CN208742549U - Reaction kettle is used in a kind of synthesis of methallyl alcohol ether - Google Patents
Reaction kettle is used in a kind of synthesis of methallyl alcohol ether Download PDFInfo
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- CN208742549U CN208742549U CN201821085609.3U CN201821085609U CN208742549U CN 208742549 U CN208742549 U CN 208742549U CN 201821085609 U CN201821085609 U CN 201821085609U CN 208742549 U CN208742549 U CN 208742549U
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- reaction kettle
- alcohol ether
- methallyl alcohol
- arc
- upper cover
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Abstract
The utility model discloses a kind of methallyl alcohol ether synthesis reaction kettles, including reaction kettle ontology, arc-shaped upper cover is equipped with above the reaction kettle ontology, infundibulate lower head is equipped with below the reaction kettle ontology, supporting leg is symmetrically arranged with below the infundibulate lower head, stirring motor is equipped with above the arc-shaped upper cover, the agitating shaft through arc-shaped upper cover is connected with below the stirring motor, stirring blade is staggeredly equipped on the agitating shaft, the reaction kettle body outer wall is welded with heating mantle, heat transfer medium is equipped in the heating mantle, heater, temperature sensor and temperature controller.The utility model compared with prior art the advantages of be: it is simple and reasonable, have the function of heating, stirring, self-cleaning and devil liquor recovery etc. simultaneously, manpower can effectively be saved, improve the combined coefficient of methallyl alcohol ether, it is more environmentally friendly, the convenient temperature in the synthesis of methallyl alcohol ether controls, and degree of regulation is high.
Description
Technical field
The utility model relates to chemical industry equipment technology field, in particular to a kind of methallyl alcohol ether synthesis reaction kettles.
Background technique
Reaction kettle is widely used in the fields such as petroleum, chemical industry, rubber, pesticide, dyestuff, medicine, food, and material generally has carbon
Manganese steel, stainless steel, zirconium, nickel-base alloy and other composite materials are set according to the structure that different process conditions demands carries out container
Meter and parameter configuration, design condition, process, inspection and manufacture, examination are needed according to Its Relevant Technology Standards, to realize what technique required
Heating, evaporation, cooling and low high speed mixture response function are also required to use reaction kettle in the synthesis of methallyl alcohol ether, use
When need temperature is controlled, air pressure is adjusted in real time, general reaction kettle is difficult to meet methallyl alcohol ether
Requirement in synthetic work.
Utility model content
The purpose of this utility model is to solve the problems, such as to mention in background technique, provides a kind of methallyl alcohol ether synthesis use
Reaction kettle.
In order to solve the above technical problems, technical solution provided by the utility model are as follows: a kind of methallyl alcohol ether synthesis use
Reaction kettle, including reaction kettle ontology, the reaction kettle ontology top are equipped with arc-shaped upper cover, set below the reaction kettle ontology
There is infundibulate lower head, supporting leg is symmetrically arranged with below the infundibulate lower head, is equipped with above the arc-shaped upper cover
Stirring motor, the stirring motor lower section are connected with the agitating shaft through arc-shaped upper cover, and the agitating shaft is separate
The end of the stirring motor is protruded into the infundibulate lower head, and stirring blade, institute are staggeredly equipped on the agitating shaft
The reaction kettle body outer wall stated is welded with heating mantle, be equipped in the heating mantle heat transfer medium, heater, temperature sensor and
The signal input part of temperature controller, the temperature controller is connected with temperature sensor, the control signal of the heater
Be connected with the temperature controller, the heating temperature value that the temperature controller is acquired according to temperature sensor come control it is described plus
The work of hot device, the arc-shaped upper cover of the stirring motor two sides is equipped with feed inlet, nitrogen inlet duct and escape pipe, described
Feed inlet cooperation be equipped with feed cap, the nitrogen inlet duct be equipped with nitrogen intake valve, the escape pipe be equipped with
Air valve, the reaction kettle ontology are connected with air gauge, and the infundibulate lower head bottom is equipped with drainage conduit, the row
Rewinding case is equipped with below expects pipe, the drainage conduit is equipped with blow-off valve, and the reaction kettle ontology ethylene oxide feed pipe connects
Be equipped with ethylene oxide measuring tank, the ethylene oxide measuring tank is located above the heating mantle, the ethylene oxide into
Expects pipe is equipped with ethylene oxide inlet valve.
As a preferred embodiment, the reaction kettle ontology between the arc-shaped upper cover and heating mantle is equipped with cleaning
Pump.
As a preferred embodiment, the heating mantle is equipped with symmetrical carrying handle.
As a preferred embodiment, the rewinding case is equipped with scale.
As a preferred embodiment, the supporting leg is welded below the infundibulate lower head, is in external-open shape.
As a preferred embodiment, heating temperature has can be preset in the temperature controller.
The utility model compared with prior art the advantages of be: simple and reasonable, reaction kettle has heating simultaneously, stirs
It mixes, the functions such as self-cleaning and devil liquor recovery, can effectively save manpower, improve the combined coefficient of methallyl alcohol ether, more ring
It protects, the air in reaction kettle can be replaced using nitrogen when use, reduce influence synthesize to methallyl alcohol ether, it is warm
The convenient temperature in the synthesis of methallyl alcohol ether of the cooperation of degree sensor, temperature controller and heater controls, and adjusts
Precision is high.
Detailed description of the invention
Fig. 1 is a kind of structural schematic diagram of methallyl alcohol ether synthesis reaction kettle of the utility model.
It is as shown in the figure: 1, reaction kettle ontology, 2, arc-shaped upper cover, 3, infundibulate lower head, 4, supporting leg, 5, stirring electricity
Machine, 6, agitating shaft, 7, stirring blade, 8, heating mantle, 9, heater, 10, temperature sensor, 11, temperature controller, 12, charging
Mouthful, 13, nitrogen inlet duct, 14, escape pipe, 15, feed cap, 16, nitrogen intake valve, 17, air outlet valve, 18, air gauge, 19, row
Expects pipe, 20, rewinding case, 21, blow-off valve, 22, ethylene oxide measuring tank, 23, ethylene oxide feed pipe, 24, ethylene oxide charging
Valve, 25, cleaning pump, 26, carrying handle.
Specific embodiment
The following describes the utility model in further detail with reference to the accompanying drawings.
In conjunction with attached drawing, a kind of synthesis of methallyl alcohol ether reaction kettle, including reaction kettle ontology 1, the reaction kettle ontology 1
Top is equipped with arc-shaped upper cover 2, is equipped with infundibulate lower head 3, the infundibulate lower head below the reaction kettle ontology 1
3 lower sections are symmetrically arranged with supporting leg 4, and stirring motor 5 is equipped with above the arc-shaped upper cover 2, is connected below the stirring motor 5
It is equipped with the agitating shaft 6 through arc-shaped upper cover 2, the agitating shaft 6 protrudes into described far from the end of the stirring motor 5
Infundibulate lower head 3 in, stirring blade 7, described 1 outer wall of the reaction kettle ontology welding are staggeredly equipped on the agitating shaft 6
There is heating mantle 8, heat transfer medium, heater 9, temperature sensor 10 and temperature controller 11 are equipped in the heating mantle 8, it is described
The signal input part of temperature controller 11 is connected with temperature sensor 10, the control signal and the temperature of the heater 9
Controller 11 is connected, and the temperature controller 11 controls the heater according to the heating temperature value that temperature sensor 10 acquires
The arc-shaped upper cover 2 of 9 work, 5 two sides of stirring motor is equipped with feed inlet 12, nitrogen inlet duct 13 and escape pipe
14, the cooperation of feed inlet 12 is equipped with feed cap 15, and the nitrogen inlet duct 13 is equipped with nitrogen intake valve 16, described
Escape pipe 14 is equipped with air outlet valve 17, and the reaction kettle ontology 1 is connected with air gauge 18, the infundibulate lower head 3
Bottom is equipped with drainage conduit 19, and rewinding case 20 is equipped with below the drainage conduit 19, and the drainage conduit 19 is equipped with blow-off valve 21,
The 1 ethylene oxide feed pipe 23 of reaction kettle ontology is connected with ethylene oxide measuring tank 22, the ethylene oxide metering
Tank 22 is located at 8 top of heating mantle, and the ethylene oxide feed pipe 23 is equipped with ethylene oxide inlet valve 24.
Reaction kettle ontology 1 between the arc-shaped upper cover 2 and heating mantle 8 is equipped with cleaning pump 25.
The heating mantle 8 is equipped with symmetrical carrying handle 26.
The rewinding case 20 is equipped with scale.
The supporting leg 4 is welded on 3 lower section of infundibulate lower head, is in external-open shape.
Heating temperature has can be preset in the temperature controller 11.
The utility model in the specific implementation, opens nitrogen intake valve, first uses the air of nitrogen metathesis reactor, closes nitrogen
Gas intake valve opens feed cap, and the pure and mild catalyst of methallyl is added into feed inlet, reacts then at being replaced at room temperature with nitrogen
Air in kettle is opened stirring motor and is stirred, and temperature controller control heater is heated to the reaction temperature of setting,
Ethylene oxide measuring tank is opened, the desired amount of ethylene oxide gas is passed through, adjusts nitrogen intake valve and air outlet valve for system pressure
Control is setting value, maintains the reaction temperature slaking reaction of setting, until reaching the reaction time of setting terminates polymerization reaction.
The utility model and embodiments thereof are described above, this description is no restricted, shown in attached drawing
Be also one of the embodiments of the present invention, actual structure is not limited to this.All in all if this field
Those of ordinary skill is enlightened by it, without deviating from the purpose of the present invention, not inventively design with
The similar frame mode of the technical solution and embodiment, all should belong to the protection range of the utility model.
Claims (6)
1. a kind of synthesis of methallyl alcohol ether reaction kettle, including reaction kettle ontology (1), it is characterised in that: the reaction kettle sheet
Arc-shaped upper cover (2) are equipped with above body (1), are equipped with infundibulate lower head (3) below the reaction kettle ontology (1), it is described
It is symmetrically arranged with supporting leg (4) below infundibulate lower head (3), is equipped with stirring motor (5) above the arc-shaped upper cover (2),
The agitating shaft (6) through arc-shaped upper cover (2) is connected with below the stirring motor (5), the agitating shaft (6) is remote
End from the stirring motor (5) is protruded into the infundibulate lower head (3), is staggeredly equipped on the agitating shaft (6)
Stirring blade (7), described reaction kettle ontology (1) outer wall are welded with heating mantle (8), and heat transfer is equipped in the heating mantle (8)
Medium, heater (9), temperature sensor (10) and temperature controller (11), the signal input part of the temperature controller (11)
It is connected with temperature sensor (10), the control signal of the heater (9) is connected with the temperature controller (11), the temperature
Degree controller (11) controls the work of the heater (9) according to the heating temperature value that temperature sensor (10) acquires, described
The arc-shaped upper cover (2) of stirring motor (5) two sides is equipped with feed inlet (12), nitrogen inlet duct (13) and escape pipe (14),
Feed inlet (12) cooperation is equipped with feed cap (15), and the nitrogen inlet duct (13) is equipped with nitrogen intake valve (16),
The escape pipe (14) is equipped with air outlet valve (17), and the reaction kettle ontology (1) is connected with air gauge (18), described
Infundibulate lower head (3) bottom is equipped with drainage conduit (19), is equipped with rewinding case (20) below the drainage conduit (19), the row
Expects pipe (19) is equipped with blow-off valve (21), and reaction kettle ontology (1) the ethylene oxide feed pipe (23) is connected with epoxy second
Alkane measuring tank (22), the ethylene oxide measuring tank (22) are located above the heating mantle (8), the ethylene oxide charging
It manages (23) and is equipped with ethylene oxide inlet valve (24).
2. a kind of methallyl alcohol ether synthesis reaction kettle according to claim 1, it is characterised in that: described is arc-shaped
Reaction kettle ontology (1) between upper cover (2) and heating mantle (8) is equipped with cleaning pump (25).
3. a kind of methallyl alcohol ether synthesis reaction kettle according to claim 1, it is characterised in that: the heating mantle
(8) symmetrical carrying handle (26) are equipped with.
4. a kind of methallyl alcohol ether synthesis reaction kettle according to claim 1, it is characterised in that: the rewinding case
(20) it is equipped with scale.
5. a kind of methallyl alcohol ether synthesis reaction kettle according to claim 1, it is characterised in that: the supporting leg
(4) it is welded below the infundibulate lower head (3), is in external-open shape.
6. a kind of methallyl alcohol ether synthesis reaction kettle according to claim 1, it is characterised in that: the temperature control
Heating temperature has can be preset in device (11) processed.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821085609.3U CN208742549U (en) | 2018-07-10 | 2018-07-10 | Reaction kettle is used in a kind of synthesis of methallyl alcohol ether |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821085609.3U CN208742549U (en) | 2018-07-10 | 2018-07-10 | Reaction kettle is used in a kind of synthesis of methallyl alcohol ether |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN208742549U true CN208742549U (en) | 2019-04-16 |
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ID=66055670
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201821085609.3U Active CN208742549U (en) | 2018-07-10 | 2018-07-10 | Reaction kettle is used in a kind of synthesis of methallyl alcohol ether |
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| CN (1) | CN208742549U (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112175347A (en) * | 2020-08-20 | 2021-01-05 | 宁波聚泰源高分子材料有限公司 | High-performance composite modified material and preparation process thereof |
| CN114700015A (en) * | 2022-03-29 | 2022-07-05 | 江苏托球农化股份有限公司 | A device for prothioconazole green production |
| CN114700014A (en) * | 2022-03-29 | 2022-07-05 | 江苏托球农化股份有限公司 | Reation kettle is used in prothioconazole production |
-
2018
- 2018-07-10 CN CN201821085609.3U patent/CN208742549U/en active Active
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112175347A (en) * | 2020-08-20 | 2021-01-05 | 宁波聚泰源高分子材料有限公司 | High-performance composite modified material and preparation process thereof |
| CN114700015A (en) * | 2022-03-29 | 2022-07-05 | 江苏托球农化股份有限公司 | A device for prothioconazole green production |
| CN114700014A (en) * | 2022-03-29 | 2022-07-05 | 江苏托球农化股份有限公司 | Reation kettle is used in prothioconazole production |
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| GR01 | Patent grant | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of utility model: A reaction kettle for the synthesis of methyl allyl alcohol ether Effective date of registration: 20230927 Granted publication date: 20190416 Pledgee: Finance and finance of Fushun Company limited by guarantee Pledgor: FUSHUN XIU LIN CHEMICAL CO.,LTD. Registration number: Y2023210000246 |