CN208612442U - It is a kind of can successive reaction chemical reaction equipment - Google Patents

It is a kind of can successive reaction chemical reaction equipment Download PDF

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Publication number
CN208612442U
CN208612442U CN201820942821.0U CN201820942821U CN208612442U CN 208612442 U CN208612442 U CN 208612442U CN 201820942821 U CN201820942821 U CN 201820942821U CN 208612442 U CN208612442 U CN 208612442U
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China
Prior art keywords
fluid
tube road
reaction
reaction vessel
solenoid valve
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CN201820942821.0U
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Chinese (zh)
Inventor
陈庆镇
章新道
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Cage (xiamen) Biotechnology Co Ltd
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Cage (xiamen) Biotechnology Co Ltd
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Abstract

The utility model provide it is a kind of can successive reaction chemical reaction equipment, including symmetrically arranged reaction vessel, fluid-through tube road is equipped in the corresponding position of the reaction vessel, it is equipped with vacuum pipe on the reaction vessel, is respectively equipped with the first solenoid valve and second solenoid valve on the fluid-through tube road and the vacuum pipe;The fluid-through tube road is divided into the first fluid-through tube road and the second fluid-through tube road, and first fluid-through tube road and the second fluid-through tube road are closed by fastener to be connected;The vacuum pipe is connected to vacuum pump;First solenoid valve, second solenoid valve and the vacuum pump and controller are electrically connected.One kind provided by the utility model can successive reaction chemical reaction equipment, have the advantages that structure design is simple, reaction can be carried out continuously, solves the problems, such as to complete to generate after back reaction substance in organic reaction and shift that cumbersome, to easily lead to final product impure.

Description

It is a kind of can successive reaction chemical reaction equipment
Technical field
The utility model relates to chemical reaction equipment, in particular to it is a kind of can successive reaction chemical reaction equipment.
Background technique
Existing organic chemical reactions device generally comprises reaction vessel, heating component, mixing component etc., passes through feed inlet Reaction raw materials are added into reaction vessel, recycles heating component to be heated, reaction solution is stirred using mixing component It mixes, finally obtains reactor product.In organic chemical reactions, usually the first step after the reaction was completed, it is also necessary to will be newly-generated Chemical substance is transferred in another reaction vessel, cumbersome in this course, and is easy to generate shadow to newly-generated substance It rings, the substance for causing end reaction to generate is impure.
Utility model content
Another reaction is transferred to solve generation substance after the completion of chemical reaction existing in the prior art mentioned above The problem that operation error causes the substance ultimately generated impure is easy to appear during container, the utility model provides one kind can The chemical reaction equipment of successive reaction, including symmetrically arranged reaction vessel are equipped in the corresponding position of the reaction vessel Fluid-through tube road, is equipped with vacuum pipe on the reaction vessel, and the is respectively equipped on the fluid-through tube road and the vacuum pipe One solenoid valve and second solenoid valve;The fluid-through tube road is divided into the first fluid-through tube road and the second fluid-through tube road, the first logical liquid Pipeline and the second fluid-through tube road are closed by fastener to be connected;The vacuum pipe is connected to vacuum pump;First solenoid valve, Second solenoid valve and the vacuum pump and controller are electrically connected.
Further, the fastener is formed by having magnetic left fastening block and right fastening block, the left fastening block and The nozzle in first fluid-through tube road and the second fluid-through tube road is closed after mutual absorption and is surrounded by right fastening block.
Further, it is designed with the first solenoid valve on first fluid-through tube road and second fluid-through tube road, described One solenoid valve receives the connection and envelope in instruction control first fluid-through tube road and second fluid-through tube road of the controller It closes.
Further, the bottom and side of the reaction vessel are additionally provided with electric heating cover, the electric heating cover and the control Device processed is electrically connected.
Further, the side of the reaction vessel is equipped with conveying mouth.
Further, blender is equipped in the reaction vessel, the blender is by being located at the top of the reaction vessel Stirring motor driving, the stirring motor connect with the controller.
It further, further include pedestal, the reaction vessel is set on the base, is equipped with display screen on the base And control button, the display screen and the control button and the controller are electrically connected.
One kind provided by the utility model can successive reaction chemical reaction equipment, changed in the reaction vessel of side After learning reaction, the second solenoid valve on the vacuum pipe of the reaction vessel of the other side can be opened, then open vacuum pump and cause negative pressure State then opens the first solenoid valve on fluid-through tube road, since the reaction vessel of the other side is negative pressure state, can will complete The chemical substance of reaction is extracted out, is entered in new reaction vessel by fluid-through tube road, is achieved the purpose that successive reaction;Extraction finishes After the first solenoid valve can be closed, the reaction vessel for completing reaction is unloaded and is cleaned, for recycling successive reaction.This is practical Novel offer it is a kind of can successive reaction chemical reaction equipment, have the advantages that structure design simply, reaction can be carried out continuously, It solves the problems, such as to complete to generate after back reaction substance in organic reaction and shifts that cumbersome, to easily lead to final product impure.
Detailed description of the invention
In order to illustrate the embodiment of the utility model or the technical proposal in the existing technology more clearly, below will be to embodiment Or attached drawing needed to be used in the description of the prior art is briefly described, it should be apparent that, the accompanying drawings in the following description is Some embodiments of the utility model, for those of ordinary skill in the art, in the premise of not making the creative labor property Under, it is also possible to obtain other drawings based on these drawings.
Fig. 1 be one kind provided by the utility model can successive reaction chemical reaction equipment structural schematic diagram;
Fig. 2 is the structural schematic diagram in fluid-through tube road and fastener in Fig. 1;
Fig. 3 is the structural schematic diagram in fluid-through tube road in Fig. 1.
Appended drawing reference:
10 reaction vessel, 11 electric heating cover, 12 conveying mouth
13 blender, 14 stirring motor, 20 fluid-through tube road
21 first 22 second fluid-through tube road of fluid-through tube road, 23 fastener
231 right 24 first solenoid valves of fastening block of left fastening block 232
30 vacuum pipe, 31 second solenoid valve, 41 display screen
42 control buttons
Specific embodiment
It is practical new below in conjunction with this to keep the objectives, technical solutions, and advantages of the embodiments of the present invention clearer Attached drawing in type embodiment, the technical scheme in the utility model embodiment is clearly and completely described, it is clear that is retouched The embodiment stated is the utility model a part of the embodiment, instead of all the embodiments.Based on the implementation in the utility model Example, every other embodiment obtained by those of ordinary skill in the art without making creative efforts belong to The range of the utility model protection.
In the description of the present invention, it should be noted that term " center ", " longitudinal direction ", " transverse direction ", "upper", "lower", The orientation or positional relationship of the instructions such as "front", "rear", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outside" is It is based on the orientation or positional relationship shown in the drawings, is merely for convenience of describing the present invention and simplifying the description, rather than indicate Or imply that signified device or element must have a particular orientation, be constructed and operated in a specific orientation, therefore cannot understand For limitations of the present invention.In addition, term " first ", " second " are used for description purposes only, and should not be understood as instruction or Imply relative importance.
Fig. 1 be one kind provided by the utility model can successive reaction chemical reaction equipment structural schematic diagram, such as Fig. 1 institute Show, including symmetrically arranged reaction vessel 10, fluid-through tube road 20 is equipped in the corresponding position of the reaction vessel 10, described Reaction vessel 10 is equipped with vacuum pipe 30, is respectively equipped with the first solenoid valve on the fluid-through tube road 20 and the vacuum pipe 30 24 and second solenoid valve 31;The fluid-through tube road 20 divides to be led to for the first fluid-through tube road 21 and the second fluid-through tube road 22, described first Liquid pipe road 21 and the second fluid-through tube road 22 pass through the closing connection of fastener 23;The vacuum pipe 30 is connected to vacuum pump;It is described First solenoid valve 24, second solenoid valve 31 and the vacuum pump and controller are electrically connected.
When it is implemented, as shown in Figure 1, the reaction vessel 10 in left side is chemically reacted first, in chemical reaction completion Afterwards, the second solenoid valve 31 of right side reaction vessel 10 is opened, and opens vacuum pump, is held by the reaction on 30 pairs of right sides of vacuum pipe Device 10 is vacuumized, and when the reaction vessel 10 on right side is in negative pressure state, closes the second electromagnetism of right side reaction vessel 10 Valve 31, and the first solenoid valve 24 is opened, enable fluid-through tube road 20 be connected to, the reactive material in the reaction vessel 10 in left side can quilt at this time It extracts into the reaction vessel on right side, after reactive material extracts, closes the first solenoid valve 24, fastener 23 is unloaded, The reaction vessel 10 for taking out left side is cleaned, and fastener 23 is reused after cleaning by the fluid-through tube road of two reaction vessels 20 closed communications, to generation substance transfer next time.
As shown in figure 3, the reaction vessel 10 in left side is connected to the first fluid-through tube road 21, the reaction vessel 10 on right side and second Fluid-through tube road 22 is connected to.
Controller is used to control the running of the first solenoid valve 24, second solenoid valve 31 and vacuum pump.
One kind provided by the utility model can successive reaction chemical reaction equipment, have structure design it is simple, can be continuous The advantages of being reacted solves and generates that substance transfer is cumbersome, it is final to easily lead to after completing back reaction in organic reaction The impure problem of product.
Preferably, the fastener 23 is formed by having magnetic left fastening block 231 and right fastening block 232, described left tight Gu block 231 and right fastening block 232 seal the nozzle in first fluid-through tube road 21 and the second fluid-through tube road 22 after mutual absorption Closure is enclosed.
When it is implemented, first is logical as shown in Fig. 2, left fastening block 231 and right fastening block 232 are by magnetic mutually absorption It is coated after alignment by fastener 23 at the nozzle in liquid pipe road 21 and the second fluid-through tube road 22, to make 21 He of the first fluid-through tube road The connection of second fluid-through tube road 22.
Preferably, the first solenoid valve 24, institute are designed on first fluid-through tube road 21 and second fluid-through tube road 22 State instruction control first fluid-through tube road 21 and second fluid-through tube road 22 that the first solenoid valve 24 receives the controller Connection and closing.
When it is implemented, as shown in figure 3, two the first solenoid valves 24 are separately positioned on the first fluid-through tube road 21 and second logical On liquid pipe road 22, two the first solenoid valves 24 are all electrically connected with controller, enable the first fluid-through tube road by the instruction of controller 21 are in the second fluid-through tube road 22 and are connected to or closed state.
Preferably, the bottom and side of the reaction vessel 10 are additionally provided with electric heating cover 11, the electric heating cover 11 and institute State controller electric connection.
When it is implemented, as shown in Figure 1, electric heating cover 11 coats the bottom and side of the reaction vessel 10, after energization It is controlled using temperature of the controller to electric heating cover 11, makes the reaction temperature controllable state in reaction vessel 10.
Preferably, the side of the reaction vessel 10 is equipped with conveying mouth 12.
When it is implemented, can pass through conveying mouth 12 will as shown in Figure 1, the side of reaction vessel 10 is arranged in conveying mouth 12 Reaction raw materials are passed through in reaction vessel 10, or the residue after reaction is poured out by conveying mouth 12.
Preferably, it is equipped with blender 13 in the reaction vessel 10, the blender 13 is by being located at the reaction vessel The stirring motor 14 at 10 tops drives, and the stirring motor 14 is connect with the controller.
When it is implemented, as shown in Figure 1, blender 13 is driven by stirring motor 14, to the reaction in reaction vessel 10 Liquid is stirred, and stirring motor 14 and controller are electrically connected, and the slewing rate of stirring motor 14 is controlled by controller.
It preferably, further include pedestal, the reaction vessel 10 is set on the base, is equipped with display screen on the base 41 and control button 42, the display screen 41 and the control button 42 and the controller are electrically connected.
When it is implemented, pedestal is that reaction vessel 10 is provided at support as shown in Figure 1, reaction vessel 10 is located on pedestal, Display screen 41 and control button 42 are set on the base, and are all electrically connected with controller, and display screen 41 can show electric heating cover 11 current temperature, control button 42 can control the first solenoid valve 24, second solenoid valve 31, electric heating cover 11, stirring motor 14 Operating.
Although herein more has used such as reaction vessel, electric heating cover, conveying mouth, blender, stirring motor, has led to The terms such as liquid pipe road, fastener, fastening block, solenoid valve, vacuum pipe, display screen, control button, but be not precluded using other A possibility that term.The use of these terms is merely for the convenience of describing and explaining the nature of the invention;Them It is contrary to the spirit of the present invention for being construed to any additional limitation all.
Finally, it should be noted that the above various embodiments is only to illustrate the technical solution of the utility model, rather than it is limited System;Although the present invention has been described in detail with reference to the aforementioned embodiments, those skilled in the art should Understand: it is still possible to modify the technical solutions described in the foregoing embodiments, or to some or all of Technical characteristic is equivalently replaced;And these are modified or replaceed, it does not separate the essence of the corresponding technical solution, and this is practical new The range of each embodiment technical solution of type.

Claims (7)

1. one kind can successive reaction chemical reaction equipment, it is characterised in that: including symmetrically arranged reaction vessel (10), in institute The corresponding position of reaction vessel (10) is stated equipped with fluid-through tube road (20), vacuum pipe is equipped on the reaction vessel (10) (30), the first solenoid valve (24) and second solenoid valve are respectively equipped on the fluid-through tube road (20) and the vacuum pipe (30) (31);
The fluid-through tube road (20) is divided into the first fluid-through tube road (21) and the second fluid-through tube road (22), first fluid-through tube road (21) and the second fluid-through tube road (22) passes through fastener (23) closing connection;
The vacuum pipe (30) is connected to vacuum pump;
First solenoid valve (24), second solenoid valve (31) and the vacuum pump and controller are electrically connected.
2. one kind according to claim 1 can successive reaction chemical reaction equipment, it is characterised in that: the fastener (23) it is formed by having magnetic left fastening block (231) and right fastening block (232), the left fastening block (231) and right fastening block (232) nozzle in first fluid-through tube road (21) and the second fluid-through tube road (22) is closed after mutual absorption and is surrounded.
3. one kind according to claim 1 can successive reaction chemical reaction equipment, it is characterised in that: the first logical liquid It is designed with the first solenoid valve (24) on pipeline (21) and second fluid-through tube road (22), first solenoid valve (24) receives institute State the connection and closing of instruction control first fluid-through tube road (21) and second fluid-through tube road (22) of controller.
4. one kind according to claim 3 can successive reaction chemical reaction equipment, it is characterised in that: the reaction vessel (10) bottom and side is additionally provided with electric heating cover (11), and the electric heating cover (11) and the controller are electrically connected.
5. one kind according to claim 1 can successive reaction chemical reaction equipment, it is characterised in that: the reaction vessel (10) side is equipped with conveying mouth (12).
6. one kind according to claim 4 can successive reaction chemical reaction equipment, it is characterised in that: the reaction vessel (10) blender (13) are equipped in, the blender (13) passes through the stirring motor (14) that is located at the top of the reaction vessel (10) Driving, the stirring motor (14) connect with the controller.
7. one kind according to claim 6 can successive reaction chemical reaction equipment, it is characterised in that: further include pedestal, The reaction vessel (10) sets on the base, is equipped with display screen (41) and control button (42) on the base, described Display screen (41) and the control button (42) and the controller are electrically connected.
CN201820942821.0U 2018-06-19 2018-06-19 It is a kind of can successive reaction chemical reaction equipment Active CN208612442U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201820942821.0U CN208612442U (en) 2018-06-19 2018-06-19 It is a kind of can successive reaction chemical reaction equipment

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201820942821.0U CN208612442U (en) 2018-06-19 2018-06-19 It is a kind of can successive reaction chemical reaction equipment

Publications (1)

Publication Number Publication Date
CN208612442U true CN208612442U (en) 2019-03-19

Family

ID=65703152

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201820942821.0U Active CN208612442U (en) 2018-06-19 2018-06-19 It is a kind of can successive reaction chemical reaction equipment

Country Status (1)

Country Link
CN (1) CN208612442U (en)

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