CN208493251U - A kind of zoopery Rotary Evaporators - Google Patents

A kind of zoopery Rotary Evaporators Download PDF

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Publication number
CN208493251U
CN208493251U CN201820788409.8U CN201820788409U CN208493251U CN 208493251 U CN208493251 U CN 208493251U CN 201820788409 U CN201820788409 U CN 201820788409U CN 208493251 U CN208493251 U CN 208493251U
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bottle body
connecting tube
condenser pipe
zoopery
bottle
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CN201820788409.8U
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顾哲明
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Jiangsu Wonder Pharmaceutical Technology Co Ltd
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Jiangsu Wonder Pharmaceutical Technology Co Ltd
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Abstract

The utility model discloses a kind of zoopery Rotary Evaporators, including support base, revolving bottle and condenser pipe, the installation end inner wall of the upper bottle body is provided with installation screw thread, the corresponding installation screw thread of the installation end of the lower bottle body is provided with limit rib, the input terminal of the revolving bottle is equipped with connecting tube by spiral mouth spiral, the connecting tube, which corresponds to, is provided with receiving flask below condenser pipe, the outside of the condenser pipe is provided with condensation interlayer, and the output end of the freezing machine inside defeated cold pipe and condensation interlayer by being connected.The zoopery Rotary Evaporators, have convenient for passing through steam extraction substance to animal blood and gas liquid, it is easy to use, convenient for splendid attire liquid bottle body cleaning, the advantages of reducing experimentation cost, solve existing evaporimeter to animal blood and other liquid by evaporated extract matter when it is inconvenient, clear up bottle body inconvenient and high use cost problem.

Description

A kind of zoopery Rotary Evaporators
Technical field
The utility model relates to evaporimeter technical field, specially a kind of zoopery Rotary Evaporators.
Background technique
Rotary Evaporators are a kind of common laboratory apparatus of chemical laboratory, and mainly continuous still is a large amount of at reduced pressure conditions Volatile solvents.Its primary structure is: including condensation segment, exhaust section, linkage section, rotation section, water-bath and controller, condensation Section is rack-mount, and one end of the middle part connection exhaust section of condensation segment, the other end of exhaust section is rotatablely connected by linkage section The bottleneck for rotating section is embedded in liftable water-bath in the lower square box upper end of rotation section, and controller controls the water in water-bath The control of temperature, pressure and motor.
When extracting detection substance to animal blood testing inspection, need to add diluent liquid to blood using to evaporimeter It puts into inside bottle body afterwards, is mostly solid to being evaporated object to evaporate obtained end product, is easily attached to the inner wall of bottle body On, it causes to be difficult to clear up, the test influenced next time carries out, and evaporimeter is bad to the condensation effect of steam at present, to cold Solidifying pipe internal condensation effect is uneven.
A kind of Rotary Evaporators revolving bottle is disclosed in application No. is 201720318312.6, uses separate structure The installation of revolving bottle spiral, easily cause to need inside revolving bottle investment to need to test evaporation object and penetrate between revolving bottle and connect Place influences the leakproofness of revolving bottle and increases the difficulty cleaned to revolving bottle.
Utility model content
The purpose of this utility model is to provide a kind of zoopery Rotary Evaporators, have convenient for animal blood with And gas liquid passes through steam extraction substance, and it is easy to use, convenient for reducing the excellent of experimentation cost to the cleaning of liquid bottle body is contained Point, solve existing evaporimeter to animal blood and other liquid by evaporated extract matter when it is inconvenient, bottle body is cleared up Inconvenience and the high problem of use cost.
To achieve the above object, the utility model provides the following technical solutions: a kind of zoopery Rotary Evaporators, packet Support base, revolving bottle and condenser pipe are included, the revolving bottle includes upper bottle body and lower bottle body, and the upper bottle body top is provided with spiral shell Mouth is revolved, the installation end inner wall of the upper bottle body is provided with installation screw thread, the corresponding installation screw thread setting of the installation end of the lower bottle body There is limit rib, the end of the limit rib is bonded setting with upper bottle body inner wall, branch is fixedly installed in the support base The input terminal of support, the revolving bottle is equipped with connecting tube by spiral mouth spiral, and the connecting tube passes through adjustment axis and support Frame is fixedly mounted, and the support base corresponds to and is provided with thermostat water bath below revolving bottle, in the condenser pipe and connecting tube Portion is connected, and the connecting tube corresponds to and is provided with receiving flask below condenser pipe, and the input terminal of the connecting tube passes through spiral Seat spiral is equipped with commissioning pipe, and the outside of the condenser pipe is provided with condensation interlayer, is fixedly installed at the top of support frame as described above Freezing machine, the output end of the freezing machine inside defeated cold pipe and condensation interlayer by being connected.
Preferably, it is in extend out structure setting that the end of the postive stop baffle, which is flexible glue structure, and the revolving bottle passes through upper bottle Body and lower bottle body are arranged in oval structure.The installation that lower bottle body passes through screw thread and upper bottle body installation end inner wall outside postive stop baffle Thread helix is fixedly mounted, and the postive stop baffle of flexible glue structure be bonded with the inner wall of upper bottle body, avoid the liquid being evaporated it is deep on Between bottle body and lower bottle body.
Preferably, the side that the connecting tube corresponds to adjustment axis is provided with connectivity port, the connecting tube and revolving bottle it Between rotation section is equipped with by connectivity port, the rotation section is fixedly mounted by the end of rotating seat and connectivity port, described Support frame, which is correspondingly connected with above port, is fixedly installed with mounting plate, and is fixedly installed with driving motor by mounting plate, described The output end of driving motor is fixedly connected by driving band with rotation section.Thermostat water bath inner rotation is accepted in revolving bottle rotation When temperature, driving motor drives rotational segment rotation by driving band, and rotational segment drives revolving bottle rotation to make the liquid inside revolving bottle Steam is generated after body thermally equivalent.
Preferably, the rotation section is provided with driving band installation place and engages tooth socket, and by engagement tooth socket to driving band Accept setting.It engages tooth socket to accept driving band, improves driving motor by driving with the stability for driving rotation section rotation.
Preferably, the input terminal that the end of the condenser pipe corresponds to receiving flask is provided with export plate, the end of the export plate End is arranged inside receiving flask.For commissioning pipe to needing the liquid by steam extraction to put into connecting tube, liquid passes through company Adapter tube enter revolving bottle inside, revolving bottle is risen to inside condenser pipe by thermogenetic hot steam, condenser pipe internal condensation at Water droplet, export plate are accepted the water droplet of condenser pipe internal condensation and are exported to receiving flask, avoid condensed water droplet again It is exported by connecting tube to revolving bottle.
Preferably, for the commissioning pipe using capsule structure setting is inhaled, the output end of the commissioning pipe is connected with efferent duct, described The end of efferent duct passes through export plate and is arranged inside connecting tube.Pressing commissioning pipe, which makes to inhale, generates pumping inside the commissioning pipe of capsule structure The Liquid extracting that needs are evaporated in power taking, and installed by the terminal helix that efferent duct passes through export plate and connecting tube, to connection The input terminal of pipe seals, and presses commissioning pipe, is directly output to the liquid inside commissioning pipe under corresponding condenser pipe by efferent duct Inside the connecting tube of square side, to be flowed into inside revolving bottle by connecting tube.
Compared with prior art, the beneficial effects of the utility model are as follows:
1, the utility model lower bottle body installs spiral inner wall installation by postive stop baffle and upper bottle body, and in the outer of condenser pipe Portion's setting condensation interlayer, pressing commissioning pipe makes to generate the liquid pumping that extraction force evaporates needs inside the commissioning pipe for inhaling capsule structure It takes, and is installed by the terminal helix that efferent duct passes through export plate and connecting tube, the input terminal of connecting tube is sealed, pressing feeds intake Pipe is directly output to the liquid inside commissioning pipe below corresponding condenser pipe inside the connecting tube of side by efferent duct, thus It is flowed into inside revolving bottle by connecting tube, keeps suitable temperature according to the needs to liquid evaporation temperature inside thermostat water bath Degree, driving motor drive rotational segment rotation by driving band, and rotational segment drives revolving bottle rotation to keep the liquid inside revolving bottle equal It is even it is heated after generate steam, revolving bottle is risen to inside condenser pipe by thermogenetic hot steam, the cold air that freezing machine operation generates It is exported by defeated cold pipe to condensation interlayer, keeps cold degree to enter condenser pipe inside condenser pipe inside by condensation interlayer Hot steam condensation, condenser pipe internal condensation at water droplet instill receiving flask inside, complete to liquid evaporation extract test effect Fruit;To liquid by revolving bottle being dismantled by spiral mouth, lower bottle body passes through between installation screw thread and upper bottle body after steam extraction Disassembly, to clearing up respectively inside lower bottle body and upper bottle body, postive stop baffle effectively prevents the liquid inside revolving bottle and passes through upper bottle Junction is oozed out between body and lower bottle body, influences the quality extracted to liquid evaporation.
2, the utility model corresponds to the end setting export plate of condenser pipe inside connecting tube, exports plate to condenser pipe inside The water droplet of condensation is accepted and is exported to receiving flask, and condensed water droplet is avoided to export again by connecting tube to revolving bottle.
Detailed description of the invention
Fig. 1 is the utility model overall structure diagram;
Fig. 2 is the utility model revolving bottle structural schematic diagram;
Fig. 3 is the utility model revolving bottle detaching structure schematic diagram.
In figure: 1 support base;11 support frames;111 mounting plates;112 driving motors;113 driving bands;12 connecting tubes;121 Spiral base;122 feeding ports;123 efferent ducts;124 adjustment axis;13 connectivity ports;131 rotation sections;132 rotating seats;1 adjustment axis 124 engagement tooth sockets;14 thermostat water baths;2 condenser pipes;21 condensation interlayers;22 freezing machines;221 defeated cold pipes;23 receiving flasks;231 lead Ejecting plate;3 revolving bottles;31 upper bottle bodies;311 spiral mouths;312 installation screw threads;32 lower bottle bodies;321 postive stop baffles.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work Every other embodiment obtained, fall within the protection scope of the utility model.
Fig. 1-3, a kind of zoopery Rotary Evaporators, including support base 1, revolving bottle 3 and condenser pipe 2 are please referred to, The revolving bottle 3 includes upper bottle body 31 and lower bottle body 32, and 31 top of upper bottle body is provided with spiral mouth 311, the upper bottle body 31 installation end inner wall is provided with installation screw thread 312, and the corresponding installation screw thread 312 of the installation end of the lower bottle body 32 is provided with limit Rib 321, the end of the limit rib 321 are bonded setting with 31 inner wall of upper bottle body, and the end of the postive stop baffle 321 is soft Plastic structure is arranged by upper bottle body and lower bottle body in oval structure in structure setting, the revolving bottle 3 is extended out.Lower bottle body 32 passes through 312 spiral of installation screw thread of screw thread and 31 installation end inner wall of upper bottle body outside postive stop baffle 321 is fixedly mounted, flexible glue structure Postive stop baffle 321 is bonded with the inner wall of upper bottle body 31, is blocked to installation place between upper bottle body 31 and lower bottle body 32, is avoided being evaporated Liquid go deep between upper bottle body 31 and lower bottle body 32.Support frame 11, the revolving bottle are fixedly installed in the support base 1 3 input terminal is equipped with connecting tube 12 by 311 spiral of spiral mouth, and the connecting tube 12 passes through adjustment axis 124 and support frame 11 It is fixedly mounted, the side of the corresponding adjustment axis 124 of the connecting tube 12 is provided with connectivity port 13, the connecting tube 12 and revolving bottle Rotation section 131 is equipped with by connectivity port 13 between 3, the rotation section 131 passes through the end of rotating seat 132 and connectivity port 13 End is fixedly mounted, and the top that support frame as described above 11 is correspondingly connected with port 13 is fixedly installed with mounting plate 111, and passes through mounting plate 111 are fixedly installed with driving motor 112, and the output end of the driving motor 112 is fixed by driving band 113 and rotation section 131 Connection.When the rotation of revolving bottle 3 accepts temperature to 14 inner rotation of thermostat water bath, driving motor 112 is driven by driving band 113 Rotational segment 131 rotates, and rotational segment 131 generates steam after driving revolving bottle 3 to rotate the liquid thermally equivalent made inside revolving bottle 3. The rotation section 131 is provided with driving 112 installation place of band and engages 133 adjustment axis 124 of tooth socket, and is adjusted by engagement tooth socket 133 124 pairs of driving bands 113 of nodal axisn accept setting.It engages 133 adjustment axis of tooth socket, 124 pairs of driving bands 113 to accept, improves driving motor 112 stability for driving rotation section 131 to rotate by driving band 113.The lower section setting of the corresponding revolving bottle 3 of the support base 1 There is thermostat water bath 14, be connected inside the condenser pipe 2 and connecting tube 12, under the corresponding condenser pipe 2 of the connecting tube 12 Side is provided with receiving flask 23, and the input terminal of the connecting tube 12 is equipped with commissioning pipe 122 by 121 spiral of spiral base, described cold The outside of solidifying pipe 2 is provided with condensation interlayer 21, and the top of support frame as described above 11 is fixedly installed with freezing machine 22, the freezing machine 22 Output end by defeated cold pipe 221 with condense interlayer 21 inside be connected.The end of the condenser pipe 2 corresponds to receiving flask 23 Input terminal is provided with export plate 231, and the end of the export plate 231 is arranged inside receiving flask 23.122 pairs of commissioning pipe need to lead to The liquid for crossing steam extraction is put into connecting tube 12, liquid by connecting tube 12 enter revolving bottle 3 inside, revolving bottle 3 by Thermogenetic hot steam rises to inside condenser pipe 2, in 2 internal condensation of condenser pipe at water droplet, exports plate 231 in condenser pipe 2 The water droplet of portion's condensation is accepted and is exported to receiving flask 23, avoids condensed water droplet again by the output of connecting tube 12 to rotation Rolling bottle 3.For the commissioning pipe 122 using capsule structure setting is inhaled, the output end of the commissioning pipe 122 is connected with efferent duct 123, described The end of efferent duct 123 passes through export plate 231 and is arranged inside connecting tube 12.Pressing commissioning pipe 122 makes to inhale feeding intake for capsule structure The Liquid extracting that extraction force evaporates needs is generated inside pipe 122, and export plate 231 and connecting tube are passed through by efferent duct 123 12 terminal helix installation, seals the input terminal of connecting tube 12, presses commissioning pipe 122, keeps the liquid inside commissioning pipe 122 logical It crosses efferent duct 123 to be directly output to inside the connecting tube 12 of corresponding 2 lower section side of condenser pipe, to flow into rotation by connecting tube 12 Inside rolling bottle 3.
In use, pressing commissioning pipe 122 makes to generate the liquid that extraction force evaporates needs inside the commissioning pipe 122 for inhaling capsule structure Body extracts, and is installed by the terminal helix that efferent duct 123 passes through export plate 231 and connecting tube 12, the input to connecting tube 12 End sealing, presses commissioning pipe 122, and the liquid inside commissioning pipe 122 is made to be directly output to corresponding condenser pipe 2 by efferent duct 123 Inside the connecting tube 12 of lower section side, to be flowed into inside revolving bottle 3 by connecting tube 12, according to right inside thermostat water bath 14 The needs of liquid evaporation temperature keep suitable temperature, and driving motor 112 drives rotational segment 131 to rotate by driving band 113, turn Dynamic section 131 generates steam after driving revolving bottle 3 to rotate the liquid thermally equivalent made inside revolving bottle 3, and revolving bottle 3 is by thermogenetic Hot steam rises to inside condenser pipe 2, and the cold air that the operation of freezing machine 22 generates passes through in the defeated cold output of pipe 221 to condensation interlayer 21 Portion, by condensation interlayer 21 to keeping cold degree to condense the hot steam entered inside condenser pipe 2 inside condenser pipe 2, in condenser pipe 2 Internal condensation instills inside receiving flask 23 at water droplet, completes the effect that test is extracted to liquid evaporation;Liquid is mentioned by steam After taking, revolving bottle 3 is dismantled by spiral mouth 311, lower bottle body 32 is right by dismantling between installation screw thread 312 and upper bottle body 31 It is cleared up respectively inside lower bottle body 31 and upper bottle body 32, postive stop baffle 321 effectively prevents the liquid inside revolving bottle 3 and passes through upper bottle Junction is oozed out between body 31 and lower bottle body 32, influences the quality extracted to liquid evaporation.
In summary: the zoopery Rotary Evaporators, lower bottle body 32 are installed by postive stop baffle 321 and upper bottle body 31 Spiral inner wall installation, and in the external setting condensation interlayer 21 of condenser pipe 2, pressing commissioning pipe 122 makes the commissioning pipe for inhaling capsule structure 122 inside generate the Liquid extracting that extraction force evaporates needs, and pass through export plate 231 and connecting tube 12 by efferent duct 123 Terminal helix installation, the input terminal of connecting tube 12 is sealed, commissioning pipe 122 is pressed, passes through the liquid inside commissioning pipe 122 Efferent duct 123 is directly output to inside the connecting tube 12 of corresponding 2 lower section side of condenser pipe, to flow into rotation by connecting tube 12 Inside bottle 3,14 inside of thermostat water bath keeps suitable temperature according to the needs to liquid evaporation temperature, and driving motor 112 is logical Band 113 of overdriving drives rotational segment 131 to rotate, and rotational segment 131 drives the rotation of revolving bottle 3 to keep the liquid inside revolving bottle 3 uniform Steam is generated after heated, revolving bottle 3 is risen to inside condenser pipe 2 by thermogenetic hot steam, and the operation of freezing machine 22 generates cold Gas by defeated cold pipe 221 output to condensation interlayer 21 inside, by condensation interlayer 21 to kept inside condenser pipe 2 cold degree to condensation The hot steam condensation entered inside pipe 2, instills inside receiving flask 23 in 2 internal condensation of condenser pipe at water droplet, completes to steam liquid Hair extracts the effect of test;To liquid by revolving bottle 3 being dismantled by spiral mouth 311, lower bottle body 32 passes through after steam extraction It is dismantled between installation screw thread 312 and upper bottle body 31, to clearing up respectively inside lower bottle body 31 and upper bottle body 32, postive stop baffle 321 has Effect avoids the liquid inside revolving bottle 3 and passes through junction exudation between upper bottle body 31 and lower bottle body 32, solves existing evaporation Inconvenient, and use cost inconvenient to bottle body cleaning when instrument passes through evaporated extract matter to animal blood and other liquid High problem.
While there has been shown and described that the embodiments of the present invention, for the ordinary skill in the art, It is understood that these embodiments can be carried out with a variety of variations in the case where not departing from the principles of the present invention and spirit, repaired Change, replacement and variant, the scope of the utility model is defined by the appended claims and the equivalents thereof.

Claims (6)

1. a kind of zoopery Rotary Evaporators, including support base (1), revolving bottle (3) and condenser pipe (2), the rotation Bottle (3) includes upper bottle body (31) and lower bottle body (32), and upper bottle body (31) top is provided with spiral mouth (311), and feature exists In: the installation end inner wall of the upper bottle body (31) is provided with installation screw thread (312), the corresponding peace of the installation end of the lower bottle body (32) Dress screw thread (312) is provided with postive stop baffle (321), and the end of the postive stop baffle (321) is bonded with upper bottle body (31) inner wall to be set It sets, is fixedly installed with support frame (11) on the support base (1), the input terminal of the revolving bottle (3) passes through spiral mouth (311) Spiral is equipped with connecting tube (12), and the connecting tube (12) is fixedly mounted by adjustment axis (124) and support frame (11), the branch Support pedestal (1) is provided with thermostat water bath (14) below corresponding revolving bottle (3), in the condenser pipe (2) and connecting tube (12) Portion is connected, and the connecting tube (12) is provided with receiving flask (23) below corresponding condenser pipe (2), the connecting tube (12) Input terminal is equipped with commissioning pipe (122) by spiral base (121) spiral, and the outside of the condenser pipe (2) is provided with condensation interlayer (21), it is fixedly installed with freezing machine (22) at the top of support frame as described above (11), the output end of the freezing machine (22) passes through defeated cold It is connected inside pipe (221) and condensation interlayer (21).
2. a kind of zoopery Rotary Evaporators according to claim 1, it is characterised in that: the postive stop baffle (321) end is flexible glue structure in structure setting is extended out, and the revolving bottle (3) passes through upper bottle body (31) and lower bottle body (32) is in Oval structure setting.
3. a kind of zoopery Rotary Evaporators according to claim 1, it is characterised in that: the connecting tube (12) is right It answers the side of adjustment axis (124) to be provided with connectivity port (13), passes through connecting pin between the connecting tube (12) and revolving bottle (3) Mouth (13) is equipped with rotation section (131), and rotation section (131) is consolidated by the end of rotating seat (132) and connectivity port (13) Dingan County's dress, support frame as described above (11), which is correspondingly connected with above port (13), is fixedly installed with mounting plate (111), and passes through mounting plate (111) it is fixedly installed with driving motor (112), the output end of the driving motor (112) passes through driving band (113) and rotation section (131) it is fixedly connected.
4. a kind of zoopery Rotary Evaporators according to claim 3, it is characterised in that: the rotation section (131) It is provided with and engages tooth socket (133) with driving band (113) installation place, and driving band (113) is accepted by engagement tooth socket (133) and is set It sets.
5. a kind of zoopery Rotary Evaporators according to claim 1, it is characterised in that: the condenser pipe (2) The input terminal that end corresponds to receiving flask (23) is provided with export plate (231), and the end of export plate (231) is arranged in receiving flask (23) internal.
6. a kind of zoopery Rotary Evaporators according to claim 5, it is characterised in that: the commissioning pipe (122) Using capsule structure setting is inhaled, the output end of the commissioning pipe (122) is connected with efferent duct (123), the end of the efferent duct (123) End is internal in connecting tube (12) across export plate (231) setting.
CN201820788409.8U 2018-05-25 2018-05-25 A kind of zoopery Rotary Evaporators Active CN208493251U (en)

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CN201820788409.8U CN208493251U (en) 2018-05-25 2018-05-25 A kind of zoopery Rotary Evaporators

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113171626A (en) * 2021-03-22 2021-07-27 重庆赛维药业有限公司 Preparation facilities of pregabalin intermediate compound
CN115521829A (en) * 2022-10-19 2022-12-27 湖北瑞晟生物有限责任公司 Rose liquid distillation plant

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113171626A (en) * 2021-03-22 2021-07-27 重庆赛维药业有限公司 Preparation facilities of pregabalin intermediate compound
CN113171626B (en) * 2021-03-22 2022-07-26 重庆赛维药业有限公司 Preparation facilities of pregabalin intermediate compound
CN115521829A (en) * 2022-10-19 2022-12-27 湖北瑞晟生物有限责任公司 Rose liquid distillation plant

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