CN208878563U - A kind of synthesis reaction vessel convenient for sampling - Google Patents
A kind of synthesis reaction vessel convenient for sampling Download PDFInfo
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- CN208878563U CN208878563U CN201821319219.8U CN201821319219U CN208878563U CN 208878563 U CN208878563 U CN 208878563U CN 201821319219 U CN201821319219 U CN 201821319219U CN 208878563 U CN208878563 U CN 208878563U
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- autoclave body
- sampling
- reaction vessel
- synthesis reaction
- fixedly connected
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Abstract
The utility model relates to synthetic reaction container technical fields, and disclose a kind of synthesis reaction vessel convenient for sampling, including autoclave body, side at the top of the autoclave body is fixedly installed with loading hopper, and the bottom of autoclave body side is fixedly connected with support base, the bottom movable sleeve of the autoclave body is connected to rotary shaft, the side of the rotary shaft is fixedly installed with stirring blade, and the bottom end of rotary shaft is fixedly attached on the output shaft of motor, the outside of the motor at the top of fixed frame and support base by being fixedly connected, the side of autoclave body bottom is fixedly installed with out funnel, the bottom of funnel side is fixedly installed with removable cover out.This is convenient for the synthesis reaction vessel of sampling, pass through the cooperation of scale layer and positioning sleeve, it can be during detection, the position of sampling box decline is positioned, it is extracted so as to the product to reaction kettle inside every aspect, so that the data of pattern detection are more abundant, and then improve the accuracy of testing result.
Description
Technical field
The utility model relates to synthetic reaction container technical field, specially a kind of synthesis reaction vessel convenient for sampling.
Background technique
Reaction kettle, which refers to, provides the container that physically or chemically reacts, and by the structure design and parameter configuration to container,
Realize that functions, the reaction kettles such as heating, evaporation and the cooling that technique requires have the characteristics that corrosion-resistant, acidproof, alkaline-resisting and high temperature resistant,
And it is widely used in the industries such as chemical industry, petroleum and rubber；Since reaction kettle is opposite in one during synthetic product
In the state of sealing, it is difficult to the progress of synthetic reaction is detected by sampling, to can not accurately judge needed for Product formation
Time, and the product of reaction kettle inside every aspect cannot be detected when detecting, be easy to cause testing result not smart
Really, we provide a kind of synthesis reaction vessels convenient for sampling thus.
Utility model content
The technical issues of solution
In view of the deficiencies of the prior art, the utility model provides a kind of synthesis reaction vessel convenient for sampling, and having can
It is convenient for sampling when detecting, so as to the time needed for accurately judging Product formation, while can be in reaction kettle
The product of portion's every aspect extracts, so that the sample of detection is more abundant, the advantages that improving the accuracy of testing result,
Solving due to reaction kettle is in the state of an opposing seal during synthetic product, it is difficult to be examined by sampling
The progress of synthetic reaction is surveyed, thus the time needed for can not accurately judging Product formation, and when detecting cannot be to reaction kettle
The product of internal every aspect is detected, and the problem that testing result is inaccurate is easy to cause.
Technical solution
It can be convenient for sampling when detecting for realization is above-mentioned, when so as to accurately judge needed for Product formation
Between, while the product of reaction kettle inside every aspect can be extracted, so that the sample of detection is more abundant, improve inspection
The purpose of result accuracy is surveyed, the utility model provides the following technical solutions: a kind of synthesis reaction vessel convenient for sampling, including kettle
Body, the side at the top of the autoclave body is fixedly installed with loading hopper, and the bottom of autoclave body side is fixedly connected with support base, institute
The bottom movable sleeve for stating autoclave body is connected to rotary shaft, and the side of the rotary shaft is fixedly installed with stirring blade, and the bottom of rotary shaft
End is fixedly attached on the output shaft of motor, and the outside of the motor passes through to be fixedly connected at the top of fixed frame and support base,
The side of the autoclave body bottom is fixedly installed with out funnel, and the bottom of the funnel side out is fixedly installed with removable cover,
The side of the removable cover is connect by fixing bolt with the bottom thread of the funnel other side out, the other side at the top of the autoclave body
It is fixedly connected with screw rod, the external activity of the screw rod is socketed with Ka Gai, and the external screw-thread of screw tip is socketed with nut, institute
The bottom for stating Ka Gai is sequentially connected by the other side at the top of movable spring and autoclave body, and the middle part movable sleeve of Ka Gai is connected to drawing
The front of bar, the pull rod is equipped with scale layer, and the external activity of pull rod is socketed with positioning sleeve, the positive side of positioning sleeve
It is threaded with bolt, the bottom of the pull rod is fixedly connected by connection frame with the bottom of sampling box inner cavity, the connection frame
Side be fixedly connected with baffle, the bottom of the baffle is connected with movable plate, and the movable plate is fixedly mounted on sampling
The side of box inner cavity, and the bottom of movable plate is sequentially connected by the inner wall of tension spring and sampling box.
Preferably, the bottom of the autoclave body inner cavity is fixedly connected with inclined plate, and the angle between inclined plate and horizontal direction is three
Ten degree.
Preferably, the fixed frame is by fixing sleeve and two support bar groups at fixing sleeve is fixedly attached to the outside of motor.
Preferably, the screw rod is located at the inside of movable spring, and the interior spiral shell of the external screw thread and nut interior outside screw rod
Line is adapted.
Preferably, the shape of the sampling box is V-arrangement, and sampling box does not contact between autoclave body during exercise.
Preferably, the tension spring is located at the inside of sampling box, and the quantity of tension spring is two, and two tension springs are to connect
Frame is that symmetrical centre is symmetrical.
Beneficial effect
Compared with prior art, the utility model provides a kind of synthesis reaction vessel convenient for sampling, has following beneficial
Effect:
1, should be convenient for synthesis reaction vessel of sampling, by the cooperation of pull rod, sampling box, baffle, movable plate and tension spring, it can be with
During reaction kettle carries out synthetic reaction, convenient for being sampled detection to reaction kettle, so as to be produced by observation synthesis
The progress of object carrys out the time needed for accurately judging Product formation.
2, should convenient for synthesis reaction vessel of sampling, by the cooperation of scale layer and positioning sleeve, can during detection,
The position of sampling box decline is positioned, is extracted so as to the product to reaction kettle inside every aspect, so that sample
The data of this detection are more abundant, and then improve the accuracy of testing result.
Detailed description of the invention
Fig. 1 is the utility model structure front schematic view；
Fig. 2 is the front schematic view of the utility model structure sampling box；
Fig. 3 is enlarged diagram at the utility model structure A；
Fig. 4 is enlarged diagram at the utility model structure B.
In figure: 1, autoclave body；2, loading hopper；3, support base；4, rotary shaft；5, stirring blade；6, motor；7, fixed
Frame；8, go out funnel；9, removable cover；10, fixing bolt；11, screw rod；12, Ka Gai；13, nut；14, movable spring；15, pull rod；
16, scale layer；17, positioning sleeve；18, bolt；19, connection frame；20, sampling box；21, baffle；22, movable plate；23, tension spring.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model
Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole
Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work
Every other embodiment obtained, fall within the protection scope of the utility model.
Fig. 1-4, a kind of synthesis reaction vessel convenient for sampling, including autoclave body 1 are please referred to, the bottom of 1 inner cavity of autoclave body is fixed to be connected
It is connected to inclined plate, the angle between inclined plate and horizontal direction is 30 degree, can be after synthetic reaction, so that synthetic product is suitable
The tilt angle of inclined plate flowed out from funnel 8 out, to accelerate the speed of product flowing, the side at the top of autoclave body 1 is fixed
Loading hopper 2 is installed, and the bottom of 1 side of autoclave body is fixedly connected with support base 3, the bottom movable sleeve of autoclave body 1 is connected to rotation
Shaft 4, the side of rotary shaft 4 is fixedly installed with stirring blade 5, and the bottom end of rotary shaft 4 is fixedly attached to the output shaft of motor 6
On, the outside of the model Y90L-2 of this motor 6, motor 6 are fixedly connected by fixed frame 7 with the top of support base 3, fixed
Frame 7 is by fixing sleeve and two support bar groups at and fixing sleeve is fixedly attached to the outside of motor 6, the mistake that can be operated in motor 6
Cheng Zhong plays the fixed effect of support to motor 6, avoids motor 6 and violent shaking occurs, ensures that motor 6 is transported
The side of stability when turning, 1 bottom of autoclave body is fixedly installed with out funnel 8, and the bottom of 8 side of funnel is fixedly installed with out
The side of removable cover 9, removable cover 9 is connect by fixing bolt 10 with the bottom thread of 8 other side of funnel out, 1 top of autoclave body
The other side is fixedly connected with screw rod 11, and screw rod 11 is located at the inside of movable spring 14, and external screw thread and nut outside screw rod 11
Internal screw thread inside 13 is adapted, and the external activity of screw rod 11 is socketed with card lid 12, and the external screw-thread socket on 11 top of screw rod
There is nut 13, rubber pad is fixedly connected in the middle part of 12 bottom end of card lid, and rubber pad is flexibly connected with the inner wall of autoclave body 1, and right
Autoclave body 1 plays the role of sealing, and the bottom of card lid 12 is sequentially connected by the other side at 1 top of movable spring 14 and autoclave body,
And the middle part movable sleeve of card lid 12 is connected to pull rod 15, the front of pull rod 15 is equipped with scale layer 16, can be right during detection
The position that sampling box 20 declines is positioned, and is extracted so as to the product to reaction kettle inside every aspect, so that sample
The data of this detection are more abundant, and then improve the accuracy of testing result, and the external activity of pull rod 15 is socketed with positioning
Set 17, the positive side of positioning sleeve 17 are threaded with bolt 18, and the bottom of pull rod 15 passes through in connection frame 19 and sampling box 20
The bottom of chamber is fixedly connected, and the shape of sampling box 20 is V-arrangement, and sampling box 20 does not contact between autoclave body 1 during exercise, can be with
During reaction kettle carries out synthetic reaction, convenient for being sampled detection to reaction kettle, so as to be produced by observation synthesis
The progress of object carrys out the time needed for accurately judging Product formation, and the side of connection frame 19 is fixedly connected with baffle 21, baffle 21
Bottom be connected with movable plate 22, movable plate 22 is fixedly mounted on the side of 20 inner cavity of sampling box, and the bottom of movable plate 22
Portion is sequentially connected by the inner wall of tension spring 23 and sampling box 20, and tension spring 23 is located at the inside of sampling box 20, and the quantity of tension spring 23
It is two, two tension springs 23 are that symmetrical centre is symmetrical with connection frame 19.
When work, reaction raw materials is added from loading hopper 2 to autoclave body 1 first, then open motor 6, makes rotary shaft 4
Rotation, and stirring blade 5 is driven to rotate, to be stirred to reaction raw materials, positioning sleeve 17 is then pressed, rotates bolt 18,
To pull rod 15, mobile length is positioned, then pushing drawing rod 15, with going deep into for sampling box 20, when the elastic force of tension spring 23 is less than
It when the weight of product, is separated between movable plate 22 and baffle 21, synthetic product flows into sampling box 20 from gap between the two
In, when the sample in sampling box 20 is filled, movable plate 22 moves up under the elastic force effect of tension spring 23, and connects with movable plate 22
Touching, to completely cut off the inflow of synthetic product, last rotating nuts 13 are allowed to mutually separate between screw rod 11, while card lid 12 exists
The elastic force of movable spring 14 acts on lower automatic spring, then extracts pull rod 15 out, consequently facilitating being sampled.
In conclusion pull rod 15, sampling box 20, baffle 21,22 and of movable plate should be passed through convenient for the synthesis reaction vessel of sampling
The cooperation of tension spring 23, can reaction kettle carry out synthetic reaction during, convenient for being sampled detection to reaction kettle, so as to
To carry out the time needed for accurately judging Product formation by the progress of observation synthetic product；Pass through scale layer 16 and positioning sleeve
17 cooperation, can be during detection, and the position declined to sampling box 20 positions, so as to reaction kettle inside
The product of every aspect extracts, so that the data of pattern detection are more abundant, and then improve the accuracy of testing result,
Solving due to reaction kettle is in the state of an opposing seal during synthetic product, it is difficult to be examined by sampling
The progress of synthetic reaction is surveyed, thus the time needed for can not accurately judging Product formation, and when detecting cannot be to reaction kettle
The product of internal every aspect is detected, and the problem that testing result is inaccurate is easy to cause.
It should be noted that, in this document, relational terms such as first and second and the like are used merely to a reality
Body or operation are distinguished with another entity or operation, are deposited without necessarily requiring or implying between these entities or operation
In any actual relationship or order or sequence.Moreover, the terms "include", "comprise" or its any other variant are intended to
Non-exclusive inclusion, so that the process, method, article or equipment including a series of elements is not only wanted including those
Element, but also including other elements that are not explicitly listed, or further include for this process, method, article or equipment
Intrinsic element.
While there has been shown and described that the embodiments of the present invention, for the ordinary skill in the art,
It is understood that these embodiments can be carried out with a variety of variations in the case where not departing from the principles of the present invention and spirit, repaired
Change, replacement and variant, the scope of the utility model is defined by the appended claims and the equivalents thereof.
Claims (6)
1. a kind of synthesis reaction vessel convenient for sampling, including autoclave body (1), it is characterised in that: the side at the top of the autoclave body (1) is solid
Dingan County is equipped with loading hopper (2), and the bottom of autoclave body (1) side is fixedly connected with support base (3), the bottom of the autoclave body (1)
Portion's movable sleeve is connected to rotary shaft (4), and the side of the rotary shaft (4) is fixedly installed with stirring blade (5), and rotary shaft (4)
Bottom end is fixedly attached on the output shaft of motor (6), and the outside of the motor (6) passes through fixed frame (7) and support base (3)
Top is fixedly connected, and the side of autoclave body (1) bottom is fixedly installed with out funnel (8), described funnel (8) side out
Bottom is fixedly installed with removable cover (9), and the side of the removable cover (9) passes through fixing bolt (10) and funnel (8) other side out
Bottom thread connection, the other side at the top of the autoclave body (1) is fixedly connected with screw rod (11), the screw rod (11) it is external living
It is dynamic to be socketed with Ka Gai (12), and the external screw-thread on screw rod (11) top is socketed with nut (13), the bottom of the Ka Gai (12) is logical
The other side crossed at the top of movable spring (14) and autoclave body (1) is sequentially connected, and the middle part movable sleeve of Ka Gai (12) is connected to pull rod
(15), the front of the pull rod (15) is equipped with scale layer (16), and the external activity of pull rod (15) is socketed with positioning sleeve (17), institute
It states positioning sleeve (17) positive side to be threaded with bolt (18), the bottom of the pull rod (15) passes through connection frame (19) and takes
The bottom of sample box (20) inner cavity is fixedly connected, and the side of the connection frame (19) is fixedly connected with baffle (21), the baffle
(21) bottom is connected with movable plate (22), and the movable plate (22) is fixedly mounted on the side of sampling box (20) inner cavity,
And the bottom of movable plate (22) is sequentially connected by the inner wall of tension spring (23) and sampling box (20).
2. a kind of synthesis reaction vessel convenient for sampling according to claim 1, it is characterised in that: autoclave body (1) inner cavity
Bottom be fixedly connected with inclined plate, the angle between inclined plate and horizontal direction is 30 degree.
3. a kind of synthesis reaction vessel convenient for sampling according to claim 1, it is characterised in that: the fixed frame (7) by
Fixing sleeve and two support bar groups are at fixing sleeve is fixedly attached to the outside of motor (6).
4. a kind of synthesis reaction vessel convenient for sampling according to claim 1, it is characterised in that: the screw rod (11) is located at
The inside of movable spring (14), and the external screw thread of screw rod (11) outside is adapted with the internal screw thread of nut (13) inside.
5. a kind of synthesis reaction vessel convenient for sampling according to claim 1, it is characterised in that: the sampling box (20)
Shape is V-arrangement, and sampling box (20) does not contact between autoclave body (1) during exercise.
6. a kind of synthesis reaction vessel convenient for sampling according to claim 1, it is characterised in that: the tension spring (23) is located at
The inside of sampling box (20), and the quantity of tension spring (23) is two, two tension springs (23) are in symmetrical with connection frame (19)
The heart is symmetrical.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821319219.8U CN208878563U (en) | 2018-08-16 | 2018-08-16 | A kind of synthesis reaction vessel convenient for sampling |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821319219.8U CN208878563U (en) | 2018-08-16 | 2018-08-16 | A kind of synthesis reaction vessel convenient for sampling |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN208878563U true CN208878563U (en) | 2019-05-21 |
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ID=66509052
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201821319219.8U Active CN208878563U (en) | 2018-08-16 | 2018-08-16 | A kind of synthesis reaction vessel convenient for sampling |
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| CN (1) | CN208878563U (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110743477A (en) * | 2019-09-17 | 2020-02-04 | 崔兵 | Chemical industry reation kettle convenient to sample observation |
| CN111632567A (en) * | 2020-06-10 | 2020-09-08 | 永旗农业科技发展(杭州)有限公司 | Disilane reaction kettle |
| CN113884336A (en) * | 2021-10-12 | 2022-01-04 | 北京华能新锐控制技术有限公司 | Hydroelectric power generation rivers sampling system |
-
2018
- 2018-08-16 CN CN201821319219.8U patent/CN208878563U/en active Active
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110743477A (en) * | 2019-09-17 | 2020-02-04 | 崔兵 | Chemical industry reation kettle convenient to sample observation |
| CN111632567A (en) * | 2020-06-10 | 2020-09-08 | 永旗农业科技发展(杭州)有限公司 | Disilane reaction kettle |
| CN113884336A (en) * | 2021-10-12 | 2022-01-04 | 北京华能新锐控制技术有限公司 | Hydroelectric power generation rivers sampling system |
| CN113884336B (en) * | 2021-10-12 | 2024-04-05 | 北京华能新锐控制技术有限公司 | Hydroelectric generation rivers sampling system |
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Address after: 312000 No.19, Weixi Road, Shangyu economic and Technological Development Zone, Hangzhou Bay, Shaoxing City, Zhejiang Province Patentee after: Zhejiang Gepai cobalt industry new material Co.,Ltd. Address before: 312000 No.19, Weixi Road, Shangyu economic and Technological Development Zone, Hangzhou Bay, Shaoxing City, Zhejiang Province Patentee before: GREATPOWER JINCHUAN ADVANCED BATTERY MATERIALS Corp. |