CN208814897U - A kind of device of sludge water hot filtrate recycling phosphate fertilizer - Google Patents

A kind of device of sludge water hot filtrate recycling phosphate fertilizer Download PDF

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Publication number
CN208814897U
CN208814897U CN201821423226.2U CN201821423226U CN208814897U CN 208814897 U CN208814897 U CN 208814897U CN 201821423226 U CN201821423226 U CN 201821423226U CN 208814897 U CN208814897 U CN 208814897U
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China
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phosphate fertilizer
feed liquid
sludge water
water hot
tank
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CN201821423226.2U
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Inventor
邓舟
吴瑞峰
荀锐
夏洲
陈科宇
金涛
李刚
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DEEPBLUE ENVIRONMENTAL PROTECTION TECHNOLOGIES Co Ltd
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DEEPBLUE ENVIRONMENTAL PROTECTION TECHNOLOGIES Co Ltd
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Abstract

The utility model discloses a kind of device of sludge water hot filtrate recycling phosphate fertilizer, is related to environmental technology field.The device includes sequentially connected buffer cell, reaction member, feed liquid separation reflux unit, product processing unit;Reaction member includes reactor tank, swirl concentrator, cyclone separator;Reactor tank has level-one discharge outlet and secondary discharge port, level-one discharge port is connected to swirl concentrator, secondary discharge port is connected to cyclone separator, swirl concentrator has concentrated solution outlet and purified liquor outlet, concentrated solution outlet has the level-one return pipe of connection reactor tank, and purified liquor outlet is connected to feed liquid separation reflux unit.The utility model passes through the separation concentration of intermediate product and the reflux of heterogeneity material, utilize each component in filtrate, reduce dosing, increase equipment buffer capacity, extend the crystal molding period, efficiency and quality that phosphate fertilizer generates are improved, efficiently phosphorus in sludge water hot filtrate is removed, reduces sewage treatment difficulty and cost.

Description

A kind of device of sludge water hot filtrate recycling phosphate fertilizer
Technical field
The utility model relates to environmental technology field, especially a kind of device of sludge water hot filtrate recycling phosphate fertilizer.
Background technique
Currently, water eutrophication problem is increasingly serious, and phosphorus is the important element for leading to water eutrophication, at sewage It is higher and higher to the attention rate of phosphorus in reason.Phosphorus as non-renewable resources simultaneously, finally have after exploitation, use, consumption 80% with Sanitary sewage discharge, after sewage plant biochemical treatment, phosphorus is largely enriched in sludge concentration tank, anaerobic sludge digestion pond supernatant again Liquid and sludge dewatering filtrate, in the discharge of phosphorus, the phosphorus in sludge occupies bigger ratio.
It is analyzed from global phosphorus storage capacity (rock phosphate), may result in the supply bottleneck of phosphorus, but phosphate fertilizer in the near future Fertilizer Market larger share is occupied, wherein the phosphate fertilizer in West Europe has occupied 80% ratio.It is some without phosphorus ore storage countries, Such as Germany, phosphorus is determined as strategic material, and widely popularize the recycling and reuse of phosphorus.Phosphorus recycling simultaneously has multi-party The economic benefit in face, phosphorus recycling can reduce or avoid adding completely chemical reagent dephosphorization, control guanite in aqueduct wall Fouling improves whole water treatment technology stability, to reduce water factory's operating cost;And therefore increased water factory's daily handling ability And the reduction of chemical reagent dosage (basicity) and aeration quantity, and reduce ammonia nitrogen removal cost;Meanwhile recycling phosphorus production Chemical fertilizer products have economic benefit.To sum up, the subsequent processing and emission problem for solving sludge filtrate are recycled by phosphate fertilizer, are most to accord with Close the joint demand of resource and environment, the best approach to earn a profit simultaneously instantly.
The chemical method that phosphorus recycles in sewage treatment mainly passes through aluminum phosphate (AlPO4), ferric phosphate (FePO4), calcium phosphate [Ca3(PO4)2], guanite) etc. crystal co-precipitation recycling.It cannot function as being sustained using ferric phosphate, aluminum phosphate as the phosphate of representative Fertile raw material, the method as recycling phosphate fertilizer have limitation, the form of general the two later in actual phosphate fertilizer recovery process It is recycled.
Due to sludge filtrate complicated component, frequently result in that crystal is not easily generated, phosphate fertilizer crystalline solid is subtle not easily settled difficult returns It receives, the problems such as crystalline solid easily blocks pipeline, it is inconvenient and be difficult to reach treatment effect, difficulty is caused to subsequent processing, most Cause water outlet not up to standard eventually, results in waste of resources and be lost.
Utility model content
The goal of the invention of the utility model is: in view of the above problems, providing a kind of sludge water hot filtrate recycling The device of phosphate fertilizer, the device can solve the problems, such as that phosphate fertilizer crystal generation particle is small, the rate of recovery is low, is easy to run off, improve phosphate fertilizer crystal Yield and purity, thus improve recycling value;The removal efficiency of phosphorus in sludge water hot filtrate, drop also can be improved simultaneously Low equipment cost.
The technical solution adopted in the utility model is as follows:
A kind of device of sludge water hot filtrate recycling phosphate fertilizer comprising sequentially connected buffer cell, reaction member, feed liquid Separate reflux unit, product processes unit;The reaction member includes reactor tank and the eddy flow concentration for being respectively connected to reactor tank Device and cyclone separator;Reactor tank is provided with level-one discharge port and secondary discharge port, and the level-one discharge port and the second level go out Material mouth is respectively connected to the swirl concentrator and the cyclone separator, and the swirl concentrator is with concentrated solution outlet and clearly Liquid outlet, the concentrated solution outlet are connected with the level-one return pipe for being connected to the reactor tank, and the purified liquor outlet is connected to described Feed liquid separates reflux unit.
A kind of device of sludge water hot filtrate recycling phosphate fertilizer of the utility model, the cyclone separator have solid-phase outlet And liquid-phase outlet, the solid-phase outlet are connected to the product processing unit, the liquid-phase outlet is connected to the feed liquid separation Reflux unit.
By adopting the above-described technical solution, the phosphate fertilizer fine particle generated in reactor tank can be first through level-one discharge port Into swirl concentrator, after eddy flow is concentrated, fine particle is back in reactor tank through level-one return pipe as subsequent reactions Crystal seed effectively facilitates growing up for the crystalline particle of phosphate fertilizer in sludge water hot filtrate, to promote the recycling of phosphate fertilizer.Then material passes through Cyclone separator separates crystalline particle with liquid, the phosphate fertilizer crude product that can be recycled, and is transported to product and adds Work order member is purified, is dried.
A kind of device of sludge water hot filtrate recycling phosphate fertilizer of the utility model, the reaction pot bottom is in conical structure; The reactor tank has been connected to medicament delivery device to put into Dephosphorization reagent thereto.
By adopting the above-described technical solution, convenient for the crystalline particle at recycling reactor tank bottom.It can according to need to reaction Dephosphorization reagent is put into tank, promotes the formation of crystalline particle.
A kind of device of sludge water hot filtrate recycling phosphate fertilizer of the utility model, the feed liquid separation reflux unit includes material Liquid collecting tank, bottom is provided with pan in the feed liquid collecting tank, and pan is funnel-shaped, has big end and small end, big end connection To the side wall of collecting tank, small end is connected to the bottom wall of collecting tank, forms Delta Region collecting pot bottom.
A kind of device of sludge water hot filtrate recycling phosphate fertilizer of the utility model, the feed liquid collecting tank are provided with connection institute The second level return pipe of reactor tank is stated, the second level return pipe is connected to the Delta Region.
By adopting the above-described technical solution, being conducive to fine particle in the clear liquid being collected into feed liquid collecting tank Continued growth passes back into reactor tank as crystal seed in enrichment, and using the crystal of enrichment, further promotes the recycling of phosphate fertilizer.
A kind of device of sludge water hot filtrate recycling phosphate fertilizer of the utility model, the buffer cell includes surge tank, institute It states and is provided with filter screen in surge tank, the filter screen is connected to the buffering top tank structure.
By adopting the above-described technical solution, filter screen can remove the impurity in sludge water hot filtrate, reduce to subsequent The influence of crystallization reaction improves crystal purity.
A kind of device of sludge water hot filtrate recycling phosphate fertilizer of the utility model, further includes pH damper box, the buffering Unit, reaction member, feed liquid separation reflux unit are connected to pH damper box respectively;The buffer cell, reaction member, feed liquid point It is respectively arranged with pH meter and blender from reflux unit, blender is driven by respective variable-frequency motor and rotated.
By adopting the above-described technical solution, stirring motor uses frequency control, dynamic regulation can stir by force as needed Degree;PH meter and pH adjusting agent collective effect, adjustment material pH, stable crystal.PH adjusting agent in different units can it is identical or It is not identical.
In conclusion by adopting the above-described technical solution, the beneficial effects of the utility model are:
The utility model can make full use of filtrate by the separation concentration and the reflux of heterogeneity material of intermediate product Middle each component reduces added amount of chemical, increases the buffer capacity of equipment, increase the crystal molding period, improve phosphate fertilizer The efficiency and quality of generation, can low cost, high yield, significantly remove sludge water hot filtrate middle and high concentration phosphorus, reduce Subsequent sewage treatment difficulty and cost.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the device for the sludge water hot filtrate recycling phosphate fertilizer that utility model provides.
Specific embodiment
With reference to the accompanying drawing, the utility model is described in detail.
In order to make the purpose of the utility model, technical solutions and advantages more clearly understood, below in conjunction with attached drawing and implementation Example, the present invention will be further described in detail.It should be appreciated that specific embodiment described herein is only used to explain The utility model is not used to limit the utility model.
As shown in Figure 1, the present embodiment provides a kind of devices of sludge water hot filtrate recycling phosphate fertilizer comprising sequentially connected Buffer cell 1, reaction member 2, feed liquid separative unit 3 and product process unit 4.
Buffer cell 1 includes surge tank 11, and 11 center of top of surge tank is provided with blender 13, and blender 13 has variable-frequency electric The driving rotation of machine 15, variable-frequency motor 15 are set to the outside of surge tank 11.Surge tank 11 is internally provided with filter screen 17, filter screen 17 are connected to the inner wall of surge tank 11.Surge tank 11 is connected with intermittent feeding pump and carries out intermittent feeding.
Reaction member 2 includes reactor tank 21, swirl concentrator 23 and cyclone separator 25.Swirl concentrator 23 and eddy flow point Reactor tank 21 is connected to from the separation of device 25.21 bottom of reactor tank is in conical structure, from sedimentation and is enriched with conducive to crystalline particle.Instead 21 center of top of tank is answered to be provided with blender 211, blender 211 is driven by variable-frequency motor 213 and rotated, and variable-frequency motor 213 is arranged In the outside of reactor tank 21.Reactor tank 21 is connected with medicament delivery device 215 to put into Dephosphorization reagent thereto, and magnesium can be selected in medicament Salt or calcium salt, such as magnesium chloride, magnesium hydroxide, calcium chloride.
Reactor tank 21 is provided with level-one discharge port and secondary discharge port material outlet, and level-one discharge port is connected to eddy flow concentration Device 23, secondary discharge port are connected to cyclone separator 25.Swirl concentrator 23 has concentrated solution outlet and purified liquor outlet, concentrate Outlet is connected with the level-one return pipe 231 of connection reactor tank 21, and purified liquor outlet is connected to feed liquid separation reflux unit 3.Eddy flow point There is solid-phase outlet and liquid-phase outlet from device, solid-phase outlet is connected to product processing unit 4, and liquid-phase outlet is connected to feed liquid separation Reflux unit 3.
Feed liquid separative unit 3 includes feed liquid collecting tank 31, the purified liquor outlet of feed liquid collecting tank 31 and swirl concentrator 23 and The liquid-phase outlet of cyclone separator is respectively communicated with to receive from material therein.Feed liquid collecting tank center of top is provided with stirring Device 33, blender 33 are driven by variable-frequency motor 35 and are rotated, and variable-frequency motor 35 is set to the outside of reactor tank 21.Feed liquid collecting tank 31 Interior bottom is provided with pan 37, and pan 37 is funnel-shaped, has big end and small end, big end is connected to the side wall of collecting tank 31, small End is connected to the bottom wall of collecting tank 31, forms Delta Region collecting pot bottom.Delta Region is connected with to be connected to reactor tank 21 Second level return pipe 35 the fine crystals being enriched in Delta Region are back to reactor tank 21.
The device of sludge water hot filtrate recycling phosphate fertilizer provided in this embodiment further includes pH damper box 39, and pH damper box 39 is divided Not in surge tank 11, reactor tank 21, the connection of feed liquid collecting tank 31 to be passed through pH adjusting agent thereto.Surge tank 11, reactor tank 21, PH meter (not shown) is respectively arranged in feed liquid collecting tank 31.
It includes sequentially connected washer, drier and product collector (not shown) that product, which processes unit,.Washing Device, drier and product collector are all made of equipment in the prior art, by way of as known to those skilled in the art into Row connection, is no longer repeated herein.
The device of sludge water hot filtrate recycling phosphate fertilizer provided in this embodiment further includes setting on the pipeline for being connected to each equipment Valves at different levels set, and to the control system that these valves carry out automatically controlling, change control system use be linked and packed and Control principle referring to the prior art, is no longer repeated herein.
The above is only the preferred embodiment of the utility model only, is not intended to limit the utility model, all at this Made any modifications, equivalent replacements, and improvements etc., should be included in the utility model within the spirit and principle of utility model Protection scope within.

Claims (7)

1. a kind of device of sludge water hot filtrate recycling phosphate fertilizer, which is characterized in that it includes sequentially connected buffer cell, reaction Unit, feed liquid separation reflux unit, product process unit;The reaction member includes reactor tank and is respectively connected to reactor tank Swirl concentrator and cyclone separator;Reactor tank is provided with level-one discharge port and secondary discharge port, the level-one discharge port and The secondary discharge port is respectively connected to the swirl concentrator and the cyclone separator, and the swirl concentrator has concentration Liquid outlet and purified liquor outlet, the concentrated solution outlet are connected with the level-one return pipe for being connected to the reactor tank, the purified liquor outlet It is connected to the feed liquid separation reflux unit.
2. the device of sludge water hot filtrate recycling phosphate fertilizer according to claim 1, which is characterized in that the cyclone separator With solid-phase outlet and liquid-phase outlet, the solid-phase outlet is connected to the product processing unit, and the liquid-phase outlet is connected to The feed liquid separates reflux unit.
3. the device of sludge water hot filtrate recycling phosphate fertilizer according to claim 2, which is characterized in that the reaction pot bottom In conical structure;The reactor tank has been connected to medicament delivery device to put into Dephosphorization reagent thereto.
4. the device of sludge water hot filtrate recycling phosphate fertilizer according to claim 1, which is characterized in that the feed liquid separates back Flowing unit includes feed liquid collecting tank, and bottom is provided with pan in the feed liquid collecting tank, and pan is funnel-shaped, has big end and small End, big end are connected to the side wall of collecting tank, and small end is connected to the bottom wall of collecting tank, form Delta Region collecting pot bottom.
5. the device of sludge water hot filtrate recycling phosphate fertilizer according to claim 4, which is characterized in that the feed liquid collecting tank It is provided with the second level return pipe for being connected to the reactor tank, the second level return pipe is connected to the Delta Region.
6. the device of sludge water hot filtrate recycling phosphate fertilizer according to any one of claims 1-5, which is characterized in that described Buffer cell includes surge tank, and filter screen is provided in the surge tank, and the filter screen is connected to the buffering top tank structure.
7. the device of sludge water hot filtrate recycling phosphate fertilizer according to claim 6, which is characterized in that it further includes that pH is adjusted Box, the buffer cell, reaction member, feed liquid separation reflux unit are connected to pH damper box respectively;The buffer cell, reaction Unit, feed liquid separation reflux unit are respectively arranged with pH meter and blender, and blender is driven by respective variable-frequency motor and rotated.
CN201821423226.2U 2018-08-31 2018-08-31 A kind of device of sludge water hot filtrate recycling phosphate fertilizer Active CN208814897U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201821423226.2U CN208814897U (en) 2018-08-31 2018-08-31 A kind of device of sludge water hot filtrate recycling phosphate fertilizer

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201821423226.2U CN208814897U (en) 2018-08-31 2018-08-31 A kind of device of sludge water hot filtrate recycling phosphate fertilizer

Publications (1)

Publication Number Publication Date
CN208814897U true CN208814897U (en) 2019-05-03

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201821423226.2U Active CN208814897U (en) 2018-08-31 2018-08-31 A kind of device of sludge water hot filtrate recycling phosphate fertilizer

Country Status (1)

Country Link
CN (1) CN208814897U (en)

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