CN208705293U - A kind of kjeldahl apparatus - Google Patents

A kind of kjeldahl apparatus Download PDF

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Publication number
CN208705293U
CN208705293U CN201821367997.4U CN201821367997U CN208705293U CN 208705293 U CN208705293 U CN 208705293U CN 201821367997 U CN201821367997 U CN 201821367997U CN 208705293 U CN208705293 U CN 208705293U
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China
Prior art keywords
pipe
furnace
return pipe
kjeldahl apparatus
water
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CN201821367997.4U
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Chinese (zh)
Inventor
缪玮
王鑫
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Jiangsu Jiaxin Detection Technology Co Ltd
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Jiangsu Jiaxin Detection Technology Co Ltd
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Priority to CN201821367997.4U priority Critical patent/CN208705293U/en
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  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

This application provides a kind of kjeldahl apparatus, the kjeldahl apparatus includes disappearing to boil furnace, the water bath heating device for boiling described disappearing stove heating, it is filled in the water bath heating device for offseting the water for boiling stove heating, described disappearing boils furnace placement in water, is provided with heater wire on the side wall of the water bath heating device.A kind of kjeldahl apparatus of the application is offseted by water bath heating device and boils furnace and heated, and the liquid boiled in furnace that disappears will not boil, and is prevented from disappearing and is boiled liquid in furnace and evaporate rapidly and generate a large amount of vapor.

Description

A kind of kjeldahl apparatus
Technical field
This application involves a kind of kjeldahl apparatus.
Background technique
Kjeldahl's method is a kind of method for measuring nitrogen pool in compound or mixture.I.e. in the condition for having catalyst Under, organic nitrogen is all transformed into inorganic ammonium salt with concentrated sulfuric acid sample digestion, then converts ammonia for ammonium salt under alkaline condition, with Steam distillation comes out and is excessive borate absorption, then with standard titration with hydrochloric acid, so that it may calculate the nitrogen quantity in sample.By It is more constant in protein nitrogen content, protein content can be calculated by its nitrogen quantity, so method is classical protein quantitation methods.
Summary of the invention
The application technical problems to be solved are to provide a kind of kjeldahl apparatus.
In order to solve the above-mentioned technical problem, this application provides a kind of kjeldahl apparatus, the kjeldahl apparatus includes Disappear and boil furnace, the water bath heating device for boiling stove heating to described disappearing, fills in the water bath heating device for offseting The water of stove heating is boiled, described disappearing is boiled furnace and placed in water, is provided with heater wire on the side wall of the water bath heating device.
Preferably, described disappear boils the return pipe that stove has one to be arranged along the vertical direction, the upper end of the return pipe It is provided with a demister, it further includes a first pipe that furnace is boiled in described disappearing, and the one end of the first pipe is connected to described Disappear and boil the bottom of furnace, the other end of the first pipe is located at the upper end of the return pipe.
Preferably, a water pump is provided in the first pipe, the water pump is for boiling described disappearing in furnace Liquid is delivered to the upper end of the return pipe, and the liquid is fallen after rise after being transported to the upper end of return pipe from return pipe It is boiled in furnace to described disappearing.
Preferably, at least part of the first pipe is located in the return pipe, and the first pipe The upper end of the return pipe is extended upwardly to from the lower end of return pipe.
Preferably, the kjeldahl apparatus further includes a titration cup, and the titration cup passes through a second pipe and institute The upper end for the return pipe stated is connected.
Preferably, a condenser is additionally provided on the second pipe.
Preferably, the condenser includes the condenser pipe of setting of spiraling, and the one end of the condenser pipe is condensed water Entrance, the other end are condensation-water drain.
Preferably, the heater wire of the side wall of the water bath heating device is carbon fiber heating wire.
A kind of kjeldahl apparatus of the application is offseted by water bath heating device and boils furnace and heated, and disappear the liquid boiled in furnace Body will not boil, and prevent from disappearing and boil liquid in furnace and evaporate rapidly and generate a large amount of vapor.
In addition, disappearing boils furnace provided with water pump, the water pump liquid boiled in furnace that will disappear is pumped into eminence, then falls after rise and boils furnace into disappearing In, it plays the role of stirring, the ammonia boiled in furnace that makes to disappear evaporates rapidly.
The condenser of the kjeldahl apparatus of the application can make gas be condensed into liquid, fall into titration cup.
Detailed description of the invention
Fig. 1 is a kind of structural schematic diagram of kjeldahl apparatus.
Wherein: 1, water bath heating device;2, disappear and boil furnace;3, it pumps;4, first pipe;5, return pipe;6, demister;7, it condenses Device;71, condensing water inlet;72, condensation-water drain;73, condenser pipe;8, second pipe;9, titration cup.
Specific embodiment
The application is described further in the following with reference to the drawings and specific embodiments, so that those skilled in the art can be with It more fully understands the application and can be practiced, but illustrated embodiment is not as the restriction to the application.
As shown in the figure.This application provides a kind of kjeldahl apparatus, the kjeldahl apparatus includes disappearing boil furnace 2, be used for The water bath heating device 1 of the heating of furnace 2 is boiled to described disappearing, and is filled in the water bath heating device 1 and is boiled the heating of furnace 2 for offseting Water, described disappearing boil furnace 2 place in water, be provided with heater wire on the side wall of the water bath heating device 1.Described disappears Furnace 2 is boiled with a return pipe 5 being arranged along the vertical direction, the upper end of the return pipe 5 is provided with a demister 6, described Disappear that boil furnace 2 further include a first pipe 4, the one end of the first pipe 4 is connected to described disappearing and boils the bottom of furnace 2, The other end of the first pipe 4 is located at the upper end of the return pipe 5.One is provided in the first pipe 4 Water pump 3, the water pump 3 is used to boil described disappearing the upper end that the liquid in furnace 2 is delivered to the return pipe 5, described Liquid be transported to behind the upper end of return pipe 5 to fall after rise from return pipe 5 to described disappearing and boil in furnace 2.The first pipe 4 At least part be located in the return pipe 5, and the first pipe 4 is extended upwardly to from the lower end of return pipe 5 The upper end of the return pipe 5.The kjeldahl apparatus further includes a titration cup 9, and the titration cup 9 passes through one second Pipeline 8 is connected with the upper end of the return pipe 5.A condenser 7 is additionally provided on the second pipe 8.Described The one end of condenser pipe 73 of the condenser 7 including setting of spiraling, the condenser pipe 73 is condensing water inlet 71, and the other end is Condensation-water drain 72.The heater wire of the side wall of the water bath heating device 1 is carbon fiber heating wire.
A kind of kjeldahl apparatus of the application is offseted by water bath heating device 1 and boils furnace 2 and heated, disappeared and boil in furnace 2 Liquid will not boil, and prevent from disappearing and boil liquid in furnace 2 and evaporate rapidly and generate a large amount of vapor.Disappear and boil furnace 2 provided with water pump 3, The liquid pump 3 boiled in furnace 2 that will disappear of water pump 3 enters eminence, then falls after rise to disappear and boil in furnace 2, play the role of stirring, makes to disappear and boil furnace 2 Interior ammonia evaporates rapidly.The condenser 7 of the kjeldahl apparatus of the application, can make gas be condensed into liquid, fall into titration cup 9 In.
Embodiment described above is only the preferred embodiment lifted to absolutely prove the application, the protection model of the application It encloses without being limited thereto.Those skilled in the art made equivalent substitute or transformation on the basis of the application, in the application Protection scope within.The protection scope of the application is subject to claims.

Claims (8)

1. a kind of kjeldahl apparatus, which is characterized in that the kjeldahl apparatus includes disappearing to boil furnace, for boiling furnace to described disappearing The water bath heating device of heating is filled for offseting the water for boiling stove heating in the water bath heating device, and furnace is boiled in described disappearing It places in water, is provided with heater wire on the side wall of the water bath heating device.
2. a kind of kjeldahl apparatus as described in claim 1, which is characterized in that stove is boiled in described disappearing to be had one along the vertical direction The return pipe of setting, the upper end of the return pipe are provided with a demister, and it further includes a first pipe that furnace is boiled in described disappearing, The one end of the first pipe is connected to described disappearing and boils the bottom of furnace, and the other end of the first pipe is located at institute The upper end for the return pipe stated.
3. a kind of kjeldahl apparatus as claimed in claim 2, which is characterized in that be provided with a water in the first pipe Pump, the water pump are used to boil described disappearing the upper end that the liquid in furnace is delivered to the return pipe, the liquid It is transported to behind the upper end of return pipe to fall after rise from return pipe to described disappearing and boil in furnace.
4. a kind of kjeldahl apparatus as claimed in claim 3, which is characterized in that at least part position of the first pipe In in the return pipe, and the first pipe extends upwardly to the upper end of the return pipe from the lower end of return pipe Portion.
5. a kind of kjeldahl apparatus as claimed in claim 4, which is characterized in that the kjeldahl apparatus further includes a titration Cup, the titration cup are connected by a second pipe with the upper end of the return pipe.
6. a kind of kjeldahl apparatus as claimed in claim 5, which is characterized in that it is cold to be additionally provided with one on the second pipe Condenser.
7. a kind of kjeldahl apparatus as claimed in claim 6, which is characterized in that the condenser includes the cold of setting that spiral The one end of solidifying pipe, the condenser pipe is condensing water inlet, and the other end is condensation-water drain.
8. a kind of kjeldahl apparatus as claimed in claim 7, which is characterized in that the side wall of the water bath heating device adds Hot line is carbon fiber heating wire.
CN201821367997.4U 2018-08-23 2018-08-23 A kind of kjeldahl apparatus Active CN208705293U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201821367997.4U CN208705293U (en) 2018-08-23 2018-08-23 A kind of kjeldahl apparatus

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201821367997.4U CN208705293U (en) 2018-08-23 2018-08-23 A kind of kjeldahl apparatus

Publications (1)

Publication Number Publication Date
CN208705293U true CN208705293U (en) 2019-04-05

Family

ID=65944593

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201821367997.4U Active CN208705293U (en) 2018-08-23 2018-08-23 A kind of kjeldahl apparatus

Country Status (1)

Country Link
CN (1) CN208705293U (en)

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