CN208627264U - Reaction kettle - Google Patents

Reaction kettle Download PDF

Info

Publication number
CN208627264U
CN208627264U CN201721926723.XU CN201721926723U CN208627264U CN 208627264 U CN208627264 U CN 208627264U CN 201721926723 U CN201721926723 U CN 201721926723U CN 208627264 U CN208627264 U CN 208627264U
Authority
CN
China
Prior art keywords
autoclave body
heating tube
reaction kettle
agitating shaft
port
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201721926723.XU
Other languages
Chinese (zh)
Inventor
钟燕龙
马跃起
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Guangzhou Cheng Na Chemical Co Ltd
Original Assignee
Guangzhou Cheng Na Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Guangzhou Cheng Na Chemical Co Ltd filed Critical Guangzhou Cheng Na Chemical Co Ltd
Priority to CN201721926723.XU priority Critical patent/CN208627264U/en
Application granted granted Critical
Publication of CN208627264U publication Critical patent/CN208627264U/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

The utility model relates to reaction kettle technical fields, and more particularly, to a kind of reaction kettle, including autoclave body and agitating device, the upper end of the autoclave body is provided with feed inlet, and the feed inlet is communicated with rectifying column;The agitating device includes driving portion and agitating shaft, and the agitating shaft is located in the autoclave body, and the agitating shaft is connected with the driving portion;Wherein, the inner wall surrounding of the autoclave body is provided with heating tube, and the first port of the heating tube is connected with the inlet on the autoclave body, the second port of the heating tube is connected with the liquid outlet on the autoclave body.In the present solution, improving its rectification effect using heating tube to heating in autoclave body, reaction efficiency is high, and binder is thorough, simple to operate, and the heating speed of product improves, and the period shortens, and cost is reduced.

Description

Reaction kettle
Technical field
The utility model relates to reaction kettle technical fields, more particularly, to a kind of reaction kettle.
Background technique
Currently, reaction kettle is that one kind is widely used in the fields such as petroleum, chemical industry, rubber, pesticide, fuel and food, it is used to The pressure vessel of the technical process such as vulcanization, nitrification, hydrogenation, polymerization or condensation is completed, in use, it is necessary in strict accordance with production The operating pressure and operating temperature that product are indicated are operated, in order to avoid causing danger, at work, reactant are generally put into reaction In kettle, then it is sufficiently stirred, so that good reactivity can be played, but some reactants only simply stir It mixes, reaction effect is unsatisfactory, and is possible to crystal block condensation phenomenon occur, and this reduces the quantity of reaction product, mention High cost, reduces economic benefit, especially when carrying out rectification process, requires more preferably reaction kettle body, general reaction kettle It is unable to reach good reactivity worth, product rectification effect is poor, and binder is difficult, and the heating speed of product is slow, and the period is long, cost It is higher.
Utility model content
One of the utility model is designed to provide a kind of reaction kettle, at least to solve technology existing in the prior art One of problem.
To achieve the goals above, the utility model provides following technical scheme;
The utility model provides a kind of reaction kettle, including autoclave body and agitating device, and the upper end of the autoclave body is provided with charging Mouthful, the feed inlet is communicated with rectifying column;
The agitating device includes driving portion and agitating shaft, and the agitating shaft is located in the autoclave body, and the agitating shaft It is connected with the driving portion;
Wherein, the inner wall surrounding of the autoclave body is provided with heating tube, and the first port of the heating tube with it is described Inlet on autoclave body is connected, and the second port of the heating tube is connected with the liquid outlet on the autoclave body.
Meanwhile adiabator layer is set on the outer wall of autoclave body.
In the above-mentioned technical solutions, further, the heating tube is arranged in the periphery of inner wall of the autoclave body in the shape of a spiral.
In the technical scheme, heating tube is arranged in the periphery of inner wall of autoclave body in the shape of a spiral, makes the intracorporal heating of kettle in this way Temperature can be more uniform, improves reaction efficiency.
In any of the above-described technical solution, further, the agitating shaft is located at the spiral center axis of helical form heating tube On.
In the technical scheme, the case where encountering heating tube when avoiding agitating shaft rotation generation.
In any of the above-described technical solution, further, the heating tube is in second port direction along first port Multiple U-shaped structure arrangements.
In the technical scheme, the end to end layout of multiple U-tubes, structure is simple, good heat dissipation effect, and then make to shed In heat transfer to autoclave body.
In any of the above-described technical solution, further, temperature sensor is provided in the heating tube.
In the technical scheme, the convenient control to fluid temperature in heating tube of the setting of temperature sensor is replaced.
In any of the above-described technical solution, further, erosion resistant coating is provided on the inner wall of the autoclave body.
In the technical scheme, erosion resistant coating has anti-corrosion material to be made, and avoids autoclave body and is corroded, and extends the use of autoclave body Service life.
In any of the above-described technical solution, further, the inner wall painting of the autoclave body is provided with catalyst layer.
In the technical scheme, the setting of catalyst layer, which can be carried out efficiently quickly to react, improves catalysis reactivity, into One step improves rectifying purity.
In any of the above-described technical solution, further, the liquid outlet is connected with water circulating pump by pipeline, described to follow The outlet of ring water pump connects having heaters, and the outlet of the heater is connected with the inlet.
In the technical scheme, heating liquid can be efficiently used, resource is saved.
In any of the above-described technical solution, further, the exit of the heater is provided with temperature sensor.
In any of the above-described technical solution, further, the bottom of the autoclave body is provided with sewage draining exit, and the sewage draining exit It is connected by pipeline with wastewater trough.Residue is handled, safety and environmental protection.
By adopting the above technical scheme, the utility model has the following beneficial effects:
Reaction kettle provided by the utility model, the upper end of autoclave body are provided with feed inlet, and feed inlet is communicated with rectifying column;Stirring Device includes driving portion and agitating shaft, and agitating shaft is located in autoclave body, and agitating shaft is connected with driving portion;Wherein, close to autoclave body Inner wall surrounding be provided with heating tube, and the first port of heating tube is connected with the inlet on autoclave body, the second of heating tube Port is connected with the liquid outlet on autoclave body, using heating tube to heating in autoclave body, improves its rectification effect, reaction effect Rate is high, and binder is thorough, simple to operate, and the heating speed of product improves, and the period shortens, and cost is reduced.
The additional aspect and advantage of the utility model will become obviously in following description section, or practical new by this The practice of type is recognized.
Detailed description of the invention
It below will be right in order to illustrate more clearly of specific embodiment of the present invention or technical solution in the prior art Specific embodiment or attached drawing needed to be used in the description of the prior art are briefly described, it should be apparent that, it is described below In attached drawing be that some embodiments of the utility model are not paying creativeness for those of ordinary skill in the art Under the premise of labour, it is also possible to obtain other drawings based on these drawings.
Fig. 1 is a kind of structural schematic diagram of embodiment of reaction kettle provided by the embodiment of the utility model;
Fig. 2 is the structural schematic diagram of reaction kettle another embodiment provided by the embodiment of the utility model.
Appended drawing reference:
10- autoclave body;101- feed inlet;102- inlet;103- liquid outlet;104- sewage draining exit;11- agitating device;111- Driving portion;112- agitating shaft;12- heating tube;13- water circulating pump;14- heater;15- wastewater trough;16- rectifying column.
Specific embodiment
The technical solution of the utility model is clearly and completely described below in conjunction with attached drawing, it is clear that described Embodiment is the utility model a part of the embodiment, instead of all the embodiments.Based on the embodiments of the present invention, originally Field those of ordinary skill every other embodiment obtained without making creative work belongs to practical Novel protected range.It should be noted that in the absence of conflict, the feature in embodiments herein and embodiment can To be combined with each other.
It is in the description of the present invention, it should be noted that term " center ", "upper", "lower", "left", "right", " perpendicular Directly ", the orientation or positional relationship of the instructions such as "horizontal", "inner", "outside" is to be based on the orientation or positional relationship shown in the drawings, and is only For ease of description the utility model and simplify description, rather than the device or element of indication or suggestion meaning must have it is specific Orientation, be constructed and operated in a specific orientation, therefore should not be understood as limiting the present invention.In addition, term " the One ", " second ", " third " are used for descriptive purposes only and cannot be understood as indicating or suggesting relative importance.
In the description of the present invention, it should be noted that unless otherwise clearly defined and limited, term " is pacified Dress ", " connected ", " connection " shall be understood in a broad sense, for example, it may be being fixedly connected, may be a detachable connection, or integrally Connection;It can be mechanical connection, be also possible to be electrically connected;Can be directly connected, can also indirectly connected through an intermediary, It can be the connection inside two elements.For the ordinary skill in the art, above-mentioned art can be understood with concrete condition The concrete meaning of language in the present invention.
Explanation is further explained to the utility model below with reference to specific embodiment.
Fig. 1 is a kind of structural schematic diagram of embodiment of reaction kettle provided by the embodiment of the utility model;Fig. 2 is that this is practical The structural schematic diagram for the reaction kettle another embodiment that new embodiment provides.
Embodiment one
As depicted in figs. 1 and 2, reaction kettle provided in this embodiment, including autoclave body 10 and agitating device 11, the autoclave body 10 Upper end be provided with feed inlet 101, the feed inlet 101 is communicated with rectifying column 16;
Specifically, the agitating device 11 includes driving portion 111 and agitating shaft 112, and the agitating shaft 112 is located at the kettle In body 10, and the agitating shaft 112 is connected with the driving portion 111;
Wherein, the inner wall surrounding of the autoclave body 10 is provided with heating tube 12, and the first port of the heating tube 12 It is connected with the inlet 102 on the autoclave body 10, the liquid outlet in the second port of the heating tube 12 and the autoclave body 10 103 are connected.
Meanwhile adiabator layer is set on the outer wall of autoclave body 10.Using heating tube 12 to being heated in autoclave body 10, make Its rectification effect improves, and reaction efficiency is high, and binder is thorough, simple to operate, and the heating speed of product improves, and the period shortens.
In an optional embodiment of the present embodiment, the heating tube 12 is arranged in the autoclave body 10 in the shape of a spiral Periphery of inner wall.
In this embodiment, heating tube 12 is arranged in the periphery of inner wall of autoclave body 10 in the shape of a spiral, makes in autoclave body 10 in this way Heating temperature can be more uniform, improve reaction efficiency.
On the basis of the above embodiment, the agitating shaft 112 is located on the spiral center axis of helical form heating tube 12.
In this embodiment, the case where encountering heating tube 12 when agitating shaft 112 rotates generation is avoided.
In another optional embodiment of the present embodiment, the heating tube 12 is along first port to second port Direction is arranged in multiple U-shaped structures.
In this embodiment, the end to end layout of multiple U-tubes, structure is simple, good heat dissipation effect, and then make to shed In heat transfer to autoclave body 10.
In an optional embodiment of the present embodiment, temperature sensor is provided in the heating tube 12.
In this embodiment, the convenient control to fluid temperature in heating tube 12 of the setting of temperature sensor is replaced.
In an optional embodiment of the present embodiment, erosion resistant coating is provided on the inner wall of the autoclave body 10.
In this embodiment, erosion resistant coating has anti-corrosion material to be made, and avoids autoclave body 10 and is corroded, extends autoclave body 10 Service life.
In an optional embodiment of the present embodiment, the inner wall painting of the autoclave body 10 is provided with catalyst layer.
In this embodiment, the setting of catalyst layer, which can be carried out efficiently quickly to react, improves catalysis reactivity, into One step improves rectifying purity.
In an optional embodiment of the present embodiment, as shown in Fig. 2, the liquid outlet 103 is connected by pipeline There is water circulating pump 13, the outlet of the water circulating pump 13 connects having heaters 14, the outlet of the heater 14 and the feed liquor Mouth 102 is connected.
In this embodiment, heating liquid can be efficiently used, resource is saved.
The temperature that liquid is heated in heater 14 is controlled for convenience, the exit of the heater 14 is provided with temperature Sensor, while temperature sensor is connected with the solenoid valve that exit is arranged, the switch exported by solenoid valve control.
Preferably, the bottom of the autoclave body 10 is provided with sewage draining exit 104, and the sewage draining exit 104 passes through pipeline and waste water Slot 15 is connected.Residue is handled, safety and environmental protection.
Specifically, reaction kettle is that one kind is widely used in the fields such as petroleum, chemical industry, rubber, pesticide, fuel and food, For completing the pressure vessel of the technical process such as vulcanization, nitrification, hydrogenation, polymerization or condensation, in use, it is necessary to strictly press The operating pressure and operating temperature indicated according to product are operated, in order to avoid danger is caused, in the prior art, at work, generally Reactant is put into reaction kettle, is then sufficiently stirred, so that good reactivity can be played, but some reactions Object only simple stirring, reaction effect is unsatisfactory, and is possible to crystal block condensation phenomenon occur, and this reduces reactions to give birth to At the quantity of object, cost is improved, reduces economic benefit, especially when carrying out rectification process, reaction kettle body is required more preferably, General reaction kettle is unable to reach good reactivity worth, and product rectification effect is poor, and binder is difficult, the heating speed of product Slowly, the period is long, higher cost.And reaction kettle provided by the utility model, the upper end of autoclave body are provided with feed inlet, feed inlet connection There is rectifying column;Agitating device includes driving portion and agitating shaft, and agitating shaft is located in autoclave body, and agitating shaft is connected with driving portion; Wherein, the inner wall surrounding of autoclave body is provided with heating tube, and the first port of heating tube is connected with the inlet on autoclave body, The second port of heating tube is connected with the liquid outlet on autoclave body, using heating tube to heating in autoclave body, imitates its rectifying Fruit is improved, and reaction efficiency is high, and binder is thorough, simple to operate, and the heating speed of product improves, and the period shortens, and cost is reduced, Heating tube is arranged in the periphery of inner wall of autoclave body in the shape of a spiral, makes the intracorporal heating temperature of kettle can be more uniform in this way, improves reaction Efficiency, the setting of catalyst layer, which can be carried out efficiently quickly to react, improves catalysis reactivity, further improves rectifying purity.
Finally, it should be noted that the above various embodiments is only to illustrate the technical solution of the utility model, rather than it is limited System;Although the present invention has been described in detail with reference to the aforementioned embodiments, those skilled in the art should Understand: it is still possible to modify the technical solutions described in the foregoing embodiments, or to some or all of Technical characteristic is equivalently replaced;And these are modified or replaceed, it does not separate the essence of the corresponding technical solution, and this is practical new The range of each embodiment technical solution of type.In addition, it will be appreciated by those of skill in the art that although some implementations described herein Example includes certain features included in other embodiments rather than other feature, but the group of the feature of different embodiments is desirable Taste within the scope of the utility model and form different embodiments.For example, in claims above, institute Claimed embodiment it is one of any can in any combination mode come using.It is disclosed in the background technology part Information is merely intended to deepen the understanding to the general background technology of the utility model, and is not construed as recognizing or with any shape Formula implies that the information constitutes the prior art known to those skilled in the art.

Claims (7)

1. a kind of reaction kettle, which is characterized in that including autoclave body and agitating device, the upper end of the autoclave body is provided with feed inlet, institute It states feed inlet and is communicated with rectifying column;
The agitating device includes driving portion and agitating shaft, and the agitating shaft is located in the autoclave body, and the agitating shaft and institute Driving portion is stated to be connected;
Wherein, the inner wall surrounding of the autoclave body is provided with heating tube, and the first port of the heating tube and the autoclave body On inlet be connected, the second port of the heating tube is connected with the liquid outlet on the autoclave body;
Erosion resistant coating is provided on the inner wall of the autoclave body;
The inner wall painting of the autoclave body is provided with catalyst layer;
The heating tube is arranged in the periphery of inner wall of the autoclave body in the shape of a spiral.
2. reaction kettle according to claim 1, which is characterized in that
The agitating shaft is located on the spiral center axis of helical form heating tube.
3. reaction kettle according to claim 2, which is characterized in that
The heating tube is arranged to second port direction in multiple U-shaped structures along first port.
4. reaction kettle according to claim 1, which is characterized in that
Temperature sensor is provided in the heating tube.
5. reaction kettle according to claim 1, which is characterized in that
The liquid outlet is connected with water circulating pump by pipeline, and the outlet of the water circulating pump connects having heaters, the heating The outlet of device is connected with the inlet.
6. reaction kettle according to claim 5, which is characterized in that
The exit of the heater is provided with temperature sensor.
7. reaction kettle according to claim 1, which is characterized in that
The bottom of the autoclave body is provided with sewage draining exit, and the sewage draining exit is connected by pipeline with wastewater trough.
CN201721926723.XU 2017-12-29 2017-12-29 Reaction kettle Active CN208627264U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201721926723.XU CN208627264U (en) 2017-12-29 2017-12-29 Reaction kettle

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201721926723.XU CN208627264U (en) 2017-12-29 2017-12-29 Reaction kettle

Publications (1)

Publication Number Publication Date
CN208627264U true CN208627264U (en) 2019-03-22

Family

ID=65731264

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201721926723.XU Active CN208627264U (en) 2017-12-29 2017-12-29 Reaction kettle

Country Status (1)

Country Link
CN (1) CN208627264U (en)

Similar Documents

Publication Publication Date Title
US5478535A (en) Apparatus for gas - liquid reactions
CN109603710A (en) It is a kind of synthesis p-chlorotoluene can temperature automatically controlled reaction kettle
CN208627264U (en) Reaction kettle
CN204865828U (en) Cinnamic acid gas -liquid mixture reation kettle
CN101735019B (en) Process for producing resorcinol by continuously hydrolyzing m-phenylenediamine
CN203944382U (en) Liquid-phase reactor
CN206463955U (en) Homogeneous continuous still reaction system and homogeneous reaction kettle for exothermic reaction
CN202876812U (en) Reaction kettle for producing petrochemical products
CN106281727B (en) A kind of novel ester exchange reaction device
CN209810150U (en) Reation kettle of medical intermediate production usefulness with cooling function
CN205392436U (en) Reation kettle with storage device
CN109012537A (en) A kind of energy-saving reaction kettle with high efficient heat exchanging function
CN205412995U (en) Reation kettle is used in preparation of controllable temperature type inhibition antisludging agent
CN201512488U (en) Cyclobutyl sulfone device for manufacturing cyclobutyl sulfone
CN201512489U (en) Device for producing sulfolene
CN207941516U (en) A kind of isothermal reaction kettle
CN206560854U (en) A kind of stainless steel cauldron
CN203244969U (en) Chemical reaction kettle
CN206014934U (en) A kind of special retort of agricultural amino acid
CN202366684U (en) Continuous ethyl hexanoate esterification reaction kettle
CN102181047B (en) Polyethylene terephthalate (PET) esterification reaction kettle
CN205684000U (en) A kind of chemical industry stirred autoclave with compound inner coil pipe
CN219092056U (en) Pilot scale device for fine chemical synthesis
CN202036994U (en) Improved reactor
CN217594630U (en) Lithium sulfate solution removes calcium intelligent reaction ware

Legal Events

Date Code Title Description
GR01 Patent grant
GR01 Patent grant