertical carbonizing tower.
Further, temperature detector is equipped in the vertical carbonizing tower.
Further, be equipped with mixing component in the vertical carbonizing tower, the mixing component include agitating shaft, stirring slurry, Motor, the stirring slurry pass through stirring axis connection motor.
Further, the bottom of vertical carbonizing tower is arranged in the mixing component, and the mixing component is arranged two groups altogether.
Further, cleaning shoe is equipped on the inside of the tower wall of the vertical carbonizing tower.
Compared with prior art, the invention has the benefit that this A Yong spray of 1, carbon dioxide and calcium hydroxide slurry Head injection, realizes three-dimensional contact, and the contact area of carbon dioxide and calcium hydroxide slurry is big, and time of contact is long, so that carbonization More evenly, carbonization speed is fast;2, being cycling in and out for calcium hydroxide slurry is realized, so that carbonization degree completely is high;3, carburizing temperature is adopted Effective carburizing temperature is maintained with the calcium hydroxide in heater warming cycle, it is easy to operate and more time saving and energy saving.
Detailed description of the invention
Fig. 1,1 structural schematic diagram of the embodiment of the present invention;
The structural schematic diagram of Fig. 2,1 slurry dispenser of the embodiment of the present invention;
Fig. 3,1 perspective view of the embodiment of the present invention;
Fig. 4,2 structural schematic diagram of the embodiment of the present invention.
Wherein: vertical carbonizing tower 1, carbon-dioxide generator 2, inlet pipe 3, grout outlet 4, loop exit 5, size circulations system System 6, circulation pipe 61, circulating pump 62, heater 63, threeway 7, slurry tank 8, slurry dispenser 9, distributor pipe 91, high-pressure nozzle 92, Carbon dioxide pipe 10, air inlet spray head 11, transparent windows 12, PH detector 13, temperature detector 14, mixing component 15, Cleaning shoe 16.
Specific embodiment
With reference to the accompanying drawings and detailed description, the present invention is furture elucidated, it should be understood that following specific embodiments are only For illustrating the present invention rather than limiting the scope of the invention.
As shown in Figure 1, Figure 2, Figure 3 shows, a kind of continuous atomizing carbonators, including vertical carbonizing tower 1, carbon-dioxide generator 2, inlet pipe 3, grout outlet 4, loop exit 5, slurry recycling system 6.Slurry enters from inlet pipe, and carbon dioxide is from carbon dioxide Generator enters in carbonators, and carburizing reagent occurs in carbonators, and mixed slurry is recycled from loop exit to flow out, again Enter from inlet pipe, after completing carburizing reagent, slurry is flowed out from grout outlet, then through processes such as subsequent filtering, filters pressing, drying Obtain nanometer grade calcium carbonate.The top of vertical carbonizing tower is equipped with inlet pipe, and the bottom of vertical carbonizing tower is equipped with grout outlet, vertical carbon The lower part side for changing tower is equipped with loop exit, and loop exit connects inlet pipe, slurry recycling system packet by slurry recycling system Circulation pipe 61, circulating pump 62, heater 63 are included, is equipped with heater on circulation pipe, circulation pipe connects inlet pipe by circulating pump; The top of inlet pipe is equipped with threeway 7, and one end of threeway connects slurry tank 8, and the other end connects circulation pipe.New slurry is from slurry tank In enter inlet pipe, subsequently into rear carbonators, after carbonators injection, be flowed into cyclic system from the loop exit of bottom In system, it then is re-introduced into carbonators through slurry tank, realizes circulation carbonization, carbonization speed is fast, carbonization effect is good.Inlet pipe Bottom connects slurry dispenser 9, and slurry dispenser includes several distributor pipes 91, high-pressure nozzle 92, and distributor pipe is equipped with high pressure spray Head;The bottom of inlet pipe connects distributor pipe, and the tower wall of the radial uniform distribution of distributor pipe, vertical carbonizing tower is equipped with dioxy Change carbon air inlet pipe 10, carbon dioxide pipe rounded circular tower wall is uniformly equipped with several air inlets on carbon dioxide pipe Spray head 11, carbon dioxide pipe connect carbon-dioxide generator.
In the present embodiment, the tower body of vertical carbonizing tower is equipped with transparent windows 12.Transparent windows are convenient to carbonization Carbonization situation observation in tower.
In the present embodiment, heater is electric heater.Electric heater is easy to use, the convenient control to temperature.
In the present embodiment, PH detector 13 is equipped in vertical carbonizing tower.Carburizing temperature is 60~70 DEG C, and carbonization terminal can It is determined with the measurement of pH value, when pH value is 7 or so, as terminal.It can judge carbonization eventually according to the testing result of PH detector Point.
In the present embodiment, temperature detector 14 is equipped in vertical carbonizing tower.Carburizing temperature is 60~70 DEG C, passes through temperature The temperature in carbonators that detector detects, controls the heated condition of electrothermal heater, and the temperature of slurry is controlled reasonable In the range of, and then realize reasonable control carburizing temperature.
Embodiment 2
As shown in figure 4, a kind of continuous atomizing carbonators is equipped with mixing component in the present embodiment in vertical carbonizing tower 15, mixing component includes agitating shaft, stirring slurry, motor, and stirring slurry passes through stirring axis connection motor.In the present embodiment, it stirs The bottom of vertical carbonizing tower is arranged in component, and mixing component is arranged two groups altogether.In the present embodiment, in the tower wall of vertical carbonizing tower Side is equipped with cleaning shoe 16, and since slurry can be ejected into tower wall in course of injection, cleaning shoe can effectively scrape this part slurry Material.Can be used motor in the prior art, traction rope, cleaning shoe structure realize that automatic scraping mud, motor pass through traction rope and connects Connect cleaning shoe.
Remaining structure is same as Example 1, and details are not described herein.
Embodiment 3
The course of work of the carbonators of the embodiment of the present invention 1: new calcium hydroxide slurry entered from slurry tank into Slurry pipe, is then ejected into tower from high-pressure nozzle, meanwhile, carbon dioxide enters carbon dioxide from carbon-dioxide generator Pipe, is then ejected into tower from air inlet spray head, and carbon dioxide is contacted with calcium hydroxide slurry occurs carburizing reagent, and slurry is by gravity It influences, drops into the bottom of carbonators, then flowed out from loop exit, be re-introduced into inlet pipe through the circulatory system, fall again It returns in tower, forms the slurry of circulation, slurry is constantly reacted with carbon dioxide exposure, when carburizing reagent is completed, opens tower The grout outlet of body bottom, the slurry (ingredient is calcium carbonate) after completing carbonization are discharged from grout outlet.
The technical means disclosed in the embodiments of the present invention is not limited only to technological means disclosed in above embodiment, further includes Technical solution consisting of any combination of the above technical features.It should be pointed out that for those skilled in the art For, various improvements and modifications may be made without departing from the principle of the present invention, these improvements and modifications are also considered as Protection scope of the present invention.

Claims (8)

1. a kind of continuous atomizing carbonators, it is characterised in that: including vertical carbonizing tower, carbon-dioxide generator, inlet pipe, go out Starch pipe, loop exit, slurry recycling system;The top of the vertical carbonizing tower is equipped with inlet pipe, the bottom of the vertical carbonizing tower Portion is equipped with grout outlet, and the lower part side of the vertical carbonizing tower is equipped with loop exit, and the loop exit passes through size circulations system System connection inlet pipe, the slurry recycling system include circulation pipe, circulating pump, heater, are equipped with heating on the circulation pipe Device, the circulation pipe connect inlet pipe by circulating pump, are also connected with slurry tank at the top of the inlet pipe;The bottom of the inlet pipe Portion connects slurry dispenser, and the slurry dispenser includes several distributor pipes, high-pressure nozzle, and the distributor pipe is equipped with high pressure spray Head;The bottom of the inlet pipe connects distributor pipe, the radial uniform distribution of distributor pipe, in the tower wall of the vertical carbonizing tower Equipped with carbon dioxide pipe, the rounded circular tower wall of carbon dioxide pipe, on the carbon dioxide pipe uniformly Be equipped with several air inlet spray heads, the carbon dioxide pipe connects carbon-dioxide generator.
2. a kind of continuous atomizing carbonators as described in claim 1, it is characterised in that: on the tower body of the vertical carbonizing tower Equipped with transparent windows.
3. a kind of continuous atomizing carbonators as described in claim 1, it is characterised in that: the heater is electric heater.
4. a kind of continuous atomizing carbonators as described in claim 1, it is characterised in that: be equipped with PH in the vertical carbonizing tower Detector.
5. a kind of continuous atomizing carbonators as described in claim 1, it is characterised in that: be equipped with temperature in the vertical carbonizing tower Spend detector.
6. a kind of continuous atomizing carbonators as described in claim 1, it is characterised in that: be equipped with and stir in the vertical carbonizing tower Component is mixed, the mixing component includes agitating shaft, stirring slurry, motor, and the stirring slurry passes through stirring axis connection motor.
7. a kind of continuous atomizing carbonators as claimed in claim 6, it is characterised in that: the mixing component is arranged vertical The bottom of carbonators, the mixing component are arranged two groups altogether.
8. a kind of continuous atomizing carbonators as described in claim 1, it is characterised in that: in the tower wall of the vertical carbonizing tower Side is equipped with cleaning shoe.
CN201821532837.0U 2018-09-19 2018-09-19 A kind of continuous atomizing carbonators Expired - Fee Related CN208883506U (en)

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Application Number Priority Date Filing Date Title
CN201821532837.0U CN208883506U (en) 2018-09-19 2018-09-19 A kind of continuous atomizing carbonators

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201821532837.0U CN208883506U (en) 2018-09-19 2018-09-19 A kind of continuous atomizing carbonators

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CN208883506U true CN208883506U (en) 2019-05-21

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2021040509A1 (en) * 2019-08-26 2021-03-04 Petroliam Nasional Berhad (Petronas) Method for sequestering carbon

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2021040509A1 (en) * 2019-08-26 2021-03-04 Petroliam Nasional Berhad (Petronas) Method for sequestering carbon

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Granted publication date: 20190521

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