CN208795653U - A kind of terahertz time-domain spectroscopy system of background and sample signal synchro measure - Google Patents

A kind of terahertz time-domain spectroscopy system of background and sample signal synchro measure Download PDF

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Publication number
CN208795653U
CN208795653U CN201820605681.8U CN201820605681U CN208795653U CN 208795653 U CN208795653 U CN 208795653U CN 201820605681 U CN201820605681 U CN 201820605681U CN 208795653 U CN208795653 U CN 208795653U
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thz
lock
amplifier
detector
background
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CN201820605681.8U
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Chinese (zh)
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徐德
丁宇洁
王艳茹
冉铮惠
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China Engineering Physics Research Institute's Metrology And Measurement Center
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China Engineering Physics Research Institute's Metrology And Measurement Center
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Abstract

The utility model discloses the terahertz time-domain spectroscopy system of a kind of background and sample signal synchro measure, including femto-second laser, chopper, M1 beam splitter, THz transmitter, H1 paraboloidal mirror, N1 reflecting mirror, N2 reflecting mirror, H2 paraboloidal mirror, M2 beam splitter, Postponement module, Q1 THz detector, THz beam splitter, H3 paraboloidal mirror, Q2 THz detector, lock-in amplifier and computer, between Postponement module and computer, between chopper and lock-in amplifier, between Q1 THz detector and lock-in amplifier, between Q2 THz detector and lock-in amplifier, it is connected between lock-in amplifier and computer using data line, rest part is light path part, it is transmitted using free space transmission or fiber coupling.By designing the optical path of synchro measure background signal and sample signal, background fluctuations situation during enabling Terahertz background signal really to reflect sample test eliminates background signal in measurement process and fluctuates influence to measurement result.

Description

A kind of terahertz time-domain spectroscopy system of background and sample signal synchro measure
Technical field
The utility model belongs to Terahertz Technology field, is related to terahertz time-domain spectroscopy measuring technology, especially a kind of back The terahertz time-domain spectroscopy system of scape and sample signal synchro measure, background and sample signal suitable for terahertz time-domain spectroscopy Synchro measure.
Background technique
THz wave refers to electromagnetic wave of the frequency between (0.1 ~ 10) THz, between far infrared and millimeter wave.Too Hertz wave has the excellent characteristics such as good medium penetrability, low ionization energy and coherence, therefore in material science, Information Center The key areas such as, aerospace have broad application prospects.
Terahertz time-domain spectroscopy system is using terahertz time-domain spectroscopic technology measurement specimen material in terahertz wave band light The instrument of spectral property.Terahertz time-domain spectroscopy instrument is widely used in material composition identification, explosive detection, biological test sample And the various fields such as gas-monitoring.
When carrying out sample test using terahertz time-domain spectroscopy instrument, it usually needs when first measuring one that sample is not added Background terahertz signal;Then it is put into sample to be tested in sample optical path, measures sample to be tested in terahertz wave band Terahertz light spectrum signal, two signals, which are divided by, can obtain sample in the transmission or reflection spectral information of terahertz wave band.By It is changed over time in background signal, measuring bias light and the temporal sequencing of signal light leads to sample signal and background signal Compared to when, cannot really reflect background signal when sample test.
Utility model content
The technical problem to be solved by the present invention is to provide when the Terahertz of a kind of background and sample signal synchro measure Domain spectroscopic system designs the optical path of synchro measure background signal and sample signal, can obtain in sample measurement simultaneously Real background signal, eliminating background signal fluctuation bring influences, and obtains the true spectral transmittance signal of sample, and then improve The reliability of terahertz wave band sample measurement.
The technical solution of the utility model is as follows:
A kind of terahertz time-domain spectroscopy system of background and sample signal synchro measure, including femto-second laser, chopper, M1 beam splitter, THz transmitter, H1 paraboloidal mirror, N1 reflecting mirror, N2 reflecting mirror, H2 paraboloidal mirror, M2 beam splitter, Postponement module, Q1 THz detector, THz beam splitter, H3 paraboloidal mirror, Q2 THz detector, lock-in amplifier and computer, Postponement module with Between computer, between chopper and lock-in amplifier, between Q1 THz detector and lock-in amplifier, Q2 THz detector with It is connected between lock-in amplifier, between lock-in amplifier and computer using data line, rest part is light path part, using certainly It is transmitted by space propagation or fiber coupling.
Femtosecond laser is divided into A1 pump light through M1 beam splitter and A2 detects light, and A2 is detected after light passes through Postponement module to be divided through M2 Shu Jing passes to Q2 THz detector all the way, and another way passes to Q1 detector through N1 reflecting mirror and N2 reflecting mirror;A1 pump light It excites THz transmitter to generate THz wave after into THz transmitter, is carried out again by THz beam splitter after H1 paraboloidal mirror collimation Optical path beam splitting, enters Q2THz detector through H3 paraboloidal mirror for sample optical path all the way, and another way is background optical path warp H2 paraboloidal mirror enters Q1 THz detector.
For chopper for being modulated to femtosecond laser and providing reference signal to lock-in amplifier, M1 beam splitter is used for will The femtosecond laser that femtosecond pulse laser issues is divided into pump light and detection light, and THz transmitter is for generating terahertz pulse letter Number, for THz wave to be collimated and focused, N1 reflecting mirror, N2 are anti-for H1 paraboloidal mirror, H2 paraboloidal mirror, H3 paraboloidal mirror Mirror is penetrated for changing optical propagation direction, M2 beam splitter is divided into two beams for that will detect light, and Postponement module prolongs for changing detection light When terahertz pulse signal is scanned, Q1 THz detector, Q2 THz detector for detecting terahertz pulse signal, THz beam splitter is used to for terahertz light being divided into background measurement light and sample measures light, and lock-in amplifier is for acquiring and amplifying too Hertz signal, computer are used for terahertz time-domain spectroscopy signal processing.
Photoconductive antenna can be selected in THz transmitter, is mainly used for generating terahertz emission in the case where femtosecond pulse motivates Wave.ZnTe crystal may be selected in Q1 THz detector, Q2 THz detector, is mainly used for THz wave detection.Postponement module is general For mechanical delayed sweep line, for generating a series of optical path difference.
Particularly, THz beam splitter is mainly used for being split incident THz wave on it.THz beam splitter will enter The THz wave penetrated is divided into transmission THz wave and reflected terahertz hereby wave, and transmission THz wave is for sample under terahertz wave band Transmitted spectrum signal measurement, reflected terahertz hereby wave for background signal measure.The energy by means of the light splitting effect of THz beam splitter Enough synchro measure background signals and sample signal, Terahertz background signal can really reflect the background wave during sample test Emotionally condition.
The effect and benefit of the utility model are:
(1) the terahertz time-domain spectroscopy system, by designing the optical path of synchro measure background signal and sample signal, so that Terahertz background signal can really reflect the background fluctuations situation during sample test;
(2) synchro measure process can be reduced in traditional test methods due to background signal and sample signal measurement process It is asynchronous and cause sample transmission signal measurement inaccurate, the true spectral transmittance signal of sample can be obtained.
Detailed description of the invention
Fig. 1 terahertz time-domain spectroscopy systematic schematic diagram.
In figure: 1 femto-second laser;2 choppers;3 M1 beam splitters;4 THz transmitters;5 H1 paraboloidal mirrors;6 N1 are anti- Penetrate mirror;7 N2 reflecting mirrors;8 H2 paraboloidal mirrors;9 M2 beam splitters;10 Postponement modules;11 Q1 THz detectors;12 THz points Shu Jing;13 H3 paraboloidal mirrors;14 Q2 THz detectors;15 lock-in amplifiers;16 computers.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work Every other embodiment obtained, fall within the protection scope of the utility model.
A kind of terahertz time-domain spectroscopy system, as shown in Figure of description 1, including femto-second laser 1, chopper 2, M1 points Beam mirror 3, THz transmitter 4, H1 paraboloidal mirror 5, N1 reflecting mirror 6, N2 reflecting mirror 7, H2 paraboloidal mirror 8, M2 beam splitter 9, delay mould Block 10, Q1 THz detector 11, THz beam splitter 12, H3 paraboloidal mirror 13, Q2 THz detector 14, lock-in amplifier 15 and meter Calculation machine 16, between Postponement module 10 and computer 16, between chopper 2 and lock-in amplifier 15, Q1 THz detector 11 and lock It is adopted between phase amplifier 15, between Q2 THz detector 14 and lock-in amplifier 15, between lock-in amplifier 15 and computer 16 It is connected with data line, rest part is light path part, is transmitted using free space transmission or fiber coupling.
Femtosecond laser divides through M1 beam splitter 3 detects light for A1 pump light and A2, and A2 detection light passes through after passing through Postponement module 10 9 one tunnel of M2 beam splitter passes to Q2 THz detector 14, and another way passes to Q1 detector through N1 reflecting mirror 6 and N2 reflecting mirror 7 11;A1 pump light enters excitation THz transmitter 4 after THz transmitter 4 and generates THz wave, after the collimation of H1 paraboloidal mirror 5 again by THz beam splitter 12 carries out optical path beam splitting, enters Q2 THz detector 14 through H3 paraboloidal mirror 13 for sample optical path all the way, separately Enter Q1 THz detector 11 through H2 paraboloidal mirror 8 for background optical path all the way.
Embodiment
Terahertz time-domain spectroscopy system operation methods:
A) output power of femto-second laser 1 is monitored using power meter, will be flown according to the requirement of THz transmitter 4 The second output power of laser 1 is adjusted to suitable position;
B) femtosecond laser for exporting femto-second laser 1 is traditionally arranged to be 3kHz by chopper 2, the frequency of chopper 2;
C) it will be divided into two bundles by the femtosecond laser of chopper 2 using M1 beam splitter 3, it is a branch of to be excited as A1 pump light THz transmitter 4 generates terahertz pulse signal, and another Shu Zuowei A2 detection light enters Postponement module 10;
D) terahertz pulse that THz transmitter 4 issues divides through THz beam splitter 12 for transmission THz wave and reflected terahertz hereby Wave, transmission THz wave are measured for sample, and hereby wave measures reflected terahertz for background;
E) THz wave on background optical path and sample optical path is respectively by H2 paraboloidal mirror 8 and H3 paraboloidal mirror It is incident to Q1 THz detector 11 and Q2 THz detector 14 respectively after 13 focusing, the detection light after delayed module 10 is also conllinear Into Q1 THz detector 11 and Q2 THz detector 14;
F) voltage signal that the electricity output port of Q1 THz detector 11 and Q2 THz detector 14 generates is directly connected to To two signal input ports of lock-in amplifier 15;
G) electrical signal of chopper 2 is connected to the reference signal input terminal of lock-in amplifier 15, by copped wave The modulating frequency of device 2 demodulates sampled signal as the reference signal of lock-in amplifier 15;
H) computer 16 controls Postponement module 10 and is moved according to the stepping-in amount of setting, and detection light is made to generate a series of pass The optical path difference of increasing, while controlling lock-in amplifier 15 and the Q1 THz detector 11 and Q2 THz detector 14 of each stepping are exported Electric signal sampled;
I) it is scanned by the step-by-step movement of the entire stroke of Postponement module 10, computer 16 can sample to obtain terahertz pulse Time domain waveform.
Figure of description is only used as the schematic illustration of the system, and actual product structure snd size are designed with inventor and produced Subject to drawing.
Embodiment described above is only that the embodiments of the present invention is described, not to the utility model Conception and scope be defined.Without departing from the design concept of the present utility model, ordinary people in the field is to this reality The all variations and modifications made with novel technical solution, should fall within the protection scope of the present utility model, this is practical new The range of type is indicated by the appended claims rather than the foregoing description, it is intended that containing for the equivalent requirements of the claims will be fallen in All changes in justice and range are embraced therein, and should not treat any reference in the claims as limiting Related claim.

Claims (4)

1. the terahertz time-domain spectroscopy system of a kind of background and sample signal synchro measure, which is characterized in that including femtosecond laser Device (1), chopper (2), M1 beam splitter (3), THz transmitter (4), H1 paraboloidal mirror (5), N1 reflecting mirror (6), N2 reflecting mirror (7), H2 paraboloidal mirror (8), M2 beam splitter (9), Postponement module (10), Q1 THz detector (11), THz beam splitter (12), H3 Paraboloidal mirror (13), Q2 THz detector (14), lock-in amplifier (15) and computer (16), the Postponement module (10) and meter Between calculation machine (16), between chopper (2) and lock-in amplifier (15), Q1 THz detector (11) and lock-in amplifier (15) it Between, between Q2 THz detector (14) and lock-in amplifier (15), number is used between lock-in amplifier (15) and computer (16) It is connected according to line, rest part is light path part, is transmitted using free space transmission or fiber coupling;Femtosecond laser is through the M1 points Shu Jing (3) is divided into A1 pump light and A2 detection light, and A2 detection light passes through Postponement module (10) by M2 beam splitter (9) all the way Q2 THz detector (14) is passed to, another way passes to Q1 detector (11) through N1 reflecting mirror (6) and N2 reflecting mirror (7);Institute State A1 pump light enter THz transmitter (4) excite afterwards THz transmitter (4) generate THz wave, through H1 paraboloidal mirror (5) collimate Optical path beam splitting is carried out by THz beam splitter (12) again afterwards, is visited all the way through H3 paraboloidal mirror (13) into Q2THz for sample optical path It surveys device (14), another way enters Q1 THz detector (11) through H2 paraboloidal mirror (8) for background optical path.
2. the terahertz time-domain spectroscopy system of a kind of background according to claim 1 and sample signal synchro measure, special Sign is: the THz transmitter (4) selects photoconductive antenna, is mainly used for generating Terahertz in the case where femtosecond pulse motivates Radiated wave.
3. the terahertz time-domain spectroscopy system of a kind of background according to claim 1 and sample signal synchro measure, special Sign is: the Q1 THz detector (11), Q2 THz detector (14) select ZnTe crystal, are mainly used for THz wave spy It surveys.
4. the terahertz time-domain spectroscopy system of a kind of background according to claim 1 and sample signal synchro measure, special Sign is: the Postponement module (10) is mechanical delayed sweep line, for generating a series of optical path difference.
CN201820605681.8U 2018-04-26 2018-04-26 A kind of terahertz time-domain spectroscopy system of background and sample signal synchro measure Expired - Fee Related CN208795653U (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108844913A (en) * 2018-04-26 2018-11-20 中国工程物理研究院计量测试中心 A kind of terahertz time-domain spectroscopy system and operating method

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108844913A (en) * 2018-04-26 2018-11-20 中国工程物理研究院计量测试中心 A kind of terahertz time-domain spectroscopy system and operating method

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