CN208494196U - The experimental provision and equipment of concentration of lye and dosage to TBC and ATBC neutralization - Google Patents
The experimental provision and equipment of concentration of lye and dosage to TBC and ATBC neutralization Download PDFInfo
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- CN208494196U CN208494196U CN201820877917.3U CN201820877917U CN208494196U CN 208494196 U CN208494196 U CN 208494196U CN 201820877917 U CN201820877917 U CN 201820877917U CN 208494196 U CN208494196 U CN 208494196U
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Abstract
The utility model discloses concentration of lye and dosages to the experimental provision and equipment of TBC and ATBC neutralization, including metal can and fixed cover, the fixed cover is fixed on the upper end position of metal can, pass through grafting ring, when fixed cover composed by annulus block and intermediate inserted block is fixed, intermediate inserted block on the middle position of fixed cover lower end will be plugged and fixed in metal can inside, and the grafting ring of fixed cover lower end will be fixed in the recess of metal can upper end, pass through the isolation of grafting ring and intermediate inserted block in this way, to reduce external test interference.It is more convenient when fixed external connecting pipe by fixed connection device composed by fixing bolt, metal outer ring, semicircular ring and intermediate inner ring, external connecting pipe need to be only plugged between semicircular ring and intermediate inner ring, to pass through fixing bolt threaded rotational movement, so that semicircular ring declines, to fix external connecting pipe.
Description
Technical field
The utility model belongs to related citrate technical field, and in particular to concentration of lye and dosage are to TBC and ATBC
The experimental provision and equipment of neutralization.
Background technique
Two principal item tributyl citrate (TBC) of citrate, tributyl 2-acetylcitrate (ATBC) have obtained
U.S. FDA approval is used as safe and nontoxic plasticizer, and China also suggests using in packaging material.And to tributyl citrate
(TBC), when tributyl 2-acetylcitrate (ATBC) carries out concentration of lye and the test of dosage neutralization, it is necessary to use one
Fixed equipment carries out neutralization reaction.
Existing citrate effect test equipment and technology has the following problems: 1, existing citrate effect test is set
Standby leakage fluid dram very easily cannot be attached fixation with external rubber tube, thus it is more troublesome when fixed use,
Testing crew is not very convenient when being fixedly mounted in this way.2, the metal top cover of existing citrate effect test equipment
When fixing seal be not it is very close, in this way when carrying out concentration of lye and dosage neutralization is tested, be easy because
It is outside air to influence test result.
Utility model content
The purpose of this utility model is to provide concentration of lye and dosages to the experimental provision of TBC and ATBC neutralization and
Equipment, cannot be very easily to solve the leakage fluid dram of existing citrate effect test equipment mentioned above in the background art
It is attached fixation with external rubber tube, thus more troublesome when fixed use, such testing crew is being fixedly mounted
When not very convenient and existing citrate effect test equipment metal top cover be not very when fixing seal
Closely, it in this way when carrying out concentration of lye and dosage neutralization is tested, is easy because outside air is to influence to test
As a result the problem of.
To achieve the above object, the utility model provides the following technical solutions:
Concentration of lye and dosage are to the experimental provision and equipment of TBC and ATBC neutralization, including metal can and fixation
Upper cover, the fixed cover are fixed on the upper end position of metal can, and the upper end of the fixed cover is connected with
Fixed hanging ring block, the fixed hanging ring block are fixedly connected by way of being welded and fixed with fixed cover, the metal can
It is connected with acid esters import above left end, the acid esters import is fixedly connected by way of being welded and fixed with metal can,
It is connected with lye import above the right end of the metal can, the lye import and metal can, which pass through, to be welded and fixed
Mode is fixedly connected, and observation panel, the left end of the metal can are connected on the front end middle position of the metal can
Lower section is connected with rotary electric machine, and the front end of the rotary electric machine, which is located inside metal can, is connected with metal stirring
It is solid by welding to be connected with control valve, the control valve and metal can among the lower end of the metal can for bar
Fixed mode is fixedly connected, and the lower end of the control valve is connected with fixed connection device, the fixed connection device and control
Valve is fixedly connected by way of being welded and fixed, and the surrounding of the fixed connection device, which is located on metal can lower end, connects setting
There is fixing leg, the fixing leg is fixedly connected by way of being welded and fixed with metal can, under the fixing leg
End is connected with firm banking, and the fixing leg is fixedly connected by way of being welded and fixed with firm banking, and described turn
Dynamic motor and external power supply are electrically connected.
Preferably, the fixed connection device includes fixing bolt, metal outer ring, semicircular ring and intermediate inner ring, the metal
Grafting is provided with fixing bolt among the both ends of outer ring, and the lower end of the fixing bolt, which is located in metal outer ring, is provided with semicircle
Ring, the centre of the semicircular ring, which is located on metal outer ring, is connected with intermediate inner ring, and the metal outer ring is connected to control valve
Men Shang.
Preferably, the fixed cover includes grafting ring, annulus block and intermediate inserted block, is set among the lower end of the annulus block
It is equipped with intermediate inserted block, the surrounding of the intermediate inserted block, which is located on annulus block, is connected with grafting ring.
Preferably, the metal stirring rod includes threaded block, intermediolateral column, fixed screw and paddle, the threaded block
Lower end is connected with intermediolateral column, and the lower end socket of the intermediolateral column is provided with paddle, and the paddle passes through fixed screw
It is fixedly connected on intermediolateral column, the threaded block is connected on rotary electric machine.
Preferably, there are four the fixing leg is arranged altogether, and the fixing leg is weldingly fixed on metal can in parallel
On the lower end of body.
Preferably, the observation panel is circular shape, and the centre of the observation panel is provided with tempered glass.
Preferably, the cylinder that the diameter of the metal can is 45 centimeters, and the maximum of the metal can holds
Amount is four decaliters.
Preferably, the rotary electric machine is fixed on indent below metal can left end by fixing screws.
Compared with prior art, the utility model provides concentration of lye and dosage to the reality of TBC and ATBC neutralization
Experiment device and equipment, have it is following the utility model has the advantages that
1, the utility model citrate effect test equipment passes through solid composed by grafting ring, annulus block and intermediate inserted block
It is even closer when fixed to determine upper cover, when fixed, the intermediate inserted block on the middle position of fixed cover lower end will be inserted
It connects and is fixed in metal can inside, and the grafting ring of fixed cover lower end will be fixed in the recess of metal can upper end,
In this way by the isolation of grafting ring and intermediate inserted block, to reduce external test interference, so that test is more accurate, and lead to
The isolation being plugged and fixed is crossed, thus also enhanced convenience when opening.
2, the utility model citrate effect test equipment passes through in fixing bolt, metal outer ring, semicircular ring and centre
Fixed connection device composed by ring is more convenient when fixed external connecting pipe, only external connecting pipe need to be plugged into semicircle
Between ring and intermediate inner ring, so that intermediate inner ring is inserted into external connecting pipe inside, to revolve by fixing bolt screw thread
Transhipment is dynamic, so that semicircular ring declines, to fix external connecting pipe, is just more convenient for when fixed in this way.
Detailed description of the invention
Attached drawing is used to provide a further understanding of the present invention, and constitutes part of specification, practical with this
Novel embodiment is used to explain the utility model together, does not constitute limitations of the present invention, in the accompanying drawings:
Fig. 1 be the utility model proposes citrate effect test device structure schematic diagram;
Fig. 2 be the utility model proposes fixed connection device fixed structure schematic diagram;
Fig. 3 be the utility model proposes fixed cover structural schematic diagram;
Fig. 4 be the utility model proposes metal stirring rod structural schematic diagram;
In figure: 1, fixed hanging ring block;2, fixed cover;21, grafting ring;22, annulus block;23, intermediate inserted block;3, acid esters into
Mouthful;4, metal can;5, rotary electric machine;6, fixing leg;7, firm banking;8, lye import;9, observation panel;10, metal stirs
Mix bar;101, threaded block;102, intermediolateral column;103, fixed screw;104, paddle;11, control valve;12, fixed connection device;
121, fixing bolt;122, metal outer ring;123, semicircular ring;124, intermediate inner ring.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model
Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole
Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work
Every other embodiment obtained, fall within the protection scope of the utility model.
Fig. 1-4 is please referred to, the utility model provides a kind of technical solution:
Concentration of lye and dosage are to the experimental provision and equipment of TBC and ATBC neutralization, including metal can 4 and fixed
Upper cover 2, fixed cover 2 are fixed on the upper end position of metal can 4, and the upper end of fixed cover 2 is connected with fixation
Hanging ring block 1, fixed hanging ring block 1 is fixedly connected by way of being welded and fixed with fixed cover 2, above the left end of metal can 4
It is connected with acid esters import 3, acid esters import 3 is fixedly connected by way of being welded and fixed with metal can 4, metal can 4
Right end above be connected with lye import 8, lye import 8 is fixedly connected by way of being welded and fixed with metal can 4,
It is connected with observation panel 9 on the front end middle position of metal can 4, is connected with rotation below the left end of metal can 4
Motor 5, the front end of rotary electric machine 5, which is located inside metal can 4, is connected with metal stirring rod 10, the lower end of metal can 4
Centre is connected with control valve 11, and control valve 11 is fixedly connected by way of being welded and fixed with metal can 4, control
The lower end of valve 11 is connected with fixed connection device 12, and fixed connection device 12 and control valve 11 are by way of being welded and fixed
Be fixedly connected, the surrounding of fixed connection device 12, which is located on 4 lower end of metal can, is connected with fixing leg 6, fixing leg 6 with
Metal can 4 is fixedly connected by way of being welded and fixed, and the lower end of fixing leg 6 is connected with firm banking 7, fixed branch
Foot 6 is fixedly connected by way of being welded and fixed with firm banking 7, and rotary electric machine 5 and external power supply are electrically connected.
Further, fixed connection device 12 includes fixing bolt 121, metal outer ring 122, semicircular ring 123 and intermediate inner ring
124, the both ends centre grafting of metal outer ring 122 is provided with fixing bolt 121, and the lower end of fixing bolt 121 is located at metal outer ring
Semicircular ring 123 is provided in 122, the centre of semicircular ring 123, which is located on metal outer ring 122, is connected with intermediate inner ring 124, gold
Belong to outer ring 122 to be connected in control valve 11, so that fixed is more convenient, so that user of service is in connection external connecting pipe
When it is more convenient.
Further, fixed cover 2 includes grafting ring 21, annulus block 22 and intermediate inserted block 23, among the lower end of annulus block 22
It is provided with intermediate inserted block 23, the surrounding of intermediate inserted block 23, which is located on annulus block 22, is connected with grafting ring 21, avoids air
Entrance so that test result is more accurate, and also more convenient when fixed.
Further, metal stirring rod 10 includes threaded block 101, intermediolateral column 102, fixed screw 103 and paddle 104, spiral shell
The lower end of line block 101 is connected with intermediolateral column 102, and the lower end socket of intermediolateral column 102 is provided with paddle 104, paddle 104
It being fixedly connected on intermediolateral column 102 by fixed screw 103, threaded block 101 is connected on rotary electric machine 5, it can be stirred,
To accelerate internal reaction, reduce the time of waiting.
Further, there are four fixing leg 6 is arranged altogether, and fixing leg 6 is weldingly fixed under metal can 4 in parallel
On end, good supporting role is played, thus more stable when placing.
Further, observation panel 9 is circular shape, and the centre of observation panel 9 is provided with tempered glass, it may be convenient to be checked
Internal-response, so that personnel convenient to use carry out some simple experiment records.
Further, the cylinder that the diameter of metal can 4 is 45 centimeters, and the maximum capacity of metal can 4 is four
Decaliter has good storage effect, so as to meet the test reaction of different lye dosages.
Further, rotary electric machine 5 is fixed on indent below 4 left end of metal can by fixing screws, so that fixing more
Add conveniently, and when placing, too big blocking will not be caused.
The working principle and process for using of the utility model: after the utility model installs, so that it may be filled by carrying
It sets citrate effect test equipment to be moved on specified position and is placed, citrate effect test equipment passes through solid
Determine stabilizer blade 6 and firm banking 7, thus it is more convenient when placing, it places after completing, so that it may connect rotary electric machine 5
It connect with external power supply, acid esters import 3 and lye import 8 is being connected in citrate container and alkali liquor container respectively
In, after connecting, so that it may external connecting pipe be connected in fixed connection device 12, citrate effect test equipment passes through
Fixed connection device 12 composed by fixing bolt 121, metal outer ring 122, semicircular ring 123 and intermediate inner ring 124 is outside fixation
It is more convenient when connecting tube, external connecting pipe need to be only plugged between semicircular ring 123 and intermediate inner ring 124, so that in
Between inner ring 124 be inserted into external connecting pipe inside, thus by 121 threaded rotational movement of fixing bolt, so that half
Annulus 123 declines, to fix external connecting pipe, is just more convenient for when fixed in this way, later can basis
Research contents is tested, and provides buck concentration to acid esters import 3 and lye import 8 by lemon acid esters container and alkali liquor container
Difference, buck amount is identical to be reacted with TBC, and such solution will react in metal can 4, when reaction, is led to
Rotary electric machine 5 is crossed, so that metal stirring rod 10 be driven to rotate, to accelerate to react, after reaction is completed, opens control valve
11, so that the material of reaction is fallen in lower section connection container, to carry out record observation, when observation, so that it may pass through gold
Belong to the observation panel 9 among tank body 4 to be observed, complete after once testing, so that it may it opens fixed cover 2 and is cleaned, from
And used next time, citrate effect test equipment passes through 23 grafting ring 21, annulus block 22 and intermediate inserted block groups
At fixed cover 2 it is even closer when fixed, when fixed, on 2 lower end middle position of fixed cover in interleave
Block 23 will be plugged and fixed in 4 inside of metal can, and the grafting ring 21 of 2 lower end of fixed cover will be fixed on metal can
In the recess of 4 upper ends, in this way by the isolation of grafting ring 21 and intermediate inserted block 23, thus reduce external test interference, so that
It is more accurate to test, and by the isolation that is plugged and fixed, thus also enhanced convenience when opening, when opening,
Fixed hanging ring block 1 need to be only passed through with handling apparatus to be lifted by crane, so that it may very easily open, thus being cleared up, it
After closing afterwards, just identical with buck concentration levels, buck amount difference is reacted with TBC, after completion, in progress ATBC
Reaction record and observation.
While there has been shown and described that the embodiments of the present invention, for the ordinary skill in the art,
It is understood that these embodiments can be carried out with a variety of variations in the case where not departing from the principles of the present invention and spirit, repaired
Change, replacement and variant, the scope of the utility model is defined by the appended claims and the equivalents thereof.
Claims (8)
1. concentration of lye and dosage be to the experimental provision and equipment of TBC and ATBC neutralization, including metal can (4) and fixed
Upper cover (2), it is characterised in that: the fixed cover (2) is fixed on the upper end position of metal can (4), the fixation
The upper end of upper cover (2) is connected with fixed hanging ring block (1), and the fixed hanging ring block (1) and fixed cover (2) are solid by welding
Fixed mode is fixedly connected, and is connected with acid esters import (3) above the left end of the metal can (4), the acid esters import
(3) it is fixedly connected by way of being welded and fixed with metal can (4), connection setting above the right end of the metal can (4)
Have lye import (8), the lye import (8) is fixedly connected by way of being welded and fixed with metal can (4), the metal
It is connected on the front end middle position of tank body (4) observation panel (9), connection setting below the left end of the metal can (4)
Have rotary electric machine (5), the front end of the rotary electric machine (5), which is located inside metal can (4), is connected with metal stirring rod
(10), it is connected with control valve (11) among the lower end of the metal can (4), the control valve (11) and metal can
Body (4) is fixedly connected by way of being welded and fixed, and the lower end of the control valve (11) is connected with fixed connection device
(12), the fixed connection device (12) is fixedly connected by way of being welded and fixed with control valve (11), described to be fixedly connected
The surrounding of device (12), which is located on metal can (4) lower end, to be connected with fixing leg (6), the fixing leg (6) and metal
Tank body (4) is fixedly connected by way of being welded and fixed, and the lower end of the fixing leg (6) is connected with firm banking (7),
The fixing leg (6) is fixedly connected by way of being welded and fixed with firm banking (7), the rotary electric machine (5) and outside
Power supply is electrically connected.
2. concentration of lye according to claim 1 and dosage be to the experimental provision and equipment of TBC and ATBC neutralization,
Be characterized in that: the fixed connection device (12) includes fixing bolt (121), metal outer ring (122), semicircular ring (123) and centre
The both ends centre grafting of inner ring (124), the metal outer ring (122) is provided with fixing bolt (121), the fixing bolt
(121) lower end, which is located in metal outer ring (122), to be provided with semicircular ring (123), and the centre of the semicircular ring (123) is located at metal
It is connected on outer ring (122) intermediate inner ring (124), the metal outer ring (122) is connected on control valve (11).
3. concentration of lye according to claim 1 and dosage be to the experimental provision and equipment of TBC and ATBC neutralization,
Be characterized in that: the fixed cover (2) includes grafting ring (21), annulus block (22) and intermediate inserted block (23), the annulus block
(22) it is provided among lower end intermediate inserted block (23), the surrounding of the intermediate inserted block (23), which is located to connect on annulus block (22), to be set
It is equipped with grafting ring (21).
4. concentration of lye according to claim 1 and dosage be to the experimental provision and equipment of TBC and ATBC neutralization,
Be characterized in that: the metal stirring rod (10) includes threaded block (101), intermediolateral column (102), fixed screw (103) and paddle
(104), the lower end of the threaded block (101) is connected with intermediolateral column (102), and the lower end socket of the intermediolateral column (102) is set
It is equipped with paddle (104), the paddle (104) is fixedly connected on intermediolateral column (102) by fixed screw (103), described
Threaded block (101) is connected on rotary electric machine (5).
5. concentration of lye according to claim 1 and dosage be to the experimental provision and equipment of TBC and ATBC neutralization,
Be characterized in that: there are four the fixing leg (6) is arranged altogether, and the fixing leg (6) is weldingly fixed on metal can in parallel
On the lower end of body (4).
6. concentration of lye according to claim 1 and dosage be to the experimental provision and equipment of TBC and ATBC neutralization,
Be characterized in that: the observation panel (9) is circular shape, and the centre of the observation panel (9) is provided with tempered glass.
7. concentration of lye according to claim 1 and dosage be to the experimental provision and equipment of TBC and ATBC neutralization,
It is characterized in that: the cylinder that the diameter of the metal can (4) is 45 centimeters, and the maximum of the metal can (4) holds
Amount is four decaliters.
8. concentration of lye according to claim 1 and dosage be to the experimental provision and equipment of TBC and ATBC neutralization,
Be characterized in that: the rotary electric machine (5) is fixed on indent below metal can (4) left end by fixing screws.
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CN201820877917.3U CN208494196U (en) | 2018-06-07 | 2018-06-07 | The experimental provision and equipment of concentration of lye and dosage to TBC and ATBC neutralization |
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CN201820877917.3U CN208494196U (en) | 2018-06-07 | 2018-06-07 | The experimental provision and equipment of concentration of lye and dosage to TBC and ATBC neutralization |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110327863A (en) * | 2019-07-19 | 2019-10-15 | 安徽尘缘节能环保科技有限公司 | A kind of efficient microwave acidolysis system accelerating the passivation of cyanobacteria toxicity |
-
2018
- 2018-06-07 CN CN201820877917.3U patent/CN208494196U/en active Active
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110327863A (en) * | 2019-07-19 | 2019-10-15 | 安徽尘缘节能环保科技有限公司 | A kind of efficient microwave acidolysis system accelerating the passivation of cyanobacteria toxicity |
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