CN208517500U - A kind of high-temperature vacuum distillation titanium sponge fused salt separator - Google Patents
A kind of high-temperature vacuum distillation titanium sponge fused salt separator Download PDFInfo
- Publication number
- CN208517500U CN208517500U CN201821244949.6U CN201821244949U CN208517500U CN 208517500 U CN208517500 U CN 208517500U CN 201821244949 U CN201821244949 U CN 201821244949U CN 208517500 U CN208517500 U CN 208517500U
- Authority
- CN
- China
- Prior art keywords
- pipeline
- distillation
- fused salt
- alembic
- vacuum pump
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Landscapes
- Manufacture And Refinement Of Metals (AREA)
Abstract
The utility model discloses a kind of high-temperature vacuum distillation titanium sponge fused salt separators, including heating device, distill pipeline vacuum pump unit and distillation pipeline, the alembic that the distillation pipeline is sequentially communicated, output channel, cooling device, guide pipeline and main rewinding tank, the heating device heats alembic, the distillation pipeline vacuum pump unit is connected to the side on the side wall of guide pipeline close to main rewinding tank, and the fluid inside alembic is passed sequentially through output channel by distillation pipeline vacuum pump unit, cooling device and the extraction of guide pipeline, solid in cooling device passes through guide pipeline under the effect of gravity and enters main rewinding tank.The not only simplified equipment overall structure of the utility model reduces its occupied space, also simplifies separating step, improves separative efficiency, and separates titanium sponge fused salt without a large amount of water, while so very big that improve sponge titanium recovery rate.
Description
Technical field
The utility model relates to the vanadium titanium field of metallurgy in chemical field, and in particular to a kind of high-temperature vacuum distillation titanium sponge
Fused salt separator.
Background technique
Titanium sponge fused salt separation method mainly uses aqueous dissolution partition method, used separator structure at present
As shown in Figure 1.The titanium sponge fused salt separation process of this separator is as follows: fused salt (NaCl, KCl, CaCl2) and titanium sponge is mixed
It closes object to fall into first order knockout drum by the entrance of first order knockout drum, then start water pump and opens the first valve, will store up
Water in pond is input in first order knockout drum by corresponding water inlet, and dissolving fused salt therein sufficiently, (water must be omited
Greater than the amount of fused salt saturation solubility), then start stirring motor, drive rabbling mechanism, with to salt unsaturation lysate with
Titanium sponge mixed liquor is stirred, and is kept its fully dispersed, is then precipitated.Under the effect of gravity, the sponge in first order knockout drum
Titanium is precipitated to level-one knockout drum bottom, then opens the second valve, salt lysate is emitted into second level knockout drum, wherein suspending
Titanium sponge in salt lysate enters the second-order separation tank with lysate, into the salt lysate in the second-order separation tank
Titanium sponge is then deposited in the second-order separation pot bottom.Then third valve is opened, salt lysate is emitted into evaporator, then starting electricity
Heating system heats evaporator makes the water evaporation in evaporator enter discharge tube, twines on discharge tube to 125~150 DEG C
Around cooling water pipeline, the water vapour moved in discharge tube is then condensed into water, into tank, liquid in evaporator with
Moisture reduce, evaporation pot bottom formed crystal salt.Finally open the first discharging that first order knockout drum lower part discharge port goes out
The second discharge valve that valve and second level knockout drum lower part discharge port go out, collects titanium sponge.This separator has following lack
Point: 1. process cycle length, low efficiency, complex steps；2. sponge titanium recovery rate is lower, 90% or so can only be recycled, in fused salt knot
It is still detected in crystal and remains pars titanium；3. water consumption is big.
Utility model content
The utility model aim is to provide a kind of high-temperature vacuum distillation titanium sponge fused salt separator, solves titanium sponge and melt
The step of salt separator separation titanium sponge fused salt, is cumbersome, time-consuming, low efficiency, water consumption are big and sponge titanium recovery rate is low
Problem.Therefore the utility model designs a kind of high-temperature vacuum distillation titanium sponge fused salt separator, is realizing that simplified equipment is whole
It on the basis of body structure, also achieves simplified separating step, improve separative efficiency, without water, and very big must improve
Sponge titanium recovery rate.
The utility model is achieved through the following technical solutions:
A kind of high-temperature vacuum distillation titanium sponge fused salt separator, including heating device, distillation pipeline vacuum pump unit and
Distill pipeline, alembic, output channel, cooling device, guide pipeline and the main rewinding tank that the distillation pipeline is sequentially communicated, institute
It states heating device to heat alembic, close to main rewinding on the side wall of the distillation pipeline vacuum pump unit and guide pipeline
The side of tank is connected to, and distills pipeline vacuum pump unit and the fluid inside alembic is passed sequentially through output channel, cooling device
It is extracted out with guide pipeline, the solid in cooling device passes through guide pipeline under the effect of gravity and enters main rewinding tank.
Distillation tray equipped with fused salt and titanium sponge mixed powder is placed in alembic, is first opened each in distillation pipeline
Valve, starting distill pipeline vacuum pump unit, are vacuumized in alembic, make alembic vacuum degree in cold conditions 1 × 10- 4Pa~1 × 10-2Pa, 1 × 10 when distillation-2Pa~1000Pa then starts heating device, carries out heat temperature raising to alembic, makes
Material in alembic then evaporates fused salt up to 800 DEG C~1150 DEG C, becomes fused salt steam and enters cooling device, and
Solid granulates are condensed into cooling device, and main rewinding tank is then entered by guide pipeline under the effect of gravity power.
Heating device can be common high using the industry such as electric heating equipment, gas heating equipment, microwave heating equipment, boiler
Warm heating device carries out the heating of alembic.Cooling device can be using the common refrigeration of the industry such as condenser, heat exchanger, refrigeration machine
Device.
Cooling device condenses fused salt steam, it is quickly become solid-state from gaseous state, is condensed into solid-state fused salt particle, and
Under gravity, entered in main rewinding tank by guide pipeline.
The boiling point of fused salt is 600 DEG C or so, and alembic heats the fused salt and titanium sponge mixed powder stored in the inner, will
Its boiling point for being heated above fused salt and the boiling point for being lower than titanium sponge, when temperature is higher than fused salt boiling point, fused salt evaporates.It is steaming
Under the action of evaporating pipeline vacuum pump assembly, distill alembic quickly to fused salt under vacuum, so that fused salt becomes rapidly from solid-state
For liquid, and eventually become gaseous state.Under the vacuum environment that distillation pipeline vacuum pump unit is formed, it is quick to become gaseous fused salt
Into output channel.It is 3287 DEG C, in 800~1150 DEG C of temperature since titanium sponge boiling point is high for fused salt
Under, titanium is still solid-state.Therefore after being evaporated by fused salt, titanium sponge is still remained in alembic.
The designed a kind of high-temperature vacuum distillation titanium sponge fused salt separator out of the utility model, by vacuum high-temperature
Get off and distills titanium sponge fused salt, so that fused salt rapid evaporation and titanium sponge keep ortho states to be located at the bottom of alembic, after
And realize the quick separating of titanium sponge fused salt.The separation equipment that the utility model is redesigned, it is relatively existing on the whole
For separation equipment, not only simplifies equipment overall structure, reduces its occupied space, also simplify separating step, mention
High separative efficiency, and titanium sponge fused salt is separated without a large amount of water, while so very big that improve sponge titanium recovery rate.
Further, a kind of high-temperature vacuum distillation titanium sponge fused salt separator of the utility model, further includes vacuum line,
The vacuum management includes the heating device vacuum pump and guide pipeline being sequentially communicated, and the alembic is located at adding for heating device
In hot chamber, and the open end of alembic be pierced by heating device after be connected to output channel, on output channel far from cooling device
One end is fixed on the top of heating device by flange seal component, and confined space is formed between heating chamber and alembic, described
One end on guide pipeline far from heating device vacuum pump is connected to from the bottom of heating device with confined space, the heating device
Vacuum pump is extracted out the gas in confined space by guide pipeline.
Pipeline vacuum pump unit is distilled in starting, while by being vacuumized in alembic, starts heating device vacuum
Pump makes in the heating chamber of heating device vacuum degree up to 1.0 × 10-1Pa~1000Pa, with cooperate the vacuum degree 1.0 of alembic ×
10-2Pa~1.0 × 1000Pa.
Heating device vacuum pump makes alembic work under high-temperature vacuum, is on the one hand to reduce the oxygen of distillation tank wall
On the other hand change degree then reduces alembic inside and outside differential pressure, guarantees the quality of alembic.
Further, the whirlwind point being sequentially communicated is provided between the distillation pipeline vacuum pump unit and guide pipeline
From device and time rewinding tank, the feed end of the cyclone separator is connected to by the first connecting pipe with guide pipeline, cyclonic separation
The gas vent of device is connected to by the second connecting pipe with distillation pipeline vacuum pump unit, the solid particle outlet of cyclone separator
It is connected to secondary rewinding tank, the solid particle that cyclone separator is isolated is fallen into time rewinding tank from its outlet under the effect of gravity.
The solid particle condensed in condensing unit is ultra-fine grain, as air-flow is in distillation pipeline vacuum pump unit
Vacuum pump under the action of, cyclone separator, centrifugal force of the ultra-fine grain in cyclone separator are entered by the first connecting pipe
Under effect, inner wall collision friction with ultra-fine grain, and under the effect of gravity, time rewinding tank is fallen into, and in cyclone separator
Gas then passes sequentially through the gas vent of cyclone separator, the second connecting pipe and distillation pipeline vacuum pump unit and allots, into
It realizes to one step that solid gas separates, the ultra-fine grain fused salt in air is collected.
Further, the gas being sequentially communicated is provided between second connecting pipe and distillation pipeline vacuum pump unit
Body filter and conduit assembly, one end in the second connecting pipe far from cyclone separator are connected to the arrival end of filter, institute
The outlet end for stating filter is connected to by conduit assembly with distillation pipeline vacuum pump unit, and filter will be from cyclone separator
Remaining fused salt in gas filters out.
Contain ultrafine dust fused salt particle in the gas that cyclone separator is sent out, directly passes through distillation pipeline vacuum pump machine
When the vacuum pump extraction of group, it can be attached on pump leaf, and corrode pump leaf.Therefore ultra-fine to being completely separated by cyclone separator
Particle fused salt is filtered, and prevents ultrafine dust fused salt from entering distillation pipeline vacuum pump unit.
Further, the conduit assembly includes sequentially connected upper pipeline, bellows and lower pipeline, the outlet of filter
End passes sequentially through pipeline, bellows and lower pipeline and is connected to distillation pipeline vacuum pump unit.
Due to the pipeline group in actual arrangement all parts, pipeline, between filter and distillation pipeline vacuum pump unit
Part length is larger, and when bringing pipeline to fluctuate because of air flowing, the extreme magnitude of one end vibration of pipeline then causes pipeline to shake
Dynamic severity can generate great stress in intermediate position on pipeline, and long-time service is got off, and it is larger from meeting with stresses to will lead to pipeline
Position fracture, being smoothly detached for titanium sponge fused salt is influenced, therefore the biggish pipeline of length is changed to conduit assembly, in centre
Bellows is set, so as to reduce stress by the deformation of bellows when pipe vibration, then guarantees the smooth of titanium sponge fused salt
Separation.
To sum up, the specific separating process of the utility model: at 800 DEG C~1200 DEG C of high temperature, vacuum degree 5 × 10-1~1
×10-2High-temperature vacuum distillation is carried out under the conditions of Pa.In such circumstances, fused salt fast vaporizing evaporates, in distillation pipeline vacuum pump
Under the action of unit vacuumizes, rapidly with disengaging mixed melting object surface under airflow function, into cooling device, rapid condensation
At solid powder；Multiple fused salt collection is carried out by main rewinding tank, secondary rewinding tank.Tail gas is true by filter device, distillation pipeline
Empty pump assembly exhaust outlet discharge.Titanium sponge is then retained among alembic, and after furnace temperature is cooling, product sea is taken out in alembic
Continuous titanium takes out fused salt powder in collector, that is, efficiently accomplishes the separation of rate titanium sponge and fused salt.
The utility model compared with prior art, has the following advantages and benefits:
1, a kind of high-temperature vacuum distillation titanium sponge fused salt separator of the utility model, on the whole relatively existing separation
For equipment, not only simplifies equipment overall structure, reduces its occupied space, also simplify separating step, improve
Separative efficiency, and titanium sponge fused salt is separated without a large amount of water, while so very big that improve sponge titanium recovery rate；
2, a kind of high-temperature vacuum distillation titanium sponge fused salt separator of the utility model, heating device vacuum pump make alembic
It works under high-temperature vacuum, is on the one hand to reduce the degree of oxidation of distillation tank wall, on the other hand then reduce in alembic
External differential guarantees the quality of alembic；
3, a kind of high-temperature vacuum distillation titanium sponge fused salt separator of the utility model, the solid condensed in condensing unit
Particle is ultra-fine grain, as air-flow is under the action of distilling the vacuum pump in pipeline vacuum pump unit, passes through the first connection
Pipeline enters cyclone separator, and under the centrifugal force effect of cyclone separator, the inner wall collision with ultra-fine grain rubs ultra-fine grain
It wipes, and under the effect of gravity, falls into time rewinding tank, and the gas in cyclone separator then passes sequentially through the gas of cyclone separator
Outlet, the second connecting pipe and distillation pipeline vacuum pump unit are allotted, and further realize solid gas separation, will be super in air
Fine grained fused salt collects；
4, a kind of high-temperature vacuum distillation titanium sponge fused salt separator of the utility model, the biggish pipeline of length is changed to
Bellows is arranged in centre, so as to reduce stress by the deformation of bellows when pipe vibration, then guarantee in conduit assembly
Titanium sponge fused salt is smoothly detached.
Detailed description of the invention
Attached drawing described herein is used to provide to further understand the utility model embodiment, constitutes the one of the application
Part does not constitute the restriction to the utility model embodiment.In the accompanying drawings:
Fig. 1 is the structural schematic diagram of the prior art；
The structural schematic diagram of Fig. 2 the utility model；
The work flow diagram of Fig. 3 the utility model.
Label and corresponding parts title in attached drawing:
1a- first order knockout drum, 2a- water pump, the first valve of 3a-, 4a- blender, 5a- feed inlet, the second valve of 6a-,
The second level 7a- knockout drum, 8a- third valve, 9a- evaporator, 10a- discharge tube, 11a- cooling water pipeline, 12a- tank,
The first discharge valve of 13a-, the second discharge valve of 14a-；
1- heating device, 2- alembic, 3- output channel, 4- cooling device, the main rewinding tank of 5-, 6- distill pipeline vacuum pump
Unit, 7- guide pipeline, 8- heating device vacuum pump, 9- guide pipeline, 10- distillation pressure table, 11- pressure vacuum gauge, 12- times
Rewinding tank, 13- cyclone separator, the first connecting pipe of 14-, the second connecting pipe of 15-, 16- filter, the upper pipeline of 17-, 18-
Bellows, pipeline under 19-, 20- temperature thermocouple.
Specific embodiment
For the purpose of this utility model, technical solution and advantage is more clearly understood, below with reference to embodiment and attached drawing,
The utility model is described in further detail, and the exemplary embodiment and its explanation of the utility model are only used for explaining this
Utility model is not intended to limit the scope of the present invention.
Embodiment 1
In the present embodiment, heating device 1 uses heating tank, and cooling device 4 uses condenser.
As shown in Fig. 2-Fig. 3, a kind of high-temperature vacuum distillation titanium sponge fused salt separator of the utility model, including heating tank
1, pipeline vacuum pump unit 6 and distillation pipeline are distilled, it is described to distill alembic 2, the output channel 3, condensation that pipeline is sequentially communicated
Device 4, guide pipeline 7 and main rewinding tank 5, the heating tank 1 heat alembic 2, the distillation pipeline vacuum pump unit 6
It is connected to the side on the side wall of guide pipeline 7 close to main rewinding tank 5, and distilling pipeline vacuum pump unit 6 will be inside alembic 2
Fluid pass sequentially through output channel 3, condenser 4 and guide pipeline 7 are extracted out, the solid in condenser 4 is in gravity
Main rewinding tank 5 is entered by guide pipeline 7 down.
Distillation tray equipped with fused salt and titanium sponge mixed powder is placed in alembic, is first opened each in distillation pipeline
Valve, starting distillation pipeline vacuum pump unit 6, is vacuumized in alembic 2, make alembic vacuum degree in cold conditions 1 ×
10-4Pa~1 × 10-2Pa, 1 × 10 when distillation-2Pa~1000Pa then starts heating tank 1, carries out heating to alembic 2 and rises
Temperature makes the material in alembic 2 up to 800 DEG C~1150 DEG C, then evaporates fused salt, becomes fused salt steam and enters condenser 4,
And solid granulates are condensed into condenser 4, main rewinding tank 5 is then entered by guide pipeline 7 under the effect of gravity power.
The boiling point of fused salt is 600 DEG C or so, and alembic heats the fused salt and titanium sponge mixed powder stored in the inner, will
Its boiling point for being heated above fused salt and the boiling point for being lower than titanium sponge, when temperature is higher than fused salt boiling point, fused salt evaporates.It is steaming
Under the action of evaporating pipeline vacuum pump assembly 6, distill alembic quickly to fused salt under vacuum, so that fused salt becomes rapidly from solid-state
For liquid, and eventually become gaseous state.Under the vacuum environment that distillation pipeline vacuum pump unit 6 is formed, it is fast to become gaseous fused salt
Speed enters output channel 3.It is 3287 DEG C, in 800~1150 DEG C of temperature since titanium sponge boiling point is high for fused salt
Under degree, titanium is still solid-state.Therefore after being evaporated by fused salt, titanium sponge is still remained in alembic.
The separating process being designed into the utility model: the quality in order to guarantee titanium sponge, to alembic cold conditions feelings
It is evacuated to change vacuum under condition: 1.0 × 10-4Pa~1.0 × 10-2Pa, at 800 DEG C~1200 DEG C of high temperature, distillation vacuum degree 1.0 ×
10-2High-temperature vacuum distillation is carried out under the conditions of Pa~1000Pa.In such circumstances, fused salt fast vaporizing evaporates, true in distillation pipeline
Under the action of empty pump assembly, rapidly with disengaging mixed melting object surface under airflow function, into condenser, rapid condensation Cheng Gu
State powder；By main rewinding tank, it is collected.The discharge of tail gas vacuum pump set exhaust outlet.Titanium sponge is then retained among alembic,
After furnace temperature is cooling, product titanium sponge is taken out in alembic, fused salt powder is taken out in main rewinding tank, that is, efficiently accomplishes rate sea
The separation of continuous titanium and fused salt.
The designed a kind of high-temperature vacuum distillation titanium sponge fused salt separator out of the utility model, by vacuum high-temperature
Get off and distills titanium sponge fused salt, so that fused salt rapid evaporation and titanium sponge keep ortho states to be located at the bottom of alembic 2, after
And realize the quick separating of titanium sponge fused salt.The separation equipment that the utility model is redesigned, it is relatively existing on the whole
For separation equipment, not only simplifies equipment overall structure, reduces its occupied space, also simplify separating step, mention
High separative efficiency, and titanium sponge fused salt is separated without a large amount of water, while so very big that improve sponge titanium recovery rate.
Embodiment 2
A kind of high-temperature vacuum distillation titanium sponge fused salt separator of the utility model, further includes vacuum line, the vacuum
Management includes the heating device vacuum pump 8 and guide pipeline 9 being sequentially communicated, and the alembic 2 is located at the heating chamber of heating tank 1
In, and the open end of alembic 2 be pierced by heating tank 1 after be connected to output channel 3, on output channel 3 far from condenser 4 one end
It is fixed on the top of heating device by flange seal component, forms confined space, the air guide between heating chamber and alembic 2
One end on pipeline 9 far from heating device vacuum pump 8 is connected to from the bottom of heating tank 1 with confined space, and the heating device is true
Sky pump 8 is extracted out the gas in confined space by guide pipeline 9.
Pipeline vacuum pump unit 6 is distilled in starting, while by being vacuumized in alembic 2, starting heating device is true
Sky pump 8, makes in the heating chamber of heating tank 1 vacuum degree up to 1.0 × 10-1Pa~1000Pa, with cooperate the vacuum degree 1 of alembic ×
10-2Pa~1000Pa.
Heating device vacuum pump 8 makes alembic 2 work under high-temperature vacuum, is on the one hand to reduce by 2 outer wall of alembic
Degree of oxidation, on the other hand then reduce by 2 inside and outside differential pressure of alembic, guarantee the quality of alembic 2.
Embodiment 3
The present embodiment is on the basis of embodiment 1, to supervise to the pressure for distilling pipeline and vacuum line in the utility model
Control, which is made, implements explanation.
As shown in Fig. 2, a kind of high-temperature vacuum distillation titanium sponge fused salt separator of the utility model, in the distillation pipeline
Middle access has distillation pressure table 10, and the distillation pressure table 10 can detect the pressure in distillation pipeline, access in vacuum line
There is pressure vacuum gauge 11, the pressure vacuum gauge can detect the pressure in vacuum line.
The setting of distillation pressure table 10 and pressure vacuum gauge 11 confirms in distillation pipeline and true convenient for relevant staff
Pressure information in blank pipe road more goes on smoothly conducive to the high temperature distillation separation of titanium sponge fused salt.
Embodiment 4
The present embodiment be on the basis of embodiment 1, in the utility model to by the air after cooling of condenser 4
The collection of ultra-fine grain, which is made, implements explanation.
As shown in Fig. 2, a kind of high-temperature vacuum distillation titanium sponge fused salt separator of the utility model, in the distillation pipeline
The cyclone separator 13 being sequentially communicated and time rewinding tank 12, the whirlwind point are provided between vacuum pump assembly 6 and guide pipeline 7
Feed end from device 13 is connected to by the first connecting pipe 14 with guide pipeline 7, and the gas vent of cyclone separator 13 passes through the
Two connecting pipes 15 are connected to distillation pipeline vacuum pump unit 6, solid particle outlet and time rewinding tank 12 of cyclone separator 13
Connection, the solid particle that cyclone separator 13 is isolated are fallen into time rewinding tank 12 from its outlet under the effect of gravity.
The solid particle condensed in condensing unit 4 is ultra-fine grain, as air-flow is in distillation pipeline vacuum pump unit 6
In vacuum pump under the action of, by the first connecting pipe 15 enter cyclone separator 13, ultra-fine grain is in cyclone separator 13
Centrifugal force effect under, the inner wall collision friction with ultra-fine grain, and under the effect of gravity falls into time rewinding tank 12, and whirlwind
It is true that gas in separator 13 then passes sequentially through the gas vent of cyclone separator 13, the second connecting pipe 15 and distillation pipeline
Empty pump assembly 6 is allotted, and further realizes solid gas separation, the ultra-fine grain fused salt in air is collected.
Embodiment 5
The present embodiment is on the basis of embodiment 1, to the air after separating in the utility model to cyclone separator 13
In ultrafine dust fused salt particle collection make implement explanation.
As shown in Fig. 2, a kind of high-temperature vacuum distillation titanium sponge fused salt separator of the utility model, in second connection
The pneumatic filter 16 and conduit assembly being sequentially communicated are provided between pipeline 15 and distillation pipeline vacuum pump unit 6, second connects
One end on adapter tube road 15 far from cyclone separator 13 is connected to the arrival end of filter 16, and the outlet end of the filter 16 is logical
Piping component is connected to distillation pipeline vacuum pump unit 6, and filter 16 is by the remaining in the gas from cyclone separator 13
Fused salt filters out.
Contain ultrafine dust fused salt particle in the gas that cyclone separator 13 is sent out, directly passes through distillation pipeline vacuum pump
When the vacuum pump extraction of unit 6, it can be attached on pump leaf, and corrode pump leaf.Therefore thoroughly divide by cyclone separator 13
It is filtered from ultrafine dust fused salt, prevents ultrafine dust fused salt from entering distillation pipeline vacuum pump unit 6.
Embodiment 6
The present embodiment is illustrated to the specific implementation structure of the conduit assembly in embodiment 5.
The conduit assembly includes sequentially connected upper pipeline 17, bellows 18 and lower pipeline 19, the outlet of filter 16
End passes sequentially through pipeline 17, bellows 18 and lower pipeline 19 and is connected to distillation pipeline vacuum pump unit 6.
Due to the pipeline in actual arrangement all parts, pipeline, between filter 16 and distillation pipeline vacuum pump unit 6
Length component is larger, and when bringing pipeline to fluctuate because of air flowing, the extreme magnitude of one end vibration of pipeline then leads to pipeline
Shake severe, great stress can be generated in intermediate position on pipeline, long-time service be got off, will lead to pipeline from meet with stresses compared with
Big position fracture, influences being smoothly detached for titanium sponge fused salt, therefore the biggish pipeline of length is changed to conduit assembly, in
Between bellows 18 is set, so as to reduce stress by the deformation of bellows 18 when pipe vibration, then guarantee titanium sponge fused salt
Be smoothly detached.
Embodiment 7
The present embodiment is to make implementing explanation to the monitoring temperature inside alembic 2.
A kind of high-temperature vacuum distillation titanium sponge fused salt separator of the utility model further includes the survey in access distillation pipeline
Galvanic couple 20 is warmed, the thermometric end of the temperature thermocouple 20 is located in alembic 2 after passing through output channel 3, temperature thermocouple 20
Detect the temperature in alembic 2.
The setting of temperature thermocouple 20 is convenient for monitoring the temperature inside alembic 2 in real time, to guarantee that titanium sponge is molten
Salt separation is gone on smoothly.
Embodiment 8
Output channel 3 described in embodiment 1 is preferably utilidor.Utilidor guarantees the fused salt steam being evaporated
It is still steam state in this section.Especially when 3 length of output channel is larger, it is especially desirable to be set to utilidor to guarantee to manage
Temperature inside road, to guarantee that fused salt is in gaseous state.
Further, the condenser 4 is condenser.
Further, the heating tank 1 is heating tank.
Embodiment 9
The present embodiment is to carry out implementation explanation to the integritied monitoring and controling system of monitoring electronic device each in the utility model.
Distillation pressure table 10 and pressure vacuum gauge 11 are electronic pressure gage, distillation pressure table 10, pressure vacuum gauge 11 with
And temperature thermocouple 20 is connect with the control centre in monitoring system, the monitoring system further includes connecting with control centre
Display, warning device and wireless communication module, while monitoring center control distillation pipeline vacuum pump unit in pump drive
The working condition of dynamic motor, the driving motor of heating device vacuum pump, heating furnace, wherein distillation pressure table 10, pressure vacuum gauge
11 acquisition distillation pipelines, the pressure information in vacuum line respectively, and control centre is sent it to, temperature thermocouple 20 will be adopted
The temperature information inside alembic 2 collected is sent to control centre, and control centre receives to come from distillation pressure table 10, vacuum pressure
The information of power table 11 and temperature thermocouple 20, and it is shown by display, synchronizing will be upper by wireless communication module
It states information and sends mobile terminal.
Embodiment 10
The present embodiment is illustrated to the processing step of the specific separation titanium sponge fused salt of the utility model.
The processing step that the utility model separates titanium sponge fused salt is as follows:
Step A: fused salt and titanium sponge fused salt mixed powder are placed on distillation tray, distillation tray is then placed in alembic
In 2；
Step B: each valve in distillation pipeline is opened；
Step C: starting distillation pipeline vacuum pump unit 6 makes alembic vacuum degree up to 1 to vacuumizing in alembic 2
×10-2Pa~1000Pa；Start heating device vacuum pump 8 simultaneously, makes in the heating chamber of heating tank 1 vacuum degree up to 1.0 × 10- 1Pa~1000Pa；
Step D: then starting heating tank 1 and condenser 4, and heating tank 1 carries out heat temperature raising to alembic 2, makes alembic 2
Interior material then evaporates fused salt up to 800 DEG C~1150 DEG C, becomes fused salt steam and enters condenser 4, and in condenser 4
In condense into solid granulates, then gravity power effect under by guide pipeline 7 enter main rewinding tank 5；
Step E: the first connection is passed through under the action of distilling pipeline vacuum pump unit 6 by the condensed gas of condenser 4
Pipeline 14, which enters in cyclone separator 13, carries out gas, solid separation, and isolated solid enters time collecting tank 12, and isolated gas passes through
Second connecting pipe 15 enters filter 16, and is distilled pipeline vacuum pump assembly 6 after the filtering of filter 16 and extracts out.
Embodiment 11
The present embodiment is that the utility model is carried out the data comparison that titanium sponge fused salt separates with the prior art (Fig. 1) to say
It is bright.
The prior art and the utility model respectively separate the titanium sponge fused salt of same 100kg, obtain
Data are as follows:
In the prior art, the titanium sponge weight being collected into first order knockout drum 1a is 40~60, second level knockout drum 7a
In the titanium sponge weight that is collected into be 20~30kg, institute's water consumption is 5t.
In the present invention, the titanium sponge weight being collected into alembic 2 is 96~99kg, and institute's water consumption is 1.5t.
Above-described specific embodiment, to the purpose of this utility model, technical scheme and beneficial effects carried out into
One step is described in detail, it should be understood that being not used to limit the foregoing is merely specific embodiment of the present utility model
Determine the protection scope of the utility model, within the spirit and principle of the utility model, any modification for being made equally is replaced
It changes, improve, should be included within the scope of protection of this utility model.
Claims (10)
1. a kind of high-temperature vacuum distillation titanium sponge fused salt separator, which is characterized in that including heating device (1), distillation pipeline
Vacuum pump assembly (6) and distillation pipeline, alembic (2), the output channel (3), cooling device that the distillation pipeline is sequentially communicated
(4), guide pipeline (7) and main rewinding tank (5), the heating device (1) heat alembic (2), the distillation pipeline
Vacuum pump assembly (6) is connected to the side on the side wall of guide pipeline (7) close to main rewinding tank (5), and distills pipeline vacuum pump
The internal fluid of alembic (2) is passed sequentially through output channel (3), cooling device (4) and guide pipeline (7) and extracted out by unit (6),
Solid in cooling device (4) passes through guide pipeline (7) under the effect of gravity and enters main rewinding tank (5).
2. a kind of high-temperature vacuum distillation titanium sponge fused salt separator according to claim 1, which is characterized in that further include
Vacuum line, the vacuum management include the heating device vacuum pump (8) and guide pipeline (9) being sequentially communicated, the alembic
(2) in the heating chamber of heating device (1), and the open end of alembic (2) is pierced by heating device (1) afterwards and output channel
(3) it is connected to, one end on output channel (3) far from cooling device (4) is fixed on the top of heating device by flange seal component
Confined space is formed between portion, heating chamber and alembic (2), on the guide pipeline (9) separate heating device vacuum pump (8)
One end is connected to from the bottom of heating device (1) with confined space, and the heating device vacuum pump (8) will by guide pipeline (9)
Gas extraction in confined space.
3. a kind of high-temperature vacuum distillation titanium sponge fused salt separator according to claim 2, which is characterized in that described
Accessing in distillation pipeline has distillation pressure table (10), and the distillation pressure table (10) can detect the pressure in distillation pipeline, true
Access has pressure vacuum gauge (11) in blank pipe road, and the pressure vacuum gauge can detect the pressure in vacuum line.
4. a kind of high-temperature vacuum distillation titanium sponge fused salt separator according to claim 1, which is characterized in that described
The cyclone separator (13) being sequentially communicated and time rewinding are provided between distillation pipeline vacuum pump unit (6) and guide pipeline (7)
The feed end of tank (12), the cyclone separator (13) is connected to by the first connecting pipe (14) with guide pipeline (7), whirlwind point
Gas vent from device (13) is connected to by the second connecting pipe (15) with distillation pipeline vacuum pump unit (6), cyclone separator
(13) solid particle outlet is connected to time rewinding tank (12), and the solid particle that cyclone separator (13) is isolated is in gravity
Under fallen into time rewinding tank (12) from its outlet.
5. a kind of high-temperature vacuum distillation titanium sponge fused salt separator according to claim 4, which is characterized in that described
The pneumatic filter (16) being sequentially communicated and pipe are provided between second connecting pipe (15) and distillation pipeline vacuum pump unit (6)
Road component, one end in the second connecting pipe (15) far from cyclone separator (13) are connected to the arrival end of filter (16), institute
The outlet end for stating filter (16) is connected to by conduit assembly with distillation pipeline vacuum pump unit (6).
6. a kind of high-temperature vacuum distillation titanium sponge fused salt separator according to claim 5, which is characterized in that the pipe
Road component includes sequentially connected upper pipeline (17), bellows (18) and lower pipeline (19), and the outlet end of filter (16) is successively
It is connected to by upper pipeline (17), bellows (18) and lower pipeline (19) with distillation pipeline vacuum pump unit (6).
7. a kind of high-temperature vacuum distillation titanium sponge fused salt separator according to claim 1 to 6, feature
It is, further includes the temperature thermocouple (20) in access distillation pipeline, the thermometric end of the temperature thermocouple (20) passes through output
Pipeline (3) is located in alembic (2) afterwards, and temperature thermocouple (20) detects the temperature in alembic (2).
8. a kind of high-temperature vacuum distillation titanium sponge fused salt separator according to claim 1 to 6, feature
It is, the output channel (3) is utilidor.
9. a kind of high-temperature vacuum distillation titanium sponge fused salt separator according to claim 1 to 6, feature
It is, the cooling device (4) is condenser.
10. a kind of high-temperature vacuum distillation titanium sponge fused salt separator according to claim 1, which is characterized in that described
Heating device (1) is heating tank.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821244949.6U CN208517500U (en) | 2018-08-02 | 2018-08-02 | A kind of high-temperature vacuum distillation titanium sponge fused salt separator |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821244949.6U CN208517500U (en) | 2018-08-02 | 2018-08-02 | A kind of high-temperature vacuum distillation titanium sponge fused salt separator |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN208517500U true CN208517500U (en) | 2019-02-19 |
Family
ID=65333339
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201821244949.6U Expired - Fee Related CN208517500U (en) | 2018-08-02 | 2018-08-02 | A kind of high-temperature vacuum distillation titanium sponge fused salt separator |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN208517500U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108690916A (en) * | 2018-08-02 | 2018-10-23 | 绵阳力洋英伦科技有限公司 | High temperature distillation separation equipment and separation method applied to titanium sponge fused salt |
-
2018
- 2018-08-02 CN CN201821244949.6U patent/CN208517500U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108690916A (en) * | 2018-08-02 | 2018-10-23 | 绵阳力洋英伦科技有限公司 | High temperature distillation separation equipment and separation method applied to titanium sponge fused salt |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103908788B (en) | MVR heat pump evaporation system | |
| CN104759108B (en) | Three grades of continuous falling liquid film circulating and evaporating concentration systems with function of mechanical steam recompression | |
| CN206596640U (en) | A kind of special concentration purifying plant of honey | |
| CN105817461B (en) | A kind of device of waste and old circuit board electronic component high added value recycling | |
| CN206103371U (en) | Spherical concentrator in vacuum | |
| CN208517500U (en) | A kind of high-temperature vacuum distillation titanium sponge fused salt separator | |
| CN206872430U (en) | A kind of air conditioner two-unit leak detection helium purifying retracting device based on UF membrane | |
| CN103143184A (en) | Distillation apparatus | |
| CN108690916A (en) | High temperature distillation separation equipment and separation method applied to titanium sponge fused salt | |
| CN201676624U (en) | Gas and oil separator | |
| CN204601640U (en) | A kind of outer circulation alcohol recovery system | |
| CN206281263U (en) | A kind of useless air-conditioning refrigerant reclaiming clean device | |
| CN205549612U (en) | Liquid treatment device | |
| CN105737457A (en) | Solvent recovery technology | |
| CN206372543U (en) | A kind of low-temperature negative-pressure purifying plant | |
| CN201164763Y (en) | Tconical baffler foam destroyer | |
| CN212091528U (en) | Tail gas emission and purification system for aluminum liquid processing | |
| CN209271101U (en) | A kind of cooling gas-liquid separator | |
| CN105582685B (en) | Liquid treatment equipment | |
| CN109340851A (en) | A kind of kitchen ventilation oil removing and residual neat recovering system | |
| CN205659427U (en) | Distilling Recycle system of silicon chip cutting oil | |
| CN218248517U (en) | Recycling system of condensed water in evaporator | |
| CN212339996U (en) | Steam condensing tank of oil-water separation system | |
| CN116062825B (en) | High-salt wastewater salt extraction device | |
| CN219983916U (en) | Solvent recycling machine |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20190219 Termination date: 20190802 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |