CN208869524U - Glycocyamine produces guarantee system - Google Patents
Glycocyamine produces guarantee system Download PDFInfo
- Publication number
- CN208869524U CN208869524U CN201821630098.9U CN201821630098U CN208869524U CN 208869524 U CN208869524 U CN 208869524U CN 201821630098 U CN201821630098 U CN 201821630098U CN 208869524 U CN208869524 U CN 208869524U
- Authority
- CN
- China
- Prior art keywords
- glycocyamine
- production
- raw material
- reaction
- reaction kettle
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The utility model relates to a kind of glycocyamines to produce guarantee system, for the auxiliary facility of glycocyamine production system, final product quality and product yield for guaranteeing glycocyamine production system is higher, it is characterized in that, the glycocyamine production guarantees that system includes: exclusion device, the higher raw material of purity is obtained for removing the impurity in raw material positioned at the discharge port of each raw material warehouse of glycocyamine production system；Automatic control system is located in control room, carries out auto-control to this system by production requirement specification；Auxiliary device is reacted, is located on glycocyamine production system component, is connected with automatic control system, to realize optimal reaction condition.Glycocyamine disclosed in the utility model produces guarantee system, reduces the production cost of glycocyamine, improves product quality and production efficiency.
Description
Technical field
The utility model relates to chemical production fields, more particularly to a kind of guarantee system of glycocyamine automated production
System.
Background technique
Glycocyamine is also known as glucocyamine (guanidine acetic acid, L) and N- miaow base glycine, molecular formula
C3H7N302, molecular mass 117.11, white foliaceous or acicular crystal are dissolved in water, atomic to be dissolved in ethyl alcohol and ether, guanidine radicals
Acetic acid is separated from the urine of people and dog by weber (weber) earliest, and proposing glycocyamine is creatine
(creatine) precursor substance is metabolic intermediate and is discharged by urine.
In current glycocyamine production system, the main production raw material of glycocyamine, such as sweet ammonia are mainly utilized
Acid, cyanamide, process water (or mother liquor) etc. are manufactured by reacting in a reaction unit using chemical technology
Method.The production key point of glycocyamine: first is that yield is to require yield as high as possible；Second is that high quality, guanidine radicals in product
The content of acetic acid, water content, dicyandiamide, melamine content will control within good critical field.
But in existing system production, due to the problem of some raw materials or production operation program etc., often it will lead to
The output capacity for producing resulting glycocyamine finished product is low, while also not getting a desired effect in quality, and there are also very big
Improvements.
Utility model content
The technical problems to be solved in the utility model is the output capacity for solving to improve glycocyamine production system, and is improved
The problems such as quality of output finished product.
In order to solve the above-mentioned technical problem, the utility model provides a kind of glycocyamine production guarantee system, it can
The output capacity of glycocyamine production system is improved, and improves the quality of output finished product.
A kind of glycocyamine disclosed in the utility model produces guarantee system, it is the mating of glycocyamine production system
Facility, final product quality and the product yield for guaranteeing glycocyamine production system are higher, which is characterized in that the guanidine radicals second
Acid production guarantees that system includes: exclusion device, positioned at the discharge port of each raw material warehouse of glycocyamine production system, for removing original
Impurity in material obtains the higher raw material of purity；Automatic control system is located in control room, is to this by production requirement specification
System carries out auto-control；Auxiliary device is reacted, is located on glycocyamine production system component, is connected with automatic control system, with
Realize optimal reaction condition.
Preferably, the exclusion device includes: filter, positioned at the feed inlet of cyanamide reserve tank, to filter removal
A small amount of impurity in raw material；Except iron instrument, it is located at charging bin discharge port external, to remove the metal impurities that may be carried secretly in raw material；Vibration
Dynamic sieve is located at charging bin discharge port external, to screen out the other impurities of possible entrainment in raw material.
Preferably, the glycocyamine production guarantees that system further includes the process water addition channel on reaction kettle and leads to
It is deionized water in road.
Preferably, the reaction auxiliary device includes: peristaltic pump, positioned at the discharge port of cyanamide reserve tank, to original
The discharging speed of material list cyanamide is controlled；Agitating paddle is located inside reaction kettle, to be stirred to reaction raw materials；Control
Valve, positioned at the outlet or entrance of each component of production system, the opening degree to control each component opening is controlled.
Preferably, the peristaltic pump is connected with automatic control system, is carried out by revolution of the automatic control system to peristaltic pump
Automatic adjustment.
Preferably, the control valve further include: exhaust, return valve, positioned at the top of reaction kettle, to realize reaction kettle
Seal included press operation；Positioned at raw material or the outlet valve of intermediate material warehouse discharge outlet, for controlling raw material or intermediate material
Additional amount or speed is added, and be connected with automatic control system, accurate material proportion；Positioned at reaction kettle cooling coil outlet pipe
On automatic temperature control valve, opened or closed by it to adjust the reaction temperature of reaction kettle, realize optimal reaction temperature.
Preferably, the reaction auxiliary device further includes the temperature measuring set on reaction kettle, and it is anti-to be used to Real-time Feedback
Answer the reaction temperature of kettle.
Have the beneficial effect that yield is increased to 92% from 78% acquired by the utility model；Product quality has obtained very big
It is promoted, it is comprehensively superior；Glycocyamine one ton of product of every production before transformation will be discharged nearly 2 cubes of sewage, and transformation post mother liquor is whole
Recycling, has been truly realized zero-emission；Production intensity mitigates significantly；Personnel, power, raw material etc. consumption are all reduced,
Utilization rate of equipment and installations is improved, thus production cost is also with reduction.
It is all greatly improved from economic benefit, social benefit.
Detailed description of the invention
By referring to the drawings to the description of the utility model embodiment, above-mentioned and other mesh of the utility model
, feature and advantage will be apparent from.
Fig. 1 shows the overall structure diagram of glycocyamine production system in the present embodiment；
Fig. 2 shows the structural block diagrams of glycocyamine production guarantee system in the utility model embodiment；
Fig. 3 shows the structure chart of reaction kettle in glycocyamine production system in the present embodiment；
Specific embodiment
Hereinafter reference will be made to the drawings is more fully described the utility model.In various figures, identical element is using similar
Appended drawing reference indicate.For the sake of clarity, the various pieces in attached drawing are not necessarily to scale.In addition, may in figure
Certain well known parts are not shown.
Many specific details of the utility model, such as the structure of device, material, size, place are described hereinafter
Science and engineering skill and technology, to be more clearly understood that the utility model.But just as the skilled person will understand,
The utility model can not be realized according to these specific details.
In the following, the utility model is described in detail referring to attached drawing.
Fig. 1 shows the overall structure diagram of glycocyamine production system in the present embodiment.
As shown in Figure 1, glycocyamine production system include cyanamide reserve tank 10, it is feeding chamber 30, glycine feed bin 60, anti-
Kettle 70, filter 80, mother liquor vacuum colletor 90, mother liquor tank 100, drier 110, packaging feed bin 120 are answered, the production is located at
The multiple control valves (Control valve) and control room 1300 of import and/or the outlet of the multiple components of system.
Fig. 2 shows the structural block diagrams of glycocyamine production guarantee system in the utility model embodiment.
This guarantee system is in the improved auxiliary facility of the entire production system of glycocyamine.
As shown in Fig. 2, glycocyamine disclosed in the utility model production guarantee system specifically include that exclusion device 40,
Automatic control system 1301 and some reaction auxiliary devices.Wherein, the exclusion device 40 is located at each raw material cabin of production system
The discharge port of room mainly carries out impurity to the required raw material of production glycocyamine and the operation such as filters out, makes to obtain as far as possible
The higher reaction raw materials of purity, it mainly includes filter 4001, except iron instrument 4002 and vibrating screen 4003, the filter
4001 are mainly filtered raw material cyanamide, remove a small amount of impurity therein；It is described to remove iron instrument 4002 and vibrating screen
4003 mainly in raw foods glycine metal impurities and other impurity reject.To realize the pure of reaction raw materials
Purification, obtains the high quality of final output finished product.The automatic control system 1301 is located in control room, is mainly basis
Production requirement and other production operation specifications carry out automatically controlling the devices such as the control valve, peristaltic pump 310, so that production system
Each component of system can meet optimal production requirement.The reaction auxiliary device includes peristaltic pump 310, agitating paddle 7005, control
The components such as valve processed, mainly reaction condition when reacted in a kettle raw material carry out real-time monitoring, while when to reaction
The materials and charging rate of required reaction raw materials are controlled, and are connected and are cooperated with each other with automatic control system, most
Enable reaction to reach optimal reaction when carrying out eventually and reach scheduled optimum material proportion and optimal reaction condition,
Improve output final product quality.To reach optimal degree, material loss is reduced, output capacity and output quality are improved.
Fig. 3 shows the structure chart of reaction kettle in glycocyamine production system in the present embodiment.
As shown in figure 3, the reaction kettle 70 includes: feed inlet 7001, discharge port 7006, exhaust, refluxing opening 7007, temperature
Sensor 7004, cooling coil 7002, stirring motor 7003 and agitating paddle 7005.Wherein, the feed inlet 7001 and
Exhaust, refluxing opening 7007 are located at the top of reaction kettle 70, and discharge port 7006 is located at the lower part of reaction kettle 70, and the temperature passes
Sensor 7004, cooling coil 7002 and agitating paddle 7005 are then located at the inside of reaction kettle 70, and the cooling coil 7002
One end is connected with the top of reaction kettle 70, while one end of the agitating paddle 7005 passes through the upper wall of reaction kettle and reacts with being located at
The stirring motor 7003 on the top of kettle is connected, and the other end is vacantly in reaction kettle 70.Wherein, the stirring motor 7003 with
Automatic control system is connected, optimal come the mixing speed for controlling agitating paddle with this.
To produce glycocyamine disclosed in the utility model below with reference to Fig. 1, Fig. 2 and Fig. 3 and guarantees system embodiment
Working condition do some simple introductions.
The production key point of glycocyamine: first is that yield is to require yield as high as possible；Second is that high quality.Guanidine in product
The content of guanidine-acetic acid, water content, dicyandiamide, melamine content will control within good critical field.Therefore,
For reach most critical the above two o'clock key request we from the following aspects set about being improved.
First we starts in terms of raw material to be introduced.It on the one hand is to select purer high-quality content of starting materials,
Concrete condition is given an account of continue as follows:
(1) raw material cyanamide is to apply the product of high concentration, high-purity, and to pass through filter before use using
4001 filtering, to remove a small amount of impurity wherein having；
(2) raw material glycine can use food glycine.Its before production system is added with remove iron instrument 4002 removal wherein
The metal impurities that may be carried secretly, and the other impurity that may be carried secretly are sifted out with vibrating screen 4003；
(3) when in addition in production system needing to use process water, this reality in process water (or mother liquor) addition channel 721
With novel using deionized water, purity is higher.
Wherein, described except iron instrument 4002 and the vibrating screen 4003 are located on the 30 lower section discharge port 301 of feeding chamber；Institute
Filter 4001 is stated to be located on the feed opening 102 of 10 top of cyanamide reserve tank.
On the other hand, it raw material accurately to match, improves product quality, reduce unnecessary material loss, improve yield.
Concrete condition is given an account of continue as follows:
(1) it conscientiously checks the situation in reaction kettle 70, observes either with or without remnants or the material leaked into, confirmation is in standby
Use state；The quality for the mother liquor that inspection amount will be added: whether clear, whether there is or not solid impurities.Then mother liquor tank liquid level is verified
It counts original scale and calculates termination scale, the number for the pipeline meter being added on pipe with mother liquor is verified, after confirmation is errorless
Start to add food glycine；
(2) inventory is conscientiously verified before raw foods glycine feeds intake, strictly 2/3 amount investment kettle makees bottom material as required,
1/3 is used as feed supplement；
(3) after cyanamide holding vessel 10 is added in raw material cyanamide, the revolution of peristaltic pump 310 is adjusted, verify additional amount and is added
Expect speed.
The quality assurance of the above, raw material is optimal, the big raw material of the three of addition: glycine, cyanamide, process water are (or female
Liquid) accurately metered it ensure that the optimum proportionings of three big materials.This process can carry out operation tune by automatic control system
Control, i.e., by automatic control system to the first outlet valve 601, the second outlet valve 101, peristaltic pump 310 and work in production system
Skill water (or mother liquor) adds the automatic control of pipeline 721, realizes the accurate proportion that the raw material of reaction is participated in when reaction.Certainly,
Personnel's cooperation can also separately be added when necessary.
Secondly, being exactly the raw operating instruction of strict implement in production system work, i.e., by automatic control system to anti-
It answers auxiliary device to be controlled, obtains optimal reaction condition.
Its primary operational process is as described below:
(1) pass through automatic control system 1301 to the automatic control of temperature control valve (TCV) 701 so that in a kettle, starting to add
Add temperature when cyanamide appropriate than optimal reaction temperature lower, the medium temperature in reacting kettle jacketing is than optimum response temperature
Slightly higher 5 DEG C or so are spent, jacket temperature can be 5 DEG C lower than optimal reaction temperature or so when reaction starts, and can guarantee to react in this way
Temperature plateau.This process can be by；
(2) charging rate of peristaltic pump 310 is adjusted by automatic control system 1301, it is ensured that when feed time and reaction
Between it is errorless；
(3) reaction kettle 70, exhaust, return valve 731, the first outlet valve 601, second are gone out by automatic control system 1301
Expect that the closure control of valve 101, third outlet valve 711, temperature control valve 701 etc., the sealing for realizing reaction kettle carry press operation,
Reduce the significant loss for participating in reaction.
(4) 7005 revolving speed of agitating paddle is adjusted by best mixing speed by automatic control system 1301, guarantees the grain of product
Degree and yield；
(5) automatic regulating valve 701 on 7002 outlet pipe of cooling coil is opened, temperature of reaction kettle sensor 7004 can be temperature
Situation feedback is spent to control system, valve 701 is then automatically opened or closed according to temperature fluctuation situation, to stablize reaction kettle
Reaction temperature；
(6) by regulation of the automatic control system 1301 to raw material glycine feeding quantity, produce glycine bottom material as expected
3% or so amount add crystal seed, may make that product crystal grain is big, free-running property is good, in this way to improve crystal form and the increasing of product
The granularity of crystallization；
It (7), can be by automatic control system 1301 to the automatic reality of the first outlet valve 601 in order to which the concentration of reaction mass is steady
When regulate and control, reaction raw materials glycine can be made to divide bottom material and feed supplement that system is added, the mother liquor amount for dissolving bottom material in this way can be reduced,
Feed supplement glycine is added when rear reaction raw materials glycine concentration becomes smaller and reacts slack-off to a certain extent in reaction simultaneously, so not only
Reaction solution concentration is high and reaction speed can also have a certain upgrade.Feed supplement glycine does not have to additionally at this time plus mother liquor keeps system
System water balance.
In addition, using special agitating paddle in glycocyamine disclosed in the utility model production guarantee system, it is
The mixing collision of reaction solution creates condition, and reaction speed is fast, and reaction is thorough；
Ensure that mother liquor keeps pure and namely ensures that mother liquor smoothly recycles simultaneously, ensure that environmentally friendly production, also guarantee
The unreacted raw material in mother liquor is made full use of, yield is improved.
This namely glycocyamine production keeps high yield, low consumption, safe and environment-friendly important key.
Guarantee system is produced using glycocyamine disclosed in the utility model, the beneficial effect that can achieve includes:
1, yield is increased to 92% from 78%；
2, product quality has obtained very big promotion, comprehensively superior；
3, glycocyamine one ton of product of every production before transformation will be discharged nearly 2 cubes of sewage, and transformation post mother liquor all recycles,
It has been truly realized zero-emission；
4, production intensity mitigates significantly, and same yield, personnel are reduced；
5, personnel, power, raw material etc. consumption is all reduced, and utilization rate of equipment and installations is improved, thus is produced
Cost is also with reduction.
It is all greatly improved from economic benefit, social benefit.
It should be noted that herein, relational terms such as first and second and the like are used merely to a reality
Body or operation are distinguished with another entity or operation, are deposited without necessarily requiring or implying between these entities or operation
In any actual relationship or order or sequence.Moreover, the terms "include", "comprise" or its any other variant are intended to
Non-exclusive inclusion, so that the process, method, article or equipment including a series of elements is not only wanted including those
Element, but also including other elements that are not explicitly listed, or further include for this process, method, article or equipment
Intrinsic element.In the absence of more restrictions, the element limited by sentence "including a ...", it is not excluded that
There is also other identical elements in process, method, article or equipment including the element.
Finally, it should be noted that obviously, above-described embodiment is merely examples for clearly illustrating the present invention,
And it does not limit the embodiments.For those of ordinary skill in the art, may be used also on the basis of the above description
To make other variations or changes in different ways.There is no necessity and possibility to exhaust all the enbodiments.And thus
Changes and variations that derived from still in the protection scope of the utility model among.
Claims (7)
1. a kind of glycocyamine produces guarantee system, it is the auxiliary facility of glycocyamine production system, for guaranteeing guanidine radicals second
The final product quality and product yield of sour production system are higher,
It is characterized in that, the glycocyamine production guarantees that system includes:
Exclusion device, the discharge port positioned at each raw material warehouse of glycocyamine production system are obtained for removing the impurity in raw material
The higher raw material of purity；
Automatic control system is located in control room, carries out auto-control to this system by production requirement specification；
Auxiliary device is reacted, is located on glycocyamine production system component, is connected with automatic control system, it is optimal anti-to realize
Answer condition.
2. glycocyamine according to claim 1 produces guarantee system, it is characterised in that: the exclusion device includes:
Filter, positioned at the feed inlet of cyanamide reserve tank, to filter a small amount of impurity in removal raw material；
Except iron instrument, it is located at charging bin discharge port external, to remove the metal impurities that may be carried secretly in raw material；
Vibrating screen is located at charging bin discharge port external, to screen out the other impurities that may be carried secretly in raw material.
3. glycocyamine according to claim 1 produces guarantee system, it is characterised in that: the glycocyamine production guarantees
System further includes that the process water on reaction kettle adds in channel and channel as deionized water.
4. glycocyamine according to claim 1 produces guarantee system, it is characterised in that: the reaction auxiliary device packet
It includes:
Peristaltic pump is controlled positioned at the discharge port of cyanamide reserve tank to the discharging speed to raw material cyanamide；
Agitating paddle is located inside reaction kettle, to be stirred to reaction raw materials；
Control valve, positioned at the outlet or entrance of each component of production system, the opening degree to control each component opening is carried out
Control.
5. glycocyamine according to claim 4 produces guarantee system, it is characterised in that: the peristaltic pump and automatic control
System is connected, and is automatically adjusted by revolution of the automatic control system to peristaltic pump.
6. glycocyamine according to claim 4 produces guarantee system, it is characterised in that: the control valve further include:
Exhaust, return valve, positioned at the top of reaction kettle, to realize that the sealing of reaction kettle carries press operation；
Positioned at raw material or the outlet valve of intermediate material warehouse discharge outlet, for controlling the additional amount of raw material or intermediate material or adding
Enter speed, and is connected with automatic control system, accurate material proportion；
Automatic temperature control valve on reaction kettle cooling coil outlet pipe, is opened or closed by it to adjust reaction kettle
Reaction temperature realizes optimal reaction temperature.
7. glycocyamine according to claim 1 produces guarantee system, it is characterised in that: the reaction auxiliary device also wraps
The temperature measuring set being located on reaction kettle is included, for the reaction temperature of Real-time Feedback reaction kettle.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821630098.9U CN208869524U (en) | 2018-10-08 | 2018-10-08 | Glycocyamine produces guarantee system |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821630098.9U CN208869524U (en) | 2018-10-08 | 2018-10-08 | Glycocyamine produces guarantee system |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN208869524U true CN208869524U (en) | 2019-05-17 |
Family
ID=66469592
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201821630098.9U Active CN208869524U (en) | 2018-10-08 | 2018-10-08 | Glycocyamine produces guarantee system |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN208869524U (en) |
-
2018
- 2018-10-08 CN CN201821630098.9U patent/CN208869524U/en active Active
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103693670B (en) | Production method of calcium sulphate dehydrate and production device thereof | |
| CN109599556A (en) | A kind of cell positive material production system | |
| CN104418388A (en) | Process and device for continuous production of superfine cobalt carbonate powder | |
| EP3901178B1 (en) | Corn fiber processing system and wet milled corn starch processing system using same | |
| CN112968164B (en) | Preparation experimental method of lithium battery anode material precursor | |
| CN103145160A (en) | Method for producing alumina by using high-alumina fly ash | |
| CN101434407B (en) | Process for continuously preparing barium titanate powder | |
| US20230312360A1 (en) | Method for continuously producing polyaluminum chloride form aluminum slag | |
| CN208869524U (en) | Glycocyamine produces guarantee system | |
| CN108275729A (en) | A kind of system and method preparing cobalt carbonate | |
| CN101264943B (en) | Water-saving discharge-reducing consume-reducing continuous production device for nickel carbonate | |
| CN103910651B (en) | Iminodiacetonitrile continuous crystallisation technique | |
| US20230158424A1 (en) | METHOD FOR CRYSTALLIZATION OF Beta-AMMONIUM TETRAMOLYBDATE | |
| CN111659153A (en) | Sodium sulfide continuous cooling crystallization system and process thereof | |
| CN209292445U (en) | The device of the continuous sulfate radical of earth solution | |
| CN103382035B (en) | Magnesium sulfate heptahydrate producing process with fully-continuous method | |
| CN216426772U (en) | Device for preparing ammonium chloride by co-production of sodium bicarbonate | |
| CN112251602B (en) | Method and device for preparing mixed rare earth chloride by continuously extracting and converting rare earth sulfate | |
| CN212954949U (en) | Chlorobutane continuous production device | |
| CN211141542U (en) | Production device of food-grade and feed-grade anhydrous magnesium sulfate | |
| CN209602559U (en) | A kind of xylose mother liquid continuous carbonation impurity removing equipment | |
| CN108529906B (en) | Quicklime digestion system and working method thereof | |
| CN209291982U (en) | The device of continuous production crystal carbonated rare earth | |
| CN202876423U (en) | Acid bath flash evaporation and crystallization device | |
| CN110510678A (en) | A kind of preparation method of efficient mixing ternary precursor |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant |