CN208705293U - A kind of kjeldahl apparatus - Google Patents
A kind of kjeldahl apparatus Download PDFInfo
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- CN208705293U CN208705293U CN201821367997.4U CN201821367997U CN208705293U CN 208705293 U CN208705293 U CN 208705293U CN 201821367997 U CN201821367997 U CN 201821367997U CN 208705293 U CN208705293 U CN 208705293U
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- pipe
- furnace
- return pipe
- kjeldahl apparatus
- water
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Abstract
This application provides a kind of kjeldahl apparatus, the kjeldahl apparatus includes disappearing to boil furnace, the water bath heating device for boiling described disappearing stove heating, it is filled in the water bath heating device for offseting the water for boiling stove heating, described disappearing boils furnace placement in water, is provided with heater wire on the side wall of the water bath heating device.A kind of kjeldahl apparatus of the application is offseted by water bath heating device and boils furnace and heated, and the liquid boiled in furnace that disappears will not boil, and is prevented from disappearing and is boiled liquid in furnace and evaporate rapidly and generate a large amount of vapor.
Description
Technical field
This application involves a kind of kjeldahl apparatus.
Background technique
Kjeldahl's method is a kind of method for measuring nitrogen pool in compound or mixture.I.e. in the condition for having catalyst
Under, organic nitrogen is all transformed into inorganic ammonium salt with concentrated sulfuric acid sample digestion, then converts ammonia for ammonium salt under alkaline condition, with
Steam distillation comes out and is excessive borate absorption, then with standard titration with hydrochloric acid, so that it may calculate the nitrogen quantity in sample.By
It is more constant in protein nitrogen content, protein content can be calculated by its nitrogen quantity, so method is classical protein quantitation methods.
Summary of the invention
The application technical problems to be solved are to provide a kind of kjeldahl apparatus.
In order to solve the above-mentioned technical problem, this application provides a kind of kjeldahl apparatus, the kjeldahl apparatus includes
Disappear and boil furnace, the water bath heating device for boiling stove heating to described disappearing, fills in the water bath heating device for offseting
The water of stove heating is boiled, described disappearing is boiled furnace and placed in water, is provided with heater wire on the side wall of the water bath heating device.
Preferably, described disappear boils the return pipe that stove has one to be arranged along the vertical direction, the upper end of the return pipe
It is provided with a demister, it further includes a first pipe that furnace is boiled in described disappearing, and the one end of the first pipe is connected to described
Disappear and boil the bottom of furnace, the other end of the first pipe is located at the upper end of the return pipe.
Preferably, a water pump is provided in the first pipe, the water pump is for boiling described disappearing in furnace
Liquid is delivered to the upper end of the return pipe, and the liquid is fallen after rise after being transported to the upper end of return pipe from return pipe
It is boiled in furnace to described disappearing.
Preferably, at least part of the first pipe is located in the return pipe, and the first pipe
The upper end of the return pipe is extended upwardly to from the lower end of return pipe.
Preferably, the kjeldahl apparatus further includes a titration cup, and the titration cup passes through a second pipe and institute
The upper end for the return pipe stated is connected.
Preferably, a condenser is additionally provided on the second pipe.
Preferably, the condenser includes the condenser pipe of setting of spiraling, and the one end of the condenser pipe is condensed water
Entrance, the other end are condensation-water drain.
Preferably, the heater wire of the side wall of the water bath heating device is carbon fiber heating wire.
A kind of kjeldahl apparatus of the application is offseted by water bath heating device and boils furnace and heated, and disappear the liquid boiled in furnace
Body will not boil, and prevent from disappearing and boil liquid in furnace and evaporate rapidly and generate a large amount of vapor.
In addition, disappearing boils furnace provided with water pump, the water pump liquid boiled in furnace that will disappear is pumped into eminence, then falls after rise and boils furnace into disappearing
In, it plays the role of stirring, the ammonia boiled in furnace that makes to disappear evaporates rapidly.
The condenser of the kjeldahl apparatus of the application can make gas be condensed into liquid, fall into titration cup.
Detailed description of the invention
Fig. 1 is a kind of structural schematic diagram of kjeldahl apparatus.
Wherein: 1, water bath heating device;2, disappear and boil furnace;3, it pumps;4, first pipe;5, return pipe;6, demister;7, it condenses
Device;71, condensing water inlet;72, condensation-water drain;73, condenser pipe;8, second pipe;9, titration cup.
Specific embodiment
The application is described further in the following with reference to the drawings and specific embodiments, so that those skilled in the art can be with
It more fully understands the application and can be practiced, but illustrated embodiment is not as the restriction to the application.
As shown in the figure.This application provides a kind of kjeldahl apparatus, the kjeldahl apparatus includes disappearing boil furnace 2, be used for
The water bath heating device 1 of the heating of furnace 2 is boiled to described disappearing, and is filled in the water bath heating device 1 and is boiled the heating of furnace 2 for offseting
Water, described disappearing boil furnace 2 place in water, be provided with heater wire on the side wall of the water bath heating device 1.Described disappears
Furnace 2 is boiled with a return pipe 5 being arranged along the vertical direction, the upper end of the return pipe 5 is provided with a demister 6, described
Disappear that boil furnace 2 further include a first pipe 4, the one end of the first pipe 4 is connected to described disappearing and boils the bottom of furnace 2,
The other end of the first pipe 4 is located at the upper end of the return pipe 5.One is provided in the first pipe 4
Water pump 3, the water pump 3 is used to boil described disappearing the upper end that the liquid in furnace 2 is delivered to the return pipe 5, described
Liquid be transported to behind the upper end of return pipe 5 to fall after rise from return pipe 5 to described disappearing and boil in furnace 2.The first pipe 4
At least part be located in the return pipe 5, and the first pipe 4 is extended upwardly to from the lower end of return pipe 5
The upper end of the return pipe 5.The kjeldahl apparatus further includes a titration cup 9, and the titration cup 9 passes through one second
Pipeline 8 is connected with the upper end of the return pipe 5.A condenser 7 is additionally provided on the second pipe 8.Described
The one end of condenser pipe 73 of the condenser 7 including setting of spiraling, the condenser pipe 73 is condensing water inlet 71, and the other end is
Condensation-water drain 72.The heater wire of the side wall of the water bath heating device 1 is carbon fiber heating wire.
A kind of kjeldahl apparatus of the application is offseted by water bath heating device 1 and boils furnace 2 and heated, disappeared and boil in furnace 2
Liquid will not boil, and prevent from disappearing and boil liquid in furnace 2 and evaporate rapidly and generate a large amount of vapor.Disappear and boil furnace 2 provided with water pump 3,
The liquid pump 3 boiled in furnace 2 that will disappear of water pump 3 enters eminence, then falls after rise to disappear and boil in furnace 2, play the role of stirring, makes to disappear and boil furnace 2
Interior ammonia evaporates rapidly.The condenser 7 of the kjeldahl apparatus of the application, can make gas be condensed into liquid, fall into titration cup 9
In.
Embodiment described above is only the preferred embodiment lifted to absolutely prove the application, the protection model of the application
It encloses without being limited thereto.Those skilled in the art made equivalent substitute or transformation on the basis of the application, in the application
Protection scope within.The protection scope of the application is subject to claims.
Claims (8)
1. a kind of kjeldahl apparatus, which is characterized in that the kjeldahl apparatus includes disappearing to boil furnace, for boiling furnace to described disappearing
The water bath heating device of heating is filled for offseting the water for boiling stove heating in the water bath heating device, and furnace is boiled in described disappearing
It places in water, is provided with heater wire on the side wall of the water bath heating device.
2. a kind of kjeldahl apparatus as described in claim 1, which is characterized in that stove is boiled in described disappearing to be had one along the vertical direction
The return pipe of setting, the upper end of the return pipe are provided with a demister, and it further includes a first pipe that furnace is boiled in described disappearing,
The one end of the first pipe is connected to described disappearing and boils the bottom of furnace, and the other end of the first pipe is located at institute
The upper end for the return pipe stated.
3. a kind of kjeldahl apparatus as claimed in claim 2, which is characterized in that be provided with a water in the first pipe
Pump, the water pump are used to boil described disappearing the upper end that the liquid in furnace is delivered to the return pipe, the liquid
It is transported to behind the upper end of return pipe to fall after rise from return pipe to described disappearing and boil in furnace.
4. a kind of kjeldahl apparatus as claimed in claim 3, which is characterized in that at least part position of the first pipe
In in the return pipe, and the first pipe extends upwardly to the upper end of the return pipe from the lower end of return pipe
Portion.
5. a kind of kjeldahl apparatus as claimed in claim 4, which is characterized in that the kjeldahl apparatus further includes a titration
Cup, the titration cup are connected by a second pipe with the upper end of the return pipe.
6. a kind of kjeldahl apparatus as claimed in claim 5, which is characterized in that it is cold to be additionally provided with one on the second pipe
Condenser.
7. a kind of kjeldahl apparatus as claimed in claim 6, which is characterized in that the condenser includes the cold of setting that spiral
The one end of solidifying pipe, the condenser pipe is condensing water inlet, and the other end is condensation-water drain.
8. a kind of kjeldahl apparatus as claimed in claim 7, which is characterized in that the side wall of the water bath heating device adds
Hot line is carbon fiber heating wire.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201821367997.4U CN208705293U (en) | 2018-08-23 | 2018-08-23 | A kind of kjeldahl apparatus |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201821367997.4U CN208705293U (en) | 2018-08-23 | 2018-08-23 | A kind of kjeldahl apparatus |
Publications (1)
Publication Number | Publication Date |
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CN208705293U true CN208705293U (en) | 2019-04-05 |
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ID=65944593
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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CN201821367997.4U Active CN208705293U (en) | 2018-08-23 | 2018-08-23 | A kind of kjeldahl apparatus |
Country Status (1)
Country | Link |
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CN (1) | CN208705293U (en) |
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2018
- 2018-08-23 CN CN201821367997.4U patent/CN208705293U/en active Active
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