CN208852463U - A kind of diluted acid decolorization adsorption tank - Google Patents

A kind of diluted acid decolorization adsorption tank Download PDF

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Publication number
CN208852463U
CN208852463U CN201821018739.5U CN201821018739U CN208852463U CN 208852463 U CN208852463 U CN 208852463U CN 201821018739 U CN201821018739 U CN 201821018739U CN 208852463 U CN208852463 U CN 208852463U
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China
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plate fins
blade
rotation axis
agitating paddle
autoclave body
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CN201821018739.5U
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Chinese (zh)
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田志高
徐明萍
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Hubei teteng New Material Technology Co.,Ltd.
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Xiangyang Heshun Da Chemical Co Ltd
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Abstract

The utility model provides a kind of diluted acid decolorization adsorption tank, including autoclave body, the kettle cover being detachably connected with autoclave body, agitating device, activated carbon adsorption cylinder is provided in the autoclave body, activated carbon adsorption cylinder upper end is fixed on autoclave body side wall, feed channel is provided on kettle cover, autoclave body lower end is provided with discharging channel, agitating device includes driving motor and agitating paddle, driving motor drives agitating paddle rotation, agitating paddle is provided with top, in, three layers of bottom paddle blade structure, bottom blade is that the plate fins of multi-disc are fixedly connected with rotation axis by disk, plate fins and rotation axis axis are in angle of 45 degrees, the rotation direction of the plate fins of bottom blade is that the retrousse mode of material is arranged, middle layer blade is that upper and lower two pairs of plate fins are interspersed with top layer blade, the plate fins of middle layer blade are that the retrousse mode of material is arranged, agitating paddle is arranged in work In property charcoal absorbing cylinder.

Description

A kind of diluted acid decolorization adsorption tank
Technical field
The utility model relates to a kind of diluted acid decolorization adsorption tanks, decolourize more particularly to a kind of high diluted acid of adsorption efficiency Adsorption tanks belong to chemical equipment technical field.
Background technique
5- nitro o-cresol, yellow or sepia crystalline powder are a kind of important chemical intermediates, in production 5- nitro In the technique of o-cresol, for discarded diluted acid by filtering, decoloration, absorption to recycle, existing absorbent charcoal adsorption tank is usual Active carbon layer without agitating function, and inside adsorption tanks is one layer or multilayer is placed perpendicular to the axis direction of tank body, The material for needing to be adsorbed is spilt from abhiseca portion to active carbon layer.But the surface area that this adsorption tanks material is contacted with active carbon Small, adsorption efficiency is not high, and this adsorption tanks, without agitating function, when absorption has the material of particle, material accumulation exists Agglomeration forms barrier layer on active carbon layer, and postorder material can not cause the reduction of active carbon layer percent of pass by activated carbon adsorption layer, Seriously affect adsorption bleaching effect.Therefore herein on the basis of existing defect, need to study a kind of with agitating function, decoloration suction The diluted acid decolorization adsorption tank that attached effect is good, adsorption efficiency is high.
Summary of the invention
To solve the problems, such as that above-mentioned existing adsorption tanks exist, the utility model provides that a kind of structure is simple, band agitating function , the diluted acid decolorization adsorption tank that decolorization adsorption effect is good, adsorption efficiency is high.
The utility model provides a kind of diluted acid decolorization adsorption tank, including autoclave body, the kettle cover being detachably connected with autoclave body, stirring Device is provided with activated carbon adsorption cylinder in the autoclave body, and activated carbon adsorption cylinder upper end is fixed on autoclave body side wall, is arranged on kettle cover There is feed channel, autoclave body lower end is provided with discharging channel, and agitating device includes driving motor and agitating paddle, and driving motor drives agitating paddle Rotation, agitating paddle be provided with top, in, three layers of bottom paddle blade structure, bottom blade is that plate fins and the rotation axis of multi-disc pass through circle Disk is fixedly connected, plate fins and rotation axis axis in angle of 45 degrees, the rotation direction of the plate fins of bottom blade be by material to The mode turned over is arranged, and middle layer blade is that upper and lower two pairs of plate fins are interspersed with top layer blade, the sheet wing of middle layer blade Piece is that the retrousse mode of material is arranged, and agitating paddle is arranged in activated carbon adsorption cylinder.
Rotation axis is divided into two sections as a further improvement of the utility model, and the lower section of rotation axis is connected with stirring Top layer blade, middle layer blade and the bottom blade of paddle, the upper section of rotation axis are fixedly connected with lower section by rubber coupling.
Rotation axis is threadedly fixedly connected with rubber coupling as a further improvement of the utility model,.
The surface of plate fins contacting material is set as the arcwall face of indent as a further improvement of the utility model,.
Bottom blade is that 6 plate fins and rotation axis are fixed by disk as a further improvement of the utility model, Connection.
Plate fins are integrally formed structures with disk as a further improvement of the utility model,.
Compared with prior art, the utility model has the beneficial effects that:
1, the activated carbon adsorption layer of the utility model is set as tubular, and the activated carbon adsorption layer compared to sheet increases work Property charcoal and material contact area, agitating paddle be arranged in activated carbon adsorption cylinder, in agitating paddle agitator tank material mix, not only Material in activated carbon adsorption cylinder can contact activated carbon adsorption cylinder and carry out adsorption bleaching, and the material outside cylinder also can be in the effect of stirring Lower contact activated carbon adsorption cylinder carries out decolorization adsorption, increases the effect of absorption.
2, material is the material with particle in the activated carbon adsorption cylinder of the utility model, in activated carbon adsorption cylinder under retention Particulate matter will not carry out accumulation agglomeration under the action of agitating paddle on the inside of activated carbon adsorption cylinder, therefore will not reduce active carbon suction The passability and absorption property of attached cylinder improve the decolorization adsorption effect of adsorption tanks.
3, the diluted acid decolorization adsorption tank of the utility model agitating paddle design have top, in, three layers of bottom paddle blade structure, bottom paddle Leaf is that 6 plate fins are fixedly connected with rotation axis by disk, plate fins and rotation axis axis in angle of 45 degrees, bottom paddle The rotation direction of the plate fins of leaf is that the retrousse mode of material is arranged, and the blade of middle layer and top layer is upper and lower two pairs of plate fins It is interspersed, for middle layer blade by material to turning over, top layer blade turns over downwards material, can using this New type agitation paddle structure The material of reaction kettle is carried out to stir up and down to a certain extent, improves material stirring mixability, increases material and work in tank Property charcoal absorbing cylinder 15 contact frequency, improve adsorption efficiency.
4, the rotation axis of the diluted acid decolorization adsorption tank of the utility model is divided into two sections, and the lower section of rotation axis, which is connected with, to be stirred The top layer blade, middle layer blade and bottom blade of paddle are mixed, the upper section of rotation axis is fixedly connected with lower section by rubber coupling, when When agitating paddle rotates, agitating paddle stirs material up and down, and agitating paddle is moved up and down by the reaction force of material, rubber coupling Rubber block can drive agitating paddle to move up and down, and not only reduce harmful reaction force of the material to agitating paddle in a manner of mitigating, And can use and increase the displacement that agitating paddle moves up and down, stirring paddle stirring range is increased, can also be further increased The uniformity of material mixing.
5, the surface of the plate fins contacting material of the agitating paddle of the diluted acid decolorization adsorption tank of the utility model is set as arc Shape face, the blade for preventing one material from directly hitting contact plane rebound along same path, then meet one object in same path Material is then easy rolling and generates bubble, and the rebound of one material in same path contact arcwall face forms different stock angle of attack not Same rebound material, then the impact force of the different rebound material of different stock angles is cancelled out each other, then will not generate bubble, prevent from producing Raw unnecessary by-product.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the diluted acid decolorization adsorption tank of the utility model;
Fig. 2 is the structural schematic diagram of the agitating paddle of the utility model.
In figure: 1, autoclave body;2, kettle cover;3, agitating device;4, feed channel;5, discharging channel;6, driving motor;7, agitating paddle; 8, bottom blade;9, plate fins;10, rotation axis;11, disk;12, middle layer blade;13, top layer blade;14, rubber shaft coupling Device;15, activated carbon adsorption cylinder.
Specific embodiment
Referring to Fig. 1 and Fig. 2, the utility model provides a kind of diluted acid decolorization adsorption tank, including autoclave body 1 and autoclave body 1 are detachably The kettle cover 2 and agitating device 3 of connection are provided with activated carbon adsorption cylinder 15 in autoclave body 1, and 15 upper end of activated carbon adsorption cylinder is fixed on kettle On 1 side wall of body, the mode that clamping can be used in activated carbon adsorption cylinder 15 is detachably mounted on side wall, can also use active carbon The mode of 15 upper end of absorbing cylinder welding is unremovably welded on side wall, and activated carbon adsorption cylinder 15 is opened close to one end of kettle cover 2 Mouth setting, the setting closed at one end close to 1 bottom of autoclave body, activated carbon adsorption cylinder 15 are the shape that active carbon particle is arranged in netted cylinder Formula adopts the active carbon for replacing adsorption saturation in netted cylinder in this way, easy to operate, the service life of equipment is improved, in kettle Feed channel 4 is provided on lid 2,1 lower end of autoclave body is provided with discharging channel 5, and agitating device 3 includes driving motor 6 and agitating paddle 7, drives Dynamic motor 6 drives agitating paddle 7 to rotate, agitating paddle 7 be provided with top, in, three layers of bottom paddle blade structure, bottom blade 8 for multi-disc piece Shape fin 9 and rotation axis 10 are fixedly connected by disk 11, plate fins 9 and 10 axis of rotation axis in angle of 45 degrees, bottom paddle The rotation direction of the plate fins 9 of leaf 8 is that the retrousse mode of material is arranged, and middle layer blade 12 and top layer blade 13 are upper and lower two pairs Plate fins 9 are interspersed, and the plate fins 9 of middle layer blade 12 are that the retrousse mode of material is arranged, top layer blade 13 Plate fins 9 are that the mode for turning over material downwards is arranged, and the material of reaction kettle can be existed using this 7 structure of new type agitation oar It carries out stirring up and down to a certain extent, improves material stirring mixability, increase connecing for material and activated carbon adsorption cylinder 15 in tank Frequency is touched, adsorption efficiency is improved, the agitating paddle 7 is arranged in activated carbon adsorption cylinder 15, the activated carbon adsorption of the utility model Layer is set as tubular, and the activated carbon adsorption layer compared to sheet increases the contact area of active carbon and material, agitating paddle setting In activated carbon adsorption cylinder 15, material is mixed in 7 agitator tank of agitating paddle, and not only the material in activated carbon adsorption cylinder 15 can contact Activated carbon adsorption cylinder 15 carries out adsorption bleaching, and the material outside cylinder can also contact the progress of activated carbon adsorption cylinder 15 under the action of stirring Decolorization adsorption increases the effect of absorption, and material is the material with particle, activity in the activated carbon adsorption cylinder 15 of the utility model Particulate matter in charcoal absorbing cylinder 15 under retention will not carry out accumulation knot under the action of agitating paddle 7 on the inside of activated carbon adsorption cylinder 15 Block, therefore the passability and absorption property of activated carbon adsorption cylinder 15 will not be reduced, improve the decolorization adsorption effect of adsorption tanks.
Rotation axis 10 is divided for two sections as a further improvement of the utility model, and the lower section of rotation axis 10 is connected with Top layer blade 13, middle layer blade 12 and the bottom blade 8 of agitating paddle 7, the upper section and lower section of rotation axis 10 pass through rubber coupling 14 are fixedly connected, and when agitating paddle 7 rotates, agitating paddle 7 stirs material up and down, and agitating paddle 7 is by above and below the reaction force of material Mobile, the rubber block of rubber coupling 14 can drive agitating paddle 7 to move up and down, not only by the anti-work of nocuousness of the material to agitating paddle 7 Firmly reduced in a manner of mitigation, and can use and increase the displacement that agitating paddle 7 moves up and down, increases agitating paddle 7 Range is stirred, the uniformity of material mixing is further increased.
Threadedly fixation connects for rotation axis 10 and rubber coupling 14 as a further improvement of the utility model, It connects.Replacement easy to disassemble.
The surface of 9 contacting material of plate fins is set as the arcwall face of indent as a further improvement of the utility model, The blade for preventing one material from directly hitting contact plane rebounds along same path, then meets one material in same path and then hold Easily rolling generates bubble, and the rebound of one material in same path contact arcwall face forms different anti-of different stock angle of attack Material is played, then the impact force of the different rebound material of different stock angles is cancelled out each other, then will not generate bubble, preventing need not The by-product wanted.
Bottom blade 8 is that 6 plate fins 9 and rotation axis 10 pass through disk as a further improvement of the utility model, 11 are fixedly connected.
Plate fins 9 are integrally formed structures with disk 11 as a further improvement of the utility model,.
A kind of diluted acid decolorization adsorption tank provided by the utility model is described in detail above.It is used herein Specific embodiment is expounded the principles of the present invention and embodiment, and the explanation of above example is only intended to help Understand the method and its core concept of the utility model.It should be pointed out that for those skilled in the art, Under the premise of not departing from the utility model principle, several improvements and modifications can be made to this utility model, these improve and Modification is also fallen into the protection scope of the utility model claims.

Claims (6)

1. a kind of diluted acid decolorization adsorption tank, it is characterised in that: including autoclave body (1), the kettle cover (2) being detachably connected with autoclave body (1) With agitating device (3), the autoclave body (1) is interior to be provided with activated carbon adsorption cylinder (15), and activated carbon adsorption cylinder (15) upper end is solid It is scheduled on autoclave body (1) side wall, is provided on kettle cover (2) feed channel (4), autoclave body (1) lower end is provided with discharging channel (5), stirring dress Setting (3) includes driving motor (6) and agitating paddle (7), and driving motor (6) drives agitating paddle (7) rotation, and agitating paddle (7) is provided with Top, in, three layers of bottom paddle blade structure, bottom blade (8) be multi-disc plate fins (9) and rotation axis (10) by disk (11) consolidate Fixed connection, in angle of 45 degrees, the rotation direction of the plate fins (9) of bottom blade (8) is for plate fins (9) and rotation axis (10) axis The retrousse mode of material is arranged, middle layer blade (12) and top layer blade (13) are that upper and lower two pairs of plate fins (9) are staggeredly divided Cloth, the plate fins (9) of middle layer blade (12) are that the retrousse mode of material is arranged, the plate fins of top layer blade (13) (9) mode to turn over material downwards is arranged, and agitating paddle (7) setting is in activated carbon adsorption cylinder (15).
2. a kind of diluted acid decolorization adsorption tank according to claim 1, it is characterised in that: the rotation axis (10) is divided into up and down Two sections, the lower section of rotation axis (10) is connected with the top layer blade (13), middle layer blade (12) and bottom blade (8) of agitating paddle (7), The upper section of rotation axis (10) is fixedly connected with lower section by rubber coupling (14).
3. a kind of diluted acid decolorization adsorption tank according to claim 2, it is characterised in that: the rotation axis (10) and rubber join Axis device (14) is threadedly fixedly connected.
4. a kind of diluted acid decolorization adsorption tank according to claim 1, it is characterised in that: plate fins (9) contactant The surface of material is set as the arcwall face of indent.
5. a kind of diluted acid decolorization adsorption tank according to claim 1, it is characterised in that: the bottom blade (8) is 6 pieces Shape fin (9) is fixedly connected with rotation axis (10) by disk (11).
6. a kind of diluted acid decolorization adsorption tank according to claim 1, it is characterised in that: the plate fins (9) and disk (11) it is integrally formed structures.
CN201821018739.5U 2018-06-27 2018-06-27 A kind of diluted acid decolorization adsorption tank Active CN208852463U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201821018739.5U CN208852463U (en) 2018-06-27 2018-06-27 A kind of diluted acid decolorization adsorption tank

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201821018739.5U CN208852463U (en) 2018-06-27 2018-06-27 A kind of diluted acid decolorization adsorption tank

Publications (1)

Publication Number Publication Date
CN208852463U true CN208852463U (en) 2019-05-14

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112473182A (en) * 2020-11-10 2021-03-12 湖南创源生物科技有限公司 Sugar liquid decoloration jar convenient to wash
CN115554731A (en) * 2022-10-24 2023-01-03 连云港贵科药业有限公司 Preparation method of gemcitabine

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112473182A (en) * 2020-11-10 2021-03-12 湖南创源生物科技有限公司 Sugar liquid decoloration jar convenient to wash
CN115554731A (en) * 2022-10-24 2023-01-03 连云港贵科药业有限公司 Preparation method of gemcitabine

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Effective date of registration: 20210914

Address after: 441400 No. 10, Leiyan Avenue, Leihe Town, Yicheng city, Xiangyang City, Hubei Province

Patentee after: Hubei teteng New Material Technology Co.,Ltd.

Address before: 441049 No. 20, Tianshun Avenue, Xiangcheng Economic Development Zone, yujiahu Power Plant Road, Xiangcheng District, Xiangyang City, Hubei Province

Patentee before: XIANGYANG HESHUNDA CHEMICAL Co.,Ltd.

TR01 Transfer of patent right