CN208814916U - A kind of system producing high pure sorbitol using chromatographic separation technology - Google Patents
A kind of system producing high pure sorbitol using chromatographic separation technology Download PDFInfo
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- CN208814916U CN208814916U CN201820979912.1U CN201820979912U CN208814916U CN 208814916 U CN208814916 U CN 208814916U CN 201820979912 U CN201820979912 U CN 201820979912U CN 208814916 U CN208814916 U CN 208814916U
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Abstract
The application belongs to the processing technology of sorbierite, specially a kind of system for producing high pure sorbitol using chromatographic separation technology, including pass through the sequentially connected starch size mixing device of pipeline, liquefying plant, saccharification apparatus, deslagging device, decoloration device, ion-exchange device, vaporising device, hydrogenation apparatus, refining plant, chromatographic separation device, mixed bed ion-exchange device, enrichment facility and 99-99.8% high pure sorbitol storage device.
Description
Technical field
The application belongs to the processing technology of sorbierite, specially a kind of to produce high pure sorbitol using chromatographic separation technology
System.
Background technique
D-sorbite has moisture absorption, and water retention has been widely used in food service industry tool, e.g., in chewing gum, candy production
Middle addition can rise a little keeps food soft, improves tissue and reduces the effect of hardening dusting；For being retained in bread, cake
Purpose；It is spoiled in logistics progress for that can be prevented in sweet food and food, moreover it is possible to chelated metal ions；For canned drink and Portugal
In grape wine, it can prevent from drawing food muddiness because of metal ion.
The industrialized production of sorbierite generally has the methods of Starch Hydrolysis, bioconversion, glucose hydrogenation to be made, wherein
Glucose hydrogenation is most common production method, however this technique prepares crystalline glucose first, reaches higher pure
Degree can just produce the crystalline sorbitol for meeting and needing and produce after being dissolved (or after purifying using UF membrane, through evaporating), hydrogenation
Product, the supplementary product onsumptions such as higher, complex technical process that there is production costs, process flow length, water power vapour are higher, production efficiency is low
The problems such as lower.
Summary of the invention
To solve the above-mentioned problems, it is using what chromatographic separation technology produced high pure sorbitol this application provides a kind of
System, the application is realized by following proposal:
A kind of system producing high pure sorbitol using chromatographic separation technology, including pass through the sequentially connected starch tune of pipeline
Sizing device, liquefying plant, saccharification apparatus, deslagging device, decoloration device, ion-exchange device, vaporising device, hydrogenation apparatus, purification dress
It sets, chromatographic separation device, product mixed bed ion-exchange device, product enrichment facility and 99-99.8% high pure sorbitol storage device.
Preferably, the chromatographic separation device includes chromatographic separation device ontology, and the chromatographic separation device is intrinsic
Top is equipped with horizontal upper orchestration, and the intrinsic lower part of chromatographic separation device is equipped with horizontal lower collector, described above to divide
Separation resin is equipped between orchestration and lower collector.
Preferably, the upper distributor and lower collector are detachably cleared up, on the upper distributor and lower collector
Equipped with aperture, aperture is uniformly distributed.
Preferably, the top of the chromatographic separation device ontology is equipped with inlet tube, and bottom is equipped with outlet, inlet tube difference
Be connected with the pipeline of feed pump and intake pump, be equipped on the pipeline of feed pump and intake pump thermometric instrument, pressure gauge and
Regulating valve.
Preferably, the outlet of the chromatographic separation device ontology is equipped with the first branch pipe, the chromatographic separation device sheet
Body inlet tube is equipped with the second branch pipe, and the of first branch pipe of chromatographic separation device ontology and adjacent chromatographic separation device ontology
Two branch pipes are connected by connecting tube, and the connecting tube is equipped with circulating pump, and pump discharge is equipped with stop valve between ontology and different groups
Divide outlet valve.
Preferably, pressure gauge, entire chromatography are equipped on the inlet tube and outlet of the chromatographic separation device ontology
Pipeline between separator ontology is equipped with a thermometric instrument and a flow instrument and a concentration instrument, chromatographic isolation
Each discharge header pipe road of device is equipped with flow instrument, concentration instrument and regulating valve；
Preferably, the chromatographic separation device is connected by pipeline with raffinate storage device, the raffinate storage device
It is connected by pipeline with film condensing device, the film condensing device is connected by pipeline with deployment device, the allotment dress
It sets and is connected by pipeline with mixed bed delicate instruments, the mixed bed delicate instruments are connected by pipeline with enrichment facility, described
Enrichment facility is connected by pipeline with daily use chemicals sorbierite storage device.
The advantages of the application:
1, processing line is short out: the original of 96.5% glucose content is obtained only with common liquefying-saccharifying refining and concentrating means
Feed liquid does not need condensing crystallizing separation (drying) process, and simple process, input cost is low；
2, product quality is high: the present invention uses DX96.5 saccharified liquid to go hydrogenation system response for raw material before hydrogenation, although
By reacting under high-temperature and high-pressure conditions, the final sorbitol content that discharges only reaches 95-96%, but using chromatographic separation technology to miscellaneous
Available sorbitol purity produces after the higher sorb raw polyol of matter carries out purification & isolation for 99.5% or more high pure sorbitol
Product；
3, operating cost is low: high pure sorbitol system is produced using chromatographic separation technology, although joined a large amount of eluting waters,
But these eluting waters mostly into raffinate, are separated again after membrane concentration, can be used for used in chromatograph eluting water；Always
Running body cost is lower than traditional handicraft.
Detailed description of the invention
Fig. 1 is the application structural schematic diagram；
Fig. 2 is chromatographic separation device structural schematic diagram；
Wherein, 1, starch size mixing device, 2, liquefying plant, 3, saccharification apparatus, 4, deslagging device, 5, decoloration device, 6, from
Friendship device, 7, vaporising device, 8, hydrogenation apparatus, 9, refining plant, 10, chromatographic separation device, 11, product mixed bed ion-exchange device,
12, product enrichment facility, 13,99-99.8% high pure sorbitol storage device, 14, raffinate storage device, 15, film condensing device,
16, deployment device, 17, mixed bed refining plant, 18, enrichment facility, 19, daily use chemicals sorbierite storage device.
Specific embodiment
Embodiment 1
A kind of system producing high pure sorbitol using chromatographic separation technology, including pass through the sequentially connected starch tune of pipeline
Sizing device 1, liquefying plant 2, saccharification apparatus 3, deslagging device 4, decoloration device 5, ion-exchange device 6, vaporising device 7, hydrogenation apparatus
8, refining plant 9, chromatographic separation device 10, product mixed bed ion-exchange device 11, product enrichment facility 12 and the high-purity mountain 99-99.8%
Pears alcohol storage device 13.
Embodiment 2
On the basis of embodiment 1, the chromatographic separation device includes chromatographic separation device ontology, the chromatographic isolation dress
Intrinsic top is set equipped with horizontal upper orchestration, the intrinsic lower part of chromatographic separation device is equipped with horizontal lower collection
Device is equipped with separation resin between the upper distributor and lower collector.
Embodiment 3
On the basis of embodiment 2, the upper distributor and lower collector are detachably cleared up, and the upper distributor is under
Aperture is equipped on collector, aperture is uniformly distributed.
Implement 4
On the basis of embodiment 3, the top of the chromatographic separation device ontology is equipped with inlet tube, and bottom is equipped with outlet
Pipe, inlet tube are connected with the pipeline of feed pump and intake pump respectively, are equipped with thermometer on the pipeline of feed pump and intake pump
Table, pressure gauge and regulating valve.
Embodiment 5
On the basis of embodiment 4, the outlet of the chromatographic separation device ontology is equipped with the first branch pipe, the chromatography
Separator ontology inlet tube is equipped with the second branch pipe, and first branch pipe of chromatographic separation device ontology and adjacent chromatographic isolation fill
The second branch pipe for setting ontology is connected by connecting tube, and the connecting tube is equipped with circulating pump, and pump discharge is cut off between being equipped with ontology
Valve and different component outlet valve.
Embodiment 6
On the basis of embodiment 5, Instrument for Pressure is equipped on the inlet tube and outlet of the chromatographic separation device ontology
Table, the pipeline between entire chromatographic separation device ontology are equipped with a thermometric instrument and a flow instrument and a concentration meter
Each discharge header pipe road of table, chromatographic separation device is equipped with flow instrument, concentration instrument and regulating valve；
Embodiment 7
On the basis of embodiment 6, the chromatographic separation device 10 is connected by pipeline with raffinate storage device 14, institute
It states raffinate storage device 14 to be connected by pipeline with film condensing device 15, the film condensing device 15 is filled by pipeline and allotment
It sets 16 to be connected, the deployment device 16 is connected by pipeline with mixed bed refining plant 17, and the mixed bed refining plant 17 is logical
It crosses pipeline to be connected with enrichment facility 18, the enrichment facility 18 is connected by pipeline with daily use chemicals sorbierite storage device 19.
Claims (7)
1. a kind of system for producing high pure sorbitol using chromatographic separation technology, which is characterized in that including successively being connected by pipeline
The starch size mixing device that connects, liquefying plant, saccharification apparatus, deslagging device, decoloration device, ion-exchange device, vaporising device, hydrogenation dress
It sets, the storage of refining plant, chromatographic separation device, product mixed bed ion-exchange device, product enrichment facility and 99-99.8% high pure sorbitol
Cryopreservation device.
2. a kind of system for producing high pure sorbitol using chromatographic separation technology as described in claim 1, which is characterized in that institute
Stating chromatographic separation device includes chromatographic separation device ontology, the intrinsic top of chromatographic separation device be equipped with it is horizontal upper point
Orchestration, the intrinsic lower part of chromatographic separation device are equipped with horizontal lower collector, the upper distributor and lower collector it
Between be equipped with separation resin.
3. a kind of system for producing high pure sorbitol using chromatographic separation technology as claimed in claim 2, which is characterized in that institute
It states distributor and lower collector is detachably cleared up, be equipped with aperture on the upper distributor and lower collector, aperture is uniform
Distribution.
4. a kind of system for producing high pure sorbitol using chromatographic separation technology as claimed in claim 2, which is characterized in that institute
State chromatographic separation device ontology top be equipped with inlet tube, bottom be equipped with outlet, inlet tube respectively with feed pump and intake pump
Pipeline be connected, thermometric instrument, pressure gauge and regulating valve are equipped on the pipeline of feed pump and intake pump.
5. a kind of system for producing high pure sorbitol using chromatographic separation technology as claimed in claim 4, which is characterized in that institute
The outlet for stating chromatographic separation device ontology is equipped with the first branch pipe, and the chromatographic separation device ontology inlet tube is equipped with second
Second branch pipe of branch pipe, first branch pipe of chromatographic separation device ontology and adjacent chromatographic separation device ontology passes through connecting tube phase
Connection, the connecting tube are equipped with circulating pump, and pump discharge is equipped with stop valve and different component outlet valve between ontology.
6. a kind of system for producing high pure sorbitol using chromatographic separation technology as claimed in claim 4, which is characterized in that institute
It states and is equipped with pressure gauge on the inlet tube and outlet of chromatographic separation device ontology, between entire chromatographic separation device ontology
Pipeline is equipped with a thermometric instrument and a flow instrument and a concentration instrument, each discharge header pipe of chromatographic separation device
Road is equipped with flow instrument, concentration instrument and regulating valve.
7. a kind of system for producing high pure sorbitol using chromatographic separation technology as described in claim 1, which is characterized in that institute
It states chromatographic separation device and is connected by pipeline with raffinate storage device, the raffinate storage device is filled by pipeline and film concentration
It sets and is connected, the film condensing device is connected by pipeline with deployment device, and the deployment device passes through pipeline and mixed bed essence
Device processed is connected, and the mixed bed refining plant is connected by pipeline with enrichment facility, the enrichment facility by pipeline with
Daily use chemicals sorbierite storage device is connected.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820979912.1U CN208814916U (en) | 2018-06-25 | 2018-06-25 | A kind of system producing high pure sorbitol using chromatographic separation technology |
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| CN201820979912.1U CN208814916U (en) | 2018-06-25 | 2018-06-25 | A kind of system producing high pure sorbitol using chromatographic separation technology |
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| CN208814916U true CN208814916U (en) | 2019-05-03 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112266319A (en) * | 2020-11-05 | 2021-01-26 | 浙江华康药业股份有限公司 | Method for preparing sorbitol solution by utilizing high fructose syrup chromatography raffinate |
-
2018
- 2018-06-25 CN CN201820979912.1U patent/CN208814916U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112266319A (en) * | 2020-11-05 | 2021-01-26 | 浙江华康药业股份有限公司 | Method for preparing sorbitol solution by utilizing high fructose syrup chromatography raffinate |
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